傅玉书父子与《潘氏八世诗集》

《潘氏八世诗集》是一部艺术价值高、教化功能强的诗歌总集,是贵州明清之际著名的文人家集,是贵州诗史中光彩夺目的篇章。诗集中有不少名宦才人为该集写序跋文,从而增添了含金量。其中傅玉书父子撰写了七篇诗序,实为难得一见的新史料。

Fast Digital Correlation Calculation Method in Extended Beacon Wavefront Detection

On the basis of Hartmann Shack sensor imaging analysis, a new method is presented with which the wavefront slope can be obtained when the object is incoherent and extended. This method, which is demonstrated by both theoretical interpreting and computer simulation, explains how to measure the wavefront slope difference between two sub apertures through the determination of image displacements on detector plane. It includes a fast and accurate digital algorithm for detecting wavefront disturbance, which is much suitable for realization in such electrical hardwares as digital signal processors.

Estimation of structural modal parameters by fourier transform with an optimal window

An adaptive Fourier Transform （FT） with an optimal window has been proposed for the time-frequency analysis of nonstationary time series. The method allows for a good estimation of both frequency and amplitude of the spectrum and can be easily applied to the general case of time-varying signals. The evaluation of the proposed approach has been performed on measured time-varying signals from a suspension bridge model and a steel frame model whose data have the typical non-stationary characteristics. The numerical results show that the proposed approach can overcome some of the difficulties encountered in the classic Fourier transform technique and can achieve higher computation accuracy.

Development of Instrument Control System Using Biosignals Created by the Change of Eyes Movement Sequence

A new biosi gn al control system that offers the disables the opportunities to control electric appliances is proposed.The four types of signals created by the eyes movements in four directions(up,down,left,and right),which are taken as four basic signals , are detected at the forehead.Permutation of 2 signals out of them creates 16 d ifferent signals.Permutation of 3 signals out of them creates 64 signals.They al l amounts to 84 control signals.They are thought to be applicable for the operat ion of some instruments.Furthermore,the dynamic biosignals created by the slow e yes movement is speculated to be applicable for the more convenient control of t hem.

Synthesis of ITQ-2 Zeolites and Catalytic Performance in n-Dodecane Cracking

ITQ-2 zeolites were prepared by sequential alkali-swelling and ultrasonic-delamination of precursor MCM-22 and characterized by X-ray powder diffraction, scanning electron microscopy, nitrogen adsorption-desorption, ammonia temperature-programmed desorption and in-situ Fourier-transform infrared spectroscopy. The delamination induced a change in the morphology of ITQ-2 zeolites from aggregated thin platelets to scattered platelets, together with a significant increase in external specific surface area, which reached a plateau at the ultrasonic treatment time of 3 h. The catalytic cracking of n-dodecane over ITQ-2 zeolites was evaluated with ITQ-2 coated on the inside wall of a tubular reactor at 550 ℃ and 4 MPa. The sample obtained by ultrasonic treatment of 3 h （ITQ-2-3） gave the highest initial conversion of n-dodecane, whereas those of 5 h and I h gave the conversion even lower than MCM-22, which was in agreement with the trend of the ratio of strong Lewis acid to the total acid amount. Although the amount of cokes deposited on ITQ-2-3 was larger than that on MCM-22, the former deactivated slowly, suggesting that a large external specific surface area benefits the stability of zeolite coatings,

The HAUSDORFF DIMENSION AND MEASURE OF THE GENERALIZED MORAN FRACTALS AND FOURIER SERIES

This paper studies the Hausdorff dimensions, the Hausdorff measures of generalized Moranfrontals and the convergence of the Fourier series of functions defined on some generalizedMoran fractals. A general formula is given for the calculatinn of the Hausdorff dimensions ofgeneralized Moran fractals and it is proved that their Hausdorff measures are finite positivenumbers under some conditions. In addition, the authors define an orthonormal system offunctions defilled on generalized Moran s-sets (gMs) and discuss the convergence of the Fourierseries, with respect to of each function f(x) E L1(gMs, Hs).

