A convenient and economic method for preparing highly ordered MCM 41 was studied in an open vessel by using waterglass as the silicon source. XRD, nitrogen adsorption and TEM show that the product has a highly ordered...A convenient and economic method for preparing highly ordered MCM 41 was studied in an open vessel by using waterglass as the silicon source. XRD, nitrogen adsorption and TEM show that the product has a highly ordered structure and the hexagonal arrangements of uniformly size pores distribution.展开更多
The β CD was first successfully introduced into the pore of MCM 41 mesoporous sieve, with γ glycidoxypr opyltrimethoxy silane (GPTS) as a coupling agent. An inorganic/organic complex mesoporous material β CD MCM 41...The β CD was first successfully introduced into the pore of MCM 41 mesoporous sieve, with γ glycidoxypr opyltrimethoxy silane (GPTS) as a coupling agent. An inorganic/organic complex mesoporous material β CD MCM 41 was synthesized, and characterized by XRD, nitrogen adsorption desorption, elemental analysis, FT IR and spectrophotofluorimetry. The results show that β CD molecular not only get into the modified inner wall, but also remain the ordered mesoporou structure of MCM 41.展开更多
文摘A convenient and economic method for preparing highly ordered MCM 41 was studied in an open vessel by using waterglass as the silicon source. XRD, nitrogen adsorption and TEM show that the product has a highly ordered structure and the hexagonal arrangements of uniformly size pores distribution.
文摘The β CD was first successfully introduced into the pore of MCM 41 mesoporous sieve, with γ glycidoxypr opyltrimethoxy silane (GPTS) as a coupling agent. An inorganic/organic complex mesoporous material β CD MCM 41 was synthesized, and characterized by XRD, nitrogen adsorption desorption, elemental analysis, FT IR and spectrophotofluorimetry. The results show that β CD molecular not only get into the modified inner wall, but also remain the ordered mesoporou structure of MCM 41.