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优化内浸式Ce掺杂ZnO光催化降解罗丹明B 被引量:16
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作者 张凯龙 施妙艳 +3 位作者 倪貌貌 陈佳祎 汤淑利 谭志文 《中国环境科学》 EI CAS CSCD 北大核心 2019年第4期1447-1455,共9页
采用沉淀法优化制备了纳米级Ce掺杂ZnO,利用BET,XRD,SEM,ICP-AES,UV-VisDRS,FT-IR等手段对催化剂结构形态组成进行表征.提出内浸式光催化降解模式,考察液层厚度对透光率的影响,优化了Ce掺杂ZnO光催化降解罗丹明B实验条件,分析了其动力... 采用沉淀法优化制备了纳米级Ce掺杂ZnO,利用BET,XRD,SEM,ICP-AES,UV-VisDRS,FT-IR等手段对催化剂结构形态组成进行表征.提出内浸式光催化降解模式,考察液层厚度对透光率的影响,优化了Ce掺杂ZnO光催化降解罗丹明B实验条件,分析了其动力学和机理.结果表明,Ce掺杂比为3%(n:n),500℃热处理2h活性最高.催化剂呈球状,尺寸均匀,粒径80~100nm, BET比表面积12.9m^2/g,测定掺杂量和理论值一致, Ce掺杂增加了光吸收.悬浮液"遮挡效应"对光透过率衰减显著,催化剂浓度为0.1g/100mL时UV_(254)处光衰减率达到溶液的3倍.内浸式光催化降解1.0×10^(-5)mol/L罗丹明B溶液,在15W紫外灯,pH值为7,温度30℃,催化剂投加量0.1g/250mL条件下,70min降解率达到92.5%,6次套用降解率保持在80%以上,降解过程符合一级动力学,反应速率常数0.05min^(-1). 展开更多
关键词 CE掺杂 氧化锌 内浸 光催化降解 罗丹明B
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热浸镀锌用新型内浸式电热管
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作者 刘经国 《电力金具》 2011年第2期19-21,共3页
寻求内浸发热、改善热传导、提高热效率,去掉镀锌铁锅,降低生产成本,是我们热浸镀锌行业内追求的新目标之一。
关键词 耐锌腐 内浸发热 耐腐涂层 装配式
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企业数智化变革悖论应对的能力基础:悖论协同能力探索 被引量:1
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作者 张志菲 罗瑾琏 +2 位作者 李树文 唐慧洁 王象路 《西安交通大学学报(社会科学版)》 CSSCI 北大核心 2024年第1期100-110,共11页
悖论持久内嵌于组织之中,数智化变革更加凸显组织内矛盾要素或新增多元悖论。同时,鉴于对悖论的差异化应对会产生或增益或减损的双重效应,有效管理悖论对数智化变革成功至关重要。尽管已有研究验证了组织中悖论应对的重要性,并从态度、... 悖论持久内嵌于组织之中,数智化变革更加凸显组织内矛盾要素或新增多元悖论。同时,鉴于对悖论的差异化应对会产生或增益或减损的双重效应,有效管理悖论对数智化变革成功至关重要。尽管已有研究验证了组织中悖论应对的重要性,并从态度、行为和传统能力视角对数智化变革悖论管理进行探究,但未有学者扎根数智化变革情境探索保障悖论应对持续有效的能力。在梳理数智化变革悖论类别以及悖论管理研究的基础上,从动态能力视角出发,融合数智化变革悖论及其管理核心特征,提出悖论协同能力是指组织通过将悖论两极矛盾要素进行相互联结和转换推动变革目标实现的能力,包含内浸式悖论协同能力和外拓式悖论协同能力两个维度。同时,探索悖论协同能力对数智化变革成效的影响,并对未来研究进行展望。通过聚焦数智化变革情境,关注悖论协同能力,以进一步融合与拓展数智化变革研究和悖论管理研究。 展开更多
关键词 数智化变革 悖论管理 能力基础 悖论协同能力 内浸式悖论协同 外拓式悖论协同
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小件热浸镀锌自动线
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作者 刘经国 《电力金具》 2012年第1期16-23,共8页
小件如玛钢件、水暖件、螺栓螺母等形状复杂,其热浸镀锌比较困难,质量难以提高,成本难以降低。全面改进与提高其热浸镀锌工艺,是镀锌业界当今的追求,最好的办法是机械化自动化。根据多年实践经验与探讨,提出了简单易行而又功能齐... 小件如玛钢件、水暖件、螺栓螺母等形状复杂,其热浸镀锌比较困难,质量难以提高,成本难以降低。全面改进与提高其热浸镀锌工艺,是镀锌业界当今的追求,最好的办法是机械化自动化。根据多年实践经验与探讨,提出了简单易行而又功能齐全品质优良的小件热浸镀锌自动线是个大胆的尝试。或许能促进本业发展提高。 展开更多
关键词 烘烤除油 液压推杆 拍节 内浸 最佳方位 拉脱力
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Recovery of carbon and cryolite from spent pot lining of aluminium reduction cells by chemical leaching 被引量:27
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作者 SHI Zhong-ning LI Wei +3 位作者 HU Xian-wei REN Bi-jun GAO Bing-liang WANG Zhao-wen 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2012年第1期222-227,共6页
A two-step alkaline-acidic leaching process was conducted to separate the cryolite from spent pot lining and to purify the carbon. The influencing factors of temperature, time, and the ratio of liquid to solid in alka... A two-step alkaline-acidic leaching process was conducted to separate the cryolite from spent pot lining and to purify the carbon. The influencing factors of temperature, time, and the ratio of liquid to solid in alkaline and acidic leaching were investigated. The results show that the recovery of soluble compounds of Na3AlF6 and Al2O3 dissolving into the solution during the NaOH leaching is 65.0%,and the purity of carbon reaches 72.7%. During the next step of HCl leaching, the recovery of soluble compounds of CaF2 and NaAl11O17 dissolving into the HCl solution is 96.2%, and the carbon purity increases to 96.4%. By mixing the acidic leaching solution and the alkaline leaching solution, the cryolite precipitates under a suitable conditions of pH value 9 at 70 °C for 2 h. The cryolite precipitating rate is 95.6%, and the purity of Na3AlF6 obtained is 96.4%. 展开更多
关键词 spent pot lining RECOVERY chemical leaching aluminium electrolysis