Easily prepared and stable functionalized magnetic ordered mesoporous silica for efficient uranium extraction

Functionalized magnetic Fe_3O_4@SiO_2 composite nanoparticles were prepared by simply embedding iron oxide nanoparticles into MCM-41 through one-step synthesis process, followed by aminopropyls grafting on the mesopore channels, aiming to efficiently and conveniently uptake U(VI) from aqueous solution. The resultant material possesses highly ordered mesoporous structure with large surface area, uniform pore size, excellent thermal stability, quick magnetic response, and desirable acids resistance, confirmed by Fourier transform infrared spectroscopy(FTIR), scanning electron microscopy(SEM), N_2 adsorption/desorption experiments, powder X-ray diffraction(PXRD), and thermogravimetric analysis(TGA). Detailed U(VI) sorption test indicated that this material is indeed an effective U(VI) sorbent with fast sorption kinetics of less than 2 h, large sorption capacity of 160 mg/g at p H 5.0±0.1, and desirable selectivity towards U(VI) ions over a range of competing metal ions. The absorbed U(VI) can be easily desorbed by 0.01 mol/L or more concentrated HNO_3 solution, and the reclaimed sorbent can be reused with no obvious decrease of sorption capacity even after 4 sorption-desorption cycles. The present results suggest the vast opportunities of this kind of magnetic composite on the solid-phase extraction of U(VI).

On temporal-spatial distribution of backscatter coefficients over China determined by TOPEX/Poseidon mission

This paper deals with the backscatter coefficients known as sigma0 at Ku band and C band based on the GDR-M (Merged Geophysical Data Record) of TOPEX/Poseidon (T/P) through Jan.1993 to Dec.2004 over land surface of China.After smoothing and interpolating the backscatter coefficients for both bands, we achieve the 5′×5′ grid data and the time series of backscatter coefficients in 12 years.The spatial distribution of sigma0 over typical areas (wetland, desert, mountainous area, agriculture base, etc.) of Chinese territory is analyzed and discussed.The fast Fourier transformation (FFT) is used to detect the cycles of seasonal variations of sigma0 time series and gives that the annual period is the major cycle.Meanwhile a semiannual period is also found in some places.We use the least squares method on both periods and find that the amplitude of annual period is obviously greater than that of semi-annual period.The relationship among the anomalousness of time series, variations of environment and climate change, and the serious natural calamity (flood, drought) is also discussed.Data of topography slope extracted from SRTM are used to do correlation analysis with the backscatter coefficients in parts of China to quantify the impact of slope on backscatter coefficients in Ku and C bands, and the results show that they all have a negative correlation but the magnitudes are different in different places with different coverages.Such as the area of Liaoning and Jilin has the maximum correlation -0.56, the Taklimakan Desert has the minimum correlation -0.11, and the other places commonly have correlations in (-0.3, -0.5).

New synthetic procedure for Na NH_2(BH_3)_2 and evaluation of its hydrogen storage properties

Tremendous efforts have been devoted to the synthesis of new light element hydrides for hydrogen storage. Ammonia borane （AB） is a promising candidate possessing high hydrogen capacity and low dehydrogenation temperature. The step-wise dehydrogenation and release of by-products, however, are obstacles to its practical application. Chemical modifications of AB to synthesize new compounds or its derivatives are of practical and fundamental importance. Here we report an improved synthesis of sodium aminodiborane （NaNH2（BH3）2, NaABB）, a derivative of ammonia borane. This procedure leads to high purity NaABB by reacting NaNH2 and 2 eq. AB. The dehydrogenation properties have been investigated by means of temperature programmed desorption-mass spectrometry, volumetric release, nuclear magnetic resonance, Fourier transform infrared spectroscopy, and X-ray diffraction. In a closed vessel, NaABB can release -2 eq. H2 when heated at 271 ℃, forming solid products of NaBH4 and highly condensed polyborazylene.