Magnetite concentrate was recovered from ferrous sulphate by co-precipitation and magnetic separation. In co-precipitation process, the effects of reaction conditions on iron recovery were studied, and the optimal rea...Magnetite concentrate was recovered from ferrous sulphate by co-precipitation and magnetic separation. In co-precipitation process, the effects of reaction conditions on iron recovery were studied, and the optimal reaction parameters are proposed as follows： n（CaO）/n（Fe2＋） 1.4：1, reaction temperature 80 ℃, ferrous ion concentration 0.4 mol/L, and the final mole ratio of Fe3＋ to FJ＋ in the reaction solution 1.9-2.1. In magnetic separation process, the effects of milling time and magnetic induction intensity on iron recovery were investigated. Wet milling played an important part in breaking the encapsulated magnetic phases. The results showed that the mixed product was wet-milled for 20 min before magnetic separation, the grade and recovery rate of iron in magnetite concentrate were increased from 51.41% and 84.15% to 62.05% and 85.35%, respectively.展开更多
Dry sliding wear tests were performed on a Mg-10Y-4Gd-1.5Zn-0.4Zr alloy using a Ball-on-Flat type wear apparatus against an AISI 52100 type bearing steel ball counterface. The wear rates were measured within a load ra...Dry sliding wear tests were performed on a Mg-10Y-4Gd-1.5Zn-0.4Zr alloy using a Ball-on-Flat type wear apparatus against an AISI 52100 type bearing steel ball counterface. The wear rates were measured within a load range of 3-25 N, a sliding speed range of 0.03-0.3 m/s and a sliding temperature range of 25-200 ℃ at a constant sliding distance of 400 m. The morphologies of the worn surfaces and wear debris were studied by scanning electron microscopy （SEM） and energy dispersive X-ray spectroscopy （EDS）. Comparatively, the wear properties of a hypereutectic Al-Si aluminium alloy under the same condition were measured. The results indicate that the wear rates of Mg-10Y-4Gd-1.5Zn-0.4Zr alloy are lower than that of cast＋T6 AC9B aluminium alloy. The dominant mechanism of cast＋T6 Mg-10Y-4Gd-1.5Zn-0.4Zr alloy is abrasion wear mixed with other wear mechanisms, which tends to be an abrasion and plastic deformation wear at high normal load such as 10-25 N, abrasion and plastic deformation wears with small participation of delamination and oxidative wears at high sliding speed such as 0.12-0.3 m/s, and an oxidative and abrasion wear at high test temperature such as 100-200 ℃. The Mg12Y1Zn1 phase in Mg-10Y-4Gd-1.5Zn-0.4Zr alloy plays an important role in the wear rate.展开更多
To improve the wear resistance of cast Al?17Si?5Cu alloy(AR alloy),isothermal heat treatment is employed to modify the morphology of Si particles(particularly eutectic Si particles).Furthermore,wear behaviour of heat-...To improve the wear resistance of cast Al?17Si?5Cu alloy(AR alloy),isothermal heat treatment is employed to modify the morphology of Si particles(particularly eutectic Si particles).Furthermore,wear behaviour of heat-treated alloy(HT alloy)along with AR alloy is studied using a pin-on-disc tribometer.Worn surfaces are then characterised using scanning electron microscope.The result reveals considerable microstructural modifications after the heat treatment.Accordingly,higher hardness value in HT alloy is obtained compared with AR alloy.The overall wear rate for HT alloy is found to be significantly lower compared with AR alloy at all the applied loads,indicating remarkable improvement in wear resistance.Eutectic Si particles become from acicular/rod-like to spherical/equiaxed morphology(aspect ratio close to 1)on heat treatment,resulting in good bonding with the matrix.Thus,they remain intact during wear and being harder,providing resistance to wear.Moreover,the increased hardness on heat treatment causes further resistance to wear.Therefore,the combined effect of intact harder Si particles on the wearing surface and higher hardness results in superior wear behavior in HT alloy at all loads compared with AR alloy.展开更多
The effect of PEG dispersant on the magnetic separation of magnetite（Fe3O4） synthesized from ferrous sulfate solution via co-precipitation method with calcium hydroxide as the precipitant was investigated. The resul...The effect of PEG dispersant on the magnetic separation of magnetite（Fe3O4） synthesized from ferrous sulfate solution via co-precipitation method with calcium hydroxide as the precipitant was investigated. The results indicated that a PEG dispersant could significantly affect Fe3O4 recovery. Adding PEG during the preparation of Fe3O4 was unfavorable for Fe3O4 recovery. When the PEG-6000 concentration was increased from 0 to 8 g/L, the iron grade and median particle size of the Fe3O4 product decreased from 65.58% and 2.35 μm to 57.79% and 1.35 μm, respectively. However, adding PEG during the wet milling of the mixed product promoted the subsequent recovery of Fe3O4. When the amount of PEG-200 increased from 0% to 4% of the powder mass, the grade of iron in the Fe3O4 product increased from 65.58% to 68.32%. While the relative molecular mass of PEG at an amount of 4% of the powder mass increased from 200 to 20000, the grade of iron was reduced from 68.32% to 66.70%.展开更多