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Small invasive ductal carcinoma of the pancreas distinct from branch duct intraductal papillary mucinous neoplasm 被引量:2
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作者 Hiroki Sakamoto Masayuki Kitano +5 位作者 Takamitsu Komaki Hajime Imai Ken Kamata Masatomo Kimura Yoshifumi Takeyama Masatoshi Kudo 《World Journal of Gastroenterology》 SCIE CAS CSCD 2009年第43期5489-5492,共4页
Endoscopic ultrasonography (EUS) is a highly sensitive diagnostic method for the detection of small pancreatic carcinomas. Recently, there have been some reports describing the utility of contrast-enhanced harmonic ... Endoscopic ultrasonography (EUS) is a highly sensitive diagnostic method for the detection of small pancreatic carcinomas. Recently, there have been some reports describing the utility of contrast-enhanced harmonic EUS (CEH-EUS) which uses sonographic contrast agent for differentiation of a pancreatic mass. This report describes a case of small adenocarcinoma of the pancreas distinct from branch duct intraductal papillary mucinous neoplasm (IPMN) in which investigation by EUS took place every 6 mo and diagnosis was made accurately by additional CEH-EUS during the follow-up of the branch duct IPMN. A 68-year-old female was admitted to our hospital because of a branch duct IPMN in the pancreatic body. She had been followed-up by EUS every 6 too. However, after 2 years EUS demonstrated a low echoic area distinct from the branch duct IPMN which was vaguely discernible by EUS, and accurate sizing and differential diagnosis were considered difficult on the EUS imaging. CHEUS with Sonazoid revealed a hypovascular tumor and we suspected small pancreatic carcinoma. The histopathological diagnosis was adenocarcinoma (10 mm) in the pancreatic tail, distinct from the branch duct IPMN of the pancreatic body. EUS and CEH-EUS may play an important role in the correct diagnosis of small pancreatic tumors, including synchronous and metachronous occurrence of IPMN and ductal adenocarcinoma of the pancreas. 展开更多
关键词 Intraductal papillary mucinous adenoma Small pancreatic cancer Endoscopic ultrasonography Contrast-enhanced harmonic endoscopic ultrasonography Pancreatic cancer PANCREAS Contrast enhanced endoscopic ultrasonography
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Gastric infiltration of diffuse large B-cell lymphoma: Endoscopic diagnosis and improvement of lesions after chemotherapy 被引量:1
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作者 Sergio Zepeda-Gómez Jesús Camacho +1 位作者 Edgar Oviedo-Cárdenas Carmen Lome-Maldonado 《World Journal of Gastroenterology》 SCIE CAS CSCD 2008年第27期4407-4409,共3页
Diffuse large B-cell lymphoma (DLBCL) is the most common histologic subtype of the non-Hodgkin’s lymphoma (NHL) accounting for about 40% of all NHLs. This is a case report about the endoscopic appearance of a DLBCL w... Diffuse large B-cell lymphoma (DLBCL) is the most common histologic subtype of the non-Hodgkin’s lymphoma (NHL) accounting for about 40% of all NHLs. This is a case report about the endoscopic appearance of a DLBCL with infiltration to the stomach in a 39-year-old female. She had a 6-mo history of lumbar and left upper quadrant pain with intermittent episodes of melena. A computer tomograghy (CT) scan showed mural thickening of the gastric antrum. Endoscopic examination revealed multiple gastric ulcers. Definite diagnosis could be made by endoscopic biopsies and the patient had a good response to chemotherapy. This response correlated well with a further endoscopic follow-up. A follow-up endoscopic examination could be considered to evaluate a good response to chemotherapy in DLBCL patients with secondary