A novel operation of batch distillation-combination of varyingcolumn pressure and total reflux-total efflux is studiedexperimentally. In the operation, the product is accumulated at thetop of the column under total re...A novel operation of batch distillation-combination of varyingcolumn pressure and total reflux-total efflux is studiedexperimentally. In the operation, the product is accumulated at thetop of the column under total reflux and then drained off completely,and the column pressure is varying in the whole process. This processhas been industrialized successfully with large profits. Theconventional model of batch distillation is improved by this methodeffectively: the separation efficiency and the yield of product areincreased greatly, the operation time is shortened and the productioncost is cut down. Moreover, the amount of condensation water isdecreased and the over-high reboiler temperature is lowered.展开更多
文摘A novel operation of batch distillation-combination of varyingcolumn pressure and total reflux-total efflux is studiedexperimentally. In the operation, the product is accumulated at thetop of the column under total reflux and then drained off completely,and the column pressure is varying in the whole process. This processhas been industrialized successfully with large profits. Theconventional model of batch distillation is improved by this methodeffectively: the separation efficiency and the yield of product areincreased greatly, the operation time is shortened and the productioncost is cut down. Moreover, the amount of condensation water isdecreased and the over-high reboiler temperature is lowered.