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固相萃取/高效液相色谱法对中成药和保健品中7种降糖化学药物的测定 被引量:25
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作者 朱炳辉 龙朝阳 +1 位作者 吴西梅 杨杏芬 《分析测试学报》 CAS CSCD 北大核心 2008年第5期534-537,541,共5页
建立了一种固相萃彬高效液相色谱测定保缝品中格列吡嗪、格列齐特、格列本脲、格列喹酮、盐酸二甲双胍、盐酸苯乙双胍和瑞格列奈7种降糖化学药物的方法。采用阳离子固相萃取柱,对提取液进行净化处理。得到的不同洗脱液分别进样,用液... 建立了一种固相萃彬高效液相色谱测定保缝品中格列吡嗪、格列齐特、格列本脲、格列喹酮、盐酸二甲双胍、盐酸苯乙双胍和瑞格列奈7种降糖化学药物的方法。采用阳离子固相萃取柱,对提取液进行净化处理。得到的不同洗脱液分别进样,用液相色谱进行分析,采用ZORBAXSB—C18柱,以乙腈-0.02mol/L磷酸缓冲盐(pH2.8)作为流动相进行梯度洗脱,7个色谱峰分离良好,两次进样在40min内可以完成,外标法定量。在3种不同剂型中药制剂中的添加回收率在83%~101%之间。 展开更多
关键词 高效液相色谱 固相萃取 降糖药物 保缝食品
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谷氨酰胺对极低出生体重儿近期预后的影响 被引量:3
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作者 林敏 杨长仪 +2 位作者 陈义忠 陈烈平 陈涵强 《海峡预防医学杂志》 CAS 2007年第5期78-79,共2页
[目的]检验生后早期常规口服谷氨酰胺(glutamine,Gln)对极低出生体重儿(VLBWI)近期预后的影响,并探讨在VLBWI中,补充Gln与血浆白细胞介素6(IL-6)和白细胞介素8(IL-8)浓度、院内感染、喂养及生长发育间的关系。[方法]将58例VLBWI随机分... [目的]检验生后早期常规口服谷氨酰胺(glutamine,Gln)对极低出生体重儿(VLBWI)近期预后的影响,并探讨在VLBWI中,补充Gln与血浆白细胞介素6(IL-6)和白细胞介素8(IL-8)浓度、院内感染、喂养及生长发育间的关系。[方法]将58例VLBWI随机分为口服Gln 0.3 g/(kg.d)的实验组和进行标准肠道喂养的对照组。比较患儿对喂养的耐受能力、几种严重感染的发生率等近期预后以及生后第1、第7和第14 d的血浆GlnI、L-6和IL-8的浓度。[结果]口服Gln能缩短VLBWI从开奶到能够耐受全肠道喂养的时间。Gln组感染发生率也低于对照组,但两组生后恢复出生体重所需的时间,以及体重增长速度相近。血浆中GlnI、L-6和IL-8的浓度也没有明显差异。[结论]口服Gln能改善VLBWI对喂养的耐受能力并降低感染发生率,但并不能改变血浆中GlnI、L-6和IL-8的浓度。 展开更多
关键词 早产儿保缝 谷氨酰胺 肠道营养 IL-6 IL-8
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重庆市北碚区学校卫生监督工作的几点经验
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作者 吴德培 胡泽鑫 《中国学校卫生》 CAS 北大核心 2008年第10期969-970,共2页
关键词 组织和管理 在职培训 学生保缝服务
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谷类食物营养价值与强化分析——食物分类、谷类食物营养分析及营养强化
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作者 戴智勇 张岩春 《农产食品科技》 2010年第4期56-58,共3页
谷类食物是人类的主要食物,它含有丰富的营养,本文介绍了谷类及谷类食物的分类,对谷类食物的营养价值、保健作用等进行了阐述,并对谷类食物营养强化进行了分析和比较研究。
关键词 谷类食物 保缝 营养强化
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Characteristics of fracture development and gas extraction of a lower protected seam
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作者 王海锋 《Journal of Chongqing University》 CAS 2009年第4期239-244,共6页
To ensure the mining safety of working face in the protective seam and meanwhile extract pressure-relief gas of the lower protected seam and eliminate its outburst risk,the present study researched into fracture devel... To ensure the mining safety of working face in the protective seam and meanwhile extract pressure-relief gas of the lower protected seam and eliminate its outburst risk,the present study researched into fracture development of floor coal-rock mass of the protective seam and migration rule of pressure-relief gas from a protected seam so as to obtain an effective pressure- relief gas extraction method.The results show that after the upper protective seam was mined,mining-induced fracturing floor coal-rock mas... 展开更多
关键词 short distance protective seam gas emission penetration borehole gas extraction
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Robowler:Design and development of a cricket bowling machine ensuring ball seam position
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作者 RAZA Ali DIEGEL Olaf ARIF Khalid Mahmood 《Journal of Central South University》 SCIE EI CAS 2014年第11期4142-4149,共8页
The art of cricket bowling is complex and arduous owing to the run-up and ball release time energy requirement to achieve speed and variations. Therefore, human bowlers cannot bowl for extended periods and numerous me... The art of cricket bowling is complex and arduous owing to the run-up and ball release time energy requirement to achieve speed and variations. Therefore, human bowlers cannot bowl for extended periods and numerous mechanical bowling machines have been built to help batsmen improve their skills during practice sessions. However, most of these existing machines are designed for spherical balls ignoring the distinguishing physical feature of a cricket ball: the raised equatorial seam, which makes it less of a sphere. The bowlers are known to often benefit from this seam in their pursuit to taking the batsmen's wicket by imparting swing, spin and bounce variations along-with other bowling variables. This lack of the seam consideration creates a void between human and mechanical bowling. In this work, we present design and development of an automatic bowling machine termed as ROBOWLER to make mechanical bowling more realistic. This machine ensures ball seam position as well as fulfills other constraints. Ball pitching and seam position accuracy results underscore the suitability of this design to enhance the capabilities of mechanical bowling. 展开更多
