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电感耦合等离子体原子发射光谱法同时测定电池级硫酸钴中12种杂质元素
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作者 佡云 马晓卉 《有色矿冶》 2024年第4期58-61,共4页
采用低温多酸溶样,利用电感耦合等离子体原子发射光谱仪(ICP-AES)同时测定电池级硫酸钴中12种杂质元素,并对仪器参数及被测元素谱线的选择进行了讨论。在选定的测量条件下,本文所述分析方法与原子吸收光谱法的测定结果进行了对比,结果... 采用低温多酸溶样,利用电感耦合等离子体原子发射光谱仪(ICP-AES)同时测定电池级硫酸钴中12种杂质元素,并对仪器参数及被测元素谱线的选择进行了讨论。在选定的测量条件下,本文所述分析方法与原子吸收光谱法的测定结果进行了对比,结果表明各元素分析误差均在允许范围内。通过对试料中待测的12种杂质元素进行多次反复测定,并对方法的检出限、精密度及加标回收率等指标进行了考察,该方法相对标准偏差小于2%,回收率为98%~100%。使用了合适的样品前处理方法和仪器分析条件,经过反复多次试验,确定了合适的分析条件,有效地实现了快速、高效地测定电池级硫酸钴中12种杂质元素。操作简便,准确性高,适合推广应用。 展开更多
关键词 低温多酸 ICP-AES 电池级硫
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Effects of polyphosphoric acid modified asphalt on the low-temperature cracking of asphalt mixtures 被引量:3
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作者 丁海波 张华 王郴平 《Journal of Southeast University(English Edition)》 EI CAS 2016年第2期215-218,共4页
In order to determine whether polyphosphoric acid (PPA) can partially or completely substitute styrene-butadiene- styrene (SBS) modifier while it does not adversely affect the resistance to thermal cracking of the... In order to determine whether polyphosphoric acid (PPA) can partially or completely substitute styrene-butadiene- styrene (SBS) modifier while it does not adversely affect the resistance to thermal cracking of the asphalt mixture, the low- temperature fracture properties of the PPA modified mixtures are evaluated and compared to the SBS modified mixtures. First, laboratory compacted test samples were tested by the indirect tensile test (IDT) and the newly developed fracture testing protocol, named as disk-shaped compact tension (DCT). Then, the effects of the test temperature and air-void ratio on the low-temperature fracture properties of asphalt mixtures were analyzed. The results show that the fracture resistance of the PPA modified mixtures is worse than that of the SBS modified mixtures. However, for those modified mixtures that use the PPA substituting part of the SBS modifier, a relatively low-temperature fracture resistance can be obtained compared with the mixture only using the SBS modifier. 展开更多
关键词 asphalt mixture low temperature polyphosphoricacid disk-shaped compact tension
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