Eutectic high entropy alloys(EHEAs)have high temperature stability,good mechanical properties,and are promising for tribological applications at high temperatures.To study the high temperature lubrication behavior,Fe_...Eutectic high entropy alloys(EHEAs)have high temperature stability,good mechanical properties,and are promising for tribological applications at high temperatures.To study the high temperature lubrication behavior,Fe_(22)Co_(26)Cr_(20)Ni_(22)Ta_(10)−(BaF_(2)/CaF_(2))x(x=3−20,wt.%)composites were prepared by spark plasma sintering(SPS),with BaF_(2)/CaF_(2) eutectic powder used as solid lubricant.The lubrication behavior and mechanical properties were studied at both room and high temperatures.With the increase of the content of BaF_(2)/CaF_(2) eutectic powder,the friction coefficients and the wear rates of the composites at 600 and 800℃ decrease significantly.The composites with eutectic powder content of 15 and 20 wt.%have the best lubricating performance at 600℃,with low friction coefficient and wear rates,mainly due to the good mechanical properties of EHEA matrix,the lubrication effect of BaF_(2)/CaF_(2) phase and the oxides formed on the worn surface.展开更多
Frictional wear of inner walls of drill pipe and casing is produced by rotational advance of drill pipe in the casing due to the joint effect of drilling fluid, temperature and contact load during drilling, among whic...Frictional wear of inner walls of drill pipe and casing is produced by rotational advance of drill pipe in the casing due to the joint effect of drilling fluid, temperature and contact load during drilling, among which the main wear is on the drill string. With development of drilling technology, deep well, ultradeep well, high angle well, directional well, extended reach well and horizontal well are taking more and more proportion. Meanwhile, the problem of serious frictional wear between drill pipe and casing are becoming more significant due to long time of drilling, high probability of dogleg severity, high contact normal stress between drill pipe and casing etc. Tool sticking may also occur due to large frictional resistance. Therefore, higher requirements are made on the study of how to predict and prevent the wear of drill pipe and casing during drilling. The residual strength of the worn casing is also studied by analysis of the law of drill pipe＇s effect on the casing wear in this paper.展开更多
基金Project(2013A090100013)supported by the Special Project on the Integration of Industry,Education and Research of Guangdong Province,ChinaProject(201407300993)supported by the High Technology Research and Development Program of Xinjiang Uygur Autonomous Region,China
文摘Magnetite concentrate was recovered from ferrous sulphate by co-precipitation and magnetic separation. In co-precipitation process, the effects of reaction conditions on iron recovery were studied, and the optimal reaction parameters are proposed as follows： n（CaO）/n（Fe2＋） 1.4：1, reaction temperature 80 ℃, ferrous ion concentration 0.4 mol/L, and the final mole ratio of Fe3＋ to FJ＋ in the reaction solution 1.9-2.1. In magnetic separation process, the effects of milling time and magnetic induction intensity on iron recovery were investigated. Wet milling played an important part in breaking the encapsulated magnetic phases. The results showed that the mixed product was wet-milled for 20 min before magnetic separation, the grade and recovery rate of iron in magnetite concentrate were increased from 51.41% and 84.15% to 62.05% and 85.35%, respectively.
基金Project(51404082)supported by the National Natural Science Foundation of ChinaProject(E201442)supported by the Natural Science Foundation of Heilongjiang Province,China+2 种基金Project(12531116)supported by the Foundation of Educational Committee of Heilongjiang Province,ChinaProject(2013RFQXJ137)supported by the Harbin Special Funds for Creative Talents in Science and Technology,ChinaProject(201510)supported by Science Funds for the Young Innovative Talents of HUST,China
文摘Dry sliding wear tests were performed on a Mg-10Y-4Gd-1.5Zn-0.4Zr alloy using a Ball-on-Flat type wear apparatus against an AISI 52100 type bearing steel ball counterface. The wear rates were measured within a load range of 3-25 N, a sliding speed range of 0.03-0.3 m/s and a sliding temperature range of 25-200 ℃ at a constant sliding distance of 400 m. The morphologies of the worn surfaces and wear debris were studied by scanning electron microscopy （SEM） and energy dispersive X-ray spectroscopy （EDS）. Comparatively, the wear properties of a hypereutectic Al-Si aluminium alloy under the same condition were measured. The results indicate that the wear rates of Mg-10Y-4Gd-1.5Zn-0.4Zr alloy are lower than that of cast＋T6 AC9B aluminium alloy. The dominant mechanism of cast＋T6 Mg-10Y-4Gd-1.5Zn-0.4Zr alloy is abrasion wear mixed with other wear mechanisms, which tends to be an abrasion and plastic deformation wear at high normal load such as 10-25 N, abrasion and plastic deformation wears with small participation of delamination and oxidative wears at high sliding speed such as 0.12-0.3 m/s, and an oxidative and abrasion wear at high test temperature such as 100-200 ℃. The Mg12Y1Zn1 phase in Mg-10Y-4Gd-1.5Zn-0.4Zr alloy plays an important role in the wear rate.