关键词 robowler bowling machine cricket bowling ball seam bowling variables
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Effect of post weld heat treatment on microstructure and mechanical properties of gas tungsten arc welded AA6061-T6 alloy 被引量:4
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作者 Firouz FADAEIFARD Khamirul Amin MATORI +2 位作者 Farhad GARAVI Muath Al-FALAHI Gholamreza Vahedi SARRIGANI 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2016年第12期3102-3114,共13页
Double-V butt TIG welding process was performed on two plates of AA6061-T6 using ER5356 filler. The microstructure,mechanical and nanomechanical properties of the joint were evaluated in as-welded and after post weld ... Double-V butt TIG welding process was performed on two plates of AA6061-T6 using ER5356 filler. The microstructure,mechanical and nanomechanical properties of the joint were evaluated in as-welded and after post weld heat treatment (PWHT) usingXRD, FESEM, EBSD, nanoindentation and tensile tests. The results show that PWHT led to microstructural recovery of the heataffected zone (HAZ) in addition to the appearance of β-phase (Al3Mg2) at the grain boundaries of weld zone. The hardness (Hnano) inall zones increased after PWHT while the elastic modulus (Enano) was improved from 69.93 GPa to 81 GPa in weld area. All resultsindicate that PWHT has created a homogenous microstructure in the weld zone in addition to outstanding improvement inmechanical properties for the weld zone which surpass the base metal. 展开更多
关键词 AA6061-T6 alloy ER5356 gas tungsten arc welding post weld heat treatment NANOINDENTATION microstructure
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Microstructures and mechanical properties of a martensitic steel welded with flux-cored wires 被引量:1
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作者 Weiqiang Zhang Zhimin Zhong Shaoguang Kang 《International Journal of Coal Science & Technology》 EI 2015年第3期254-260,共7页
This study was focused on wear-resistant material prepared by CO2 GMAW method to basically determine the alloys and hardfacing technology which could be employed into mining equipment. Three flux-cored wires with diff... This study was focused on wear-resistant material prepared by CO2 GMAW method to basically determine the alloys and hardfacing technology which could be employed into mining equipment. Three flux-cored wires with different chemical compositions, marked by DM-I, DM-II and DM-III were used in welding a martensitic steel for the comparison of the microstructures and mechanical properties of the welding metals and HAZ. The results show that DM-I weld metal contains martensite plus other reinforced phases, while both DM-II and DM-III alloys lead to mainly martensitic microstructures with little precipitates. Among all of the tested materials the DM-I alloy has the highest hardness and wear resistance but the lowest impact toughness among the experimental weld metals. Meanwhile, the hardness, impact toughness and wear resistance of the DM-II and DM-III alloys are close to those of the base metal but the DM-III is not as strong as DM-II. Dimples can be found on the impact fracture of the weld metals, but the steel fracture consists of both cleavage and dimples. Thus HAZ has less risk for cracking than the welds, and the DM-II wire which produces the weld having identical mechanical properties to the base metal is suitable for further application. 展开更多
关键词 HARDFACING MICROSTRUCTURE Mechanical property Flux-cored wire GMAW
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中小血管吻合的连续缝合和间断缝合法对比研究 被引量:2
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作者 向志 时德 《中华实验外科杂志》 CAS CSCD 北大核心 1996年第6期326-326,共1页
中小血管吻合技术已广泛应用于外科领域。我们通过缝合时间、吻合口漏血及通畅情况,组织形态学等方面,对连续缝合和间断缝合法进行对比研究,着重对术后内皮细胞跨越吻合口的变化过程及血管壁愈合过程进行对比分析,为临床两种血管吻合法... 中小血管吻合技术已广泛应用于外科领域。我们通过缝合时间、吻合口漏血及通畅情况,组织形态学等方面,对连续缝合和间断缝合法进行对比研究,着重对术后内皮细胞跨越吻合口的变化过程及血管壁愈合过程进行对比分析,为临床两种血管吻合法的选择提供实验依据。材料和方法选用健康家犬18条,体重10~15kg,每条犬分别在左右侧股动脉采用7-0无损伤带针尼龙缝线行两定点连续缝合和间断缝合,缝合针数均在16~18针之间。记录缝合时间,观察吻合口漏血情况,并于术后1小时、24小时、3天、7天、14天、21天、28天、56天、91天解剖动物,解剖前经腹主动脉穿刺行双侧股动脉造影,解剖后观察吻合口通畅情况并取吻合口处血管行光镜、扫描电镜及透射电镜检查。 展开更多
关键词 血管吻合术 连续 间断
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