基于傅立叶变换的电能质量分析

在对电能质量问题进行研究探讨的基础上,提出基于傅立叶变换的电能质量分析方法。利用快速傅立叶算法完成稳态电能质量的检测,然后利用MATLAB软件进行仿真试验,并得到对实际生产有意义的结果,证明该分析方法具有实用性和可行性,可为电能质量分析提供新思路。

圆板振子超谐分岔和混沌运动的实验研究

设计了非线性圆板混沌实验振动台 .就轴对称圆板在简谐载荷作用下的非线性动力学行为进行了较为系统的实验研究、理论分析和数值计算 .对基础作简谐运动 ,周边固支圆板 ,进行了实验 .通过测量时间—中心挠度的加速度曲线 ,进行快速傅立叶变换 (FFT)分析 ,实验发现了对称破缺 ,超谐分岔 ,调幅调相等复杂现象 ;对基础作简谐运动 ,周边固支 ,中心加质量块的圆板 ,进行了实验 .通过测量时间—周边应变曲线 ,进行 FFT分析 ,实验发现了混沌。

Carbonization mechanism of bamboo (phyllostachys) by means of Fourier Transform Infrared and elemental analysis

通过测定在200-600℃炭化竹材得到的固体产物的碳、氢、氧元素的含量及它们的红外光谱,研究了在炭化过程中竹材中半纤维素、纤维素及木素的变化规律。结果表明,结合元素分析,红外光谱分析方法是研究竹材炭化机理的有效手段。在200℃以前,竹材中的半纤维素和纤维素的大量羟基断裂,并结合成水而失去。在200-250℃之间,竹材中的纤维素被降解,其中的吡喃型环也遭到破坏。并且木素中的甲氧基也被脱去。竹材中的木素网状结构在250-400℃之间遭到完全的破坏。竹炭中的碳原子在600℃已基本上完成了芳环化。图3表2参15。

Estimation of structural modal parameters by fourier transform with an optimal window

An adaptive Fourier Transform （FT） with an optimal window has been proposed for the time-frequency analysis of nonstationary time series. The method allows for a good estimation of both frequency and amplitude of the spectrum and can be easily applied to the general case of time-varying signals. The evaluation of the proposed approach has been performed on measured time-varying signals from a suspension bridge model and a steel frame model whose data have the typical non-stationary characteristics. The numerical results show that the proposed approach can overcome some of the difficulties encountered in the classic Fourier transform technique and can achieve higher computation accuracy.

Construction of a macromolecular structural model of Chinese lignite and analysis of its low-temperature oxidation behavior

The aim of this paper is to analyze the change in the active structure of lignite during the process of lowtemperature oxidation by constructing a molecular structure model for lignite. Using quantum computation combined with experimental results of proximate analysis, ultimate analysis, Fourier transform infrared spectroscopy(FTIR) and X-ray photoelectron spectroscopy(XPS), a structural model for the large molecular structure was constructed. By analyzing the bond lengths in the model molecule, the evolution law for the active structure of lignite was predicted for the process of low-temperature oxidation. In low-temperature oxidation,alkanes and hydroxyls are the primary active structures observed in lignite, though ether may also react. These active functional groups react with oxygen to release heat, thereby speeding up the reaction between coal and oxygen. Finally, the content of various functional groups in the process of lignite low-temperature oxidation was analyzed by infrared analysis, and the accuracy of the model was verified.

Effect of temperature and stress on molecular structure and carbon monoxide generation of lignite from Kailuan mining area