基金DST-SERB grant, vide Project No. YSS/2014/000172 dated 2015-08-17
文摘To improve the wear resistance of cast Al?17Si?5Cu alloy(AR alloy),isothermal heat treatment is employed to modify the morphology of Si particles(particularly eutectic Si particles).Furthermore,wear behaviour of heat-treated alloy(HT alloy)along with AR alloy is studied using a pin-on-disc tribometer.Worn surfaces are then characterised using scanning electron microscope.The result reveals considerable microstructural modifications after the heat treatment.Accordingly,higher hardness value in HT alloy is obtained compared with AR alloy.The overall wear rate for HT alloy is found to be significantly lower compared with AR alloy at all the applied loads,indicating remarkable improvement in wear resistance.Eutectic Si particles become from acicular/rod-like to spherical/equiaxed morphology(aspect ratio close to 1)on heat treatment,resulting in good bonding with the matrix.Thus,they remain intact during wear and being harder,providing resistance to wear.Moreover,the increased hardness on heat treatment causes further resistance to wear.Therefore,the combined effect of intact harder Si particles on the wearing surface and higher hardness results in superior wear behavior in HT alloy at all loads compared with AR alloy.
基金Project(2016JJ6017) supported by Hunan Provincial Natural Science Foundation of,ChinaProject(15C0245) supported by the Research Foundation of Education Bureau of Hunan Province,ChinaProject(2013A090100013) supported by the Special Foundation of Major Science&Technology Program of Guangdong Province,China
文摘The effect of PEG dispersant on the magnetic separation of magnetite（Fe3O4） synthesized from ferrous sulfate solution via co-precipitation method with calcium hydroxide as the precipitant was investigated. The results indicated that a PEG dispersant could significantly affect Fe3O4 recovery. Adding PEG during the preparation of Fe3O4 was unfavorable for Fe3O4 recovery. When the PEG-6000 concentration was increased from 0 to 8 g/L, the iron grade and median particle size of the Fe3O4 product decreased from 65.58% and 2.35 μm to 57.79% and 1.35 μm, respectively. However, adding PEG during the wet milling of the mixed product promoted the subsequent recovery of Fe3O4. When the amount of PEG-200 increased from 0% to 4% of the powder mass, the grade of iron in the Fe3O4 product increased from 65.58% to 68.32%. While the relative molecular mass of PEG at an amount of 4% of the powder mass increased from 200 to 20000, the grade of iron was reduced from 68.32% to 66.70%.
基金The authors acknowledge the financial support from the National Natural Science Foundation of China(51671217).
文摘Eutectic high entropy alloys(EHEAs)have high temperature stability,good mechanical properties,and are promising for tribological applications at high temperatures.To study the high temperature lubrication behavior,Fe_(22)Co_(26)Cr_(20)Ni_(22)Ta_(10)−(BaF_(2)/CaF_(2))x(x=3−20,wt.%)composites were prepared by spark plasma sintering(SPS),with BaF_(2)/CaF_(2) eutectic powder used as solid lubricant.The lubrication behavior and mechanical properties were studied at both room and high temperatures.With the increase of the content of BaF_(2)/CaF_(2) eutectic powder,the friction coefficients and the wear rates of the composites at 600 and 800℃ decrease significantly.The composites with eutectic powder content of 15 and 20 wt.%have the best lubricating performance at 600℃,with low friction coefficient and wear rates,mainly due to the good mechanical properties of EHEA matrix,the lubrication effect of BaF_(2)/CaF_(2) phase and the oxides formed on the worn surface.
文摘Frictional wear of inner walls of drill pipe and casing is produced by rotational advance of drill pipe in the casing due to the joint effect of drilling fluid, temperature and contact load during drilling, among which the main wear is on the drill string. With development of drilling technology, deep well, ultradeep well, high angle well, directional well, extended reach well and horizontal well are taking more and more proportion. Meanwhile, the problem of serious frictional wear between drill pipe and casing are becoming more significant due to long time of drilling, high probability of dogleg severity, high contact normal stress between drill pipe and casing etc. Tool sticking may also occur due to large frictional resistance. Therefore, higher requirements are made on the study of how to predict and prevent the wear of drill pipe and casing during drilling. The residual strength of the worn casing is also studied by analysis of the law of drill pipe＇s effect on the casing wear in this paper.