In order to analyze the origin of carbon monoxide(CO) in coal seams, stress–strain experiments under temperature of 50, 150 and 250 °C were conducted using lignite from Kailuan mining area. Fourier transform infrared spectroscopy and elemental analysis were carried out before and after deformation of the samples. The results indicated that CO generated at 150 and 250 °C; the gas component was mostly oxygen(O_2), with small amount of carbon dioxide(CO_2), methane(CH_4) and hydrogen(H_2). At 50 °C, O_2 and a little CO_2 were observed and no CO was found. The carbon content of the coal samples increased slightly after deformation, and the oxygen content, H/C ratio, and O/C ratio decreased. The molecular structure of coal displayed different evolution characteristics at various temperatures. At 50 and 150 °C, the falling off of side chains, broken of ether bond and directional realignment of the aliphatic chains resulting in the formation of long chains were the main performance of coal molecular structure evolution. While at 250 °C, the side chains fell off and short chains formed. Furthermore, at both 150 and 250 °C, condensed degree of aromatic ring increased. Under the action of temperature and pressure, CO forms in two ways.The first is that ether bond breaks, oxygen and carbon atoms combine together and forms CO, or O_2 forming in the broken of ether–oxygen bond leads to the oxidation of free radicals and resulting in the formation of CO. And the second is that CO derives from falling off of C=O group.

Numerical Simulation of Surface Acoustic Wave and Detection of Surface Crack in Steel

The surface acoustic wave （SAW） propagating in a sample of steel is simulated by using finite element method （FEM）. The waves are excited by a load function with propagation properties such as phase velocity disper- sion and wide bandwidth. A two-dimensional model consisting of surface defects loaded with a wideband 50--200 M Hz and short time 0.1 gs displacement function is investigated in the time and frequency domains. By transient dy- namic analysis, Fourier transform and dispersion calculation, snapshots of propagating wave and responses from sens- ing points are presented. It is indicated that this supervision approach is sensitive to the surface cracks and reflections.

Evaluating ultrasound signals of carbon steel fatigue testing using signal analysis approaches

The application of ultrasound techniques to monitor the condition of structures is becoming more prominent because these techniques can detect the early symptoms of defects such as cracks and other defects.The early detection of defects is of vital importance to avoid major failures with catastrophic consequences.An assessment of an ultrasound technique was used to investigate fatigue damage behaviour.Fatigue tests were performed according to the ASTM E466-96 standard with the attachment of an ultrasound sensor to the test specimen.AISI 1045 carbon steel was used due to its wide application in the automotive industry.A fatigue test was performed under constant loading stress at a sampling frequency of 8 Hz.Two sets of data acquisition systems were used to collect the fatigue strain signals and ultrasound signals.All of the signals were edited and analysed using a signal processing approach.Two methods were used to evaluate the signals,the integrated Kurtosis-based algorithm for z-filter technique(I-kaz) and the short-time Fourier transform(STFT).The fatigue damage behaviour was observed from the initial stage until the last stage of the fatigue test.The results of the I-kaz coefficient and the STFT spectrum were used to explain and describe the behaviour of the fatigue damage.I-kaz coefficients were ranged from 60 to 61 for strain signals and ranged from 5 to 76 for ultrasound signals.I-kaz values tend to be high at failure point due to high amplitude of respective signals.STFT spectrogram displays the colour intensity which represents the damage severity of the strain signals.I-kaz technique is found very useful and capable in assessing both stationary and non-stationary signals while STFT technique is suitable only for non-stationary signals by displaying its spectrogram.

Quantitative Analysis Using Fourier Transform Ion Cyclotron Resonance Mass Spectrometry and Correlation between Mass Spectrometry Data and Sulfur Content of Crude Oils

Fourier transform ion cyclotron resonance mass spectrometry(FT-ICR MS) has become a powerful tool for analyzing the detailed composition of petroleum samples. However, the correlation between the numerous peaks obtained by FT-ICR MS and bulk properties of petroleum samples is still a challenge. In this study, the internal standard method was applied for the quantitative analysis of four straight-run vacuum gas oils(VGO) by atmospheric pressure photoionization(APPI) FT-ICR MS. The heteroatom class distribution of these VGO samples turned to be different when the concentration changed. Linear relationship between the normalized abundance and the concentration of VGO samples was identified for the total aromatic compounds, aromatic hydrocarbons, S1 and N1 species. The differences of the response factors were also discussed. The sulfur contents of a series of crude oils were proved to be linear with the FT-ICR MS data calibrated by the response factor of S1 species. This study demonstrated the feasibility of the internal standard method in quantitative analysis with APPI FT-ICR MS, and the bulk properties of petroleum samples could be correlated directly with the FT-ICR MS data.

Carob Origin Classification by FTIR Spectroscopy and Chemometrics

The goal of this study was to use Fourier transform mid-infrared （FTIR） spectroscopy for discrimination of samples of pods and seeds of carob from three Moroccan regions. The origin of samples Pods and seeds of carob could be distinguished from their IR spectra and this measurement was used for discriminate analysis. A multivariate analysis procedure based on the combined use of Hierarchical Cluster Aanalysis （HCA） and Partial Least Squares-Discriminant Analysis （PLS-DA） was tested and provided good classification results. Three distinctive clusters were recognised, related to the three Moroccan regions. Afterwards, PLS-DA was used for the discrimination and classification of the origin of the various Pods and seeds of carob samples. The results demonstrated that the combined use of FTIR and chemometric analysis （cluster analysis and discrimination by PLS- DA） can be used to rapidly and simply determine the origin of carob pulpe samples.

The Preparation and Characterization of Vermiculite Hydrosol

The dispersibility of vermiculite is the key factor that affects the application of vermiculite.In this paper,the milled natural vermiculite was pillared by organic quaternary ammonium salts.Then the pillared vermiculite was ground and homogenized under the existence of dispersive agent to form a stable vermiculite hydrosol system.Small angle X-ray diffraction(SA-XRD),fourier transform infrared spectroscopy(FTIR),and thermogravimetric analyses(TGA)were used to characterize the structure and thermal property of the vermiculite.The results indicate that the exfoliated vermiculite is successfully obtained.The analyses of laser particle size analyzer,transmission electron microscope(TEM),and Tyndall phenomenon analyzer demonstrate that the vermiculite hydrosol prepared is a stable hydrosol system.

Pricing Variance Swaps Under Stochastic Volatility with an Ornstein-Uhlenbeck Process

Pricing variance swaps under stochastic volatility has been an important subject pursued recently. Various approaches have been proposed, mainly due to the substantially increased trading activities of volatility-related derivatives in the past few years. In this note, the authors develop analytical method for pricing variance swaps under stochastic volatility with an Ornstein-Uhlenbeck(OU) process. By using Fourier transform algorithm, a closed-form solution for pricing variance swaps with stochastic volatility is obtained, and to give a comparison of fair strike value based on the discrete model, continuous model, and the Monte Carlo simulations.

Effects of drying process of Yuanzhi (Radix Palygalae) on its bioactive ingredients

OBJECTIVE： To study the effects of the drying processing in terms operational parameters on the bio- active constituents of six YuanzhJ （Radix Palygalae） samples across China. METHODS： Six Yuanzhi （Radix Palygalae） samples were investigated using thermogravimetry analysis. The heating courses were set in two ways： the temperature-programmed process from room temperature to 150℃ ,and the constant-temperature course at 50℃, 70℃ and 90℃. RESULTS： The peak temperature of six Yuanzhi （Radix Palygalae） samples ranged from 78℃ to 88℃. The mass loss rate of Yuanzhi （Radix Palygalae） alcohol-soluble extract was significantly increased when heated at 90℃. Four types of bioactive ingredients were detected in volatile oils of Yuanzhi （Radix Palygalae） sample from Shanxi province by Gas Chromatography-mass spectrometry analysis. Fourier Transform Infrared Spectroscopy results showed that the drying temperature exerted a great influence on types and amount of ingredients of Yuanzhi （Radix Palygalae）. The kinetic study showed that the constant-temperature drying process of Yuanzhi Radix Palygalae） samples could be well de- scribed by the Page Model, especially for the drying process at 50~C, in which R2 and SD values were more than 0.98 and less than 0.04, respectively.The drying constant k of three Yuanzhi （Radix Palygalae） samples from Shanxi, Gansu and Shaanxi provinces in China was corresponding to the Arrhenius equation, and their activation energies were 28.07, 2.5.38 and 21.48 kJ/mol, respectively. CONCLUSION： The drying process of Yuanzhi （Radix Palygalae） was very important for bioactive ingredients improvement in Yuanzhi （Radix Palygalae）. Temperature was a thermodynamic property significantly affecting the process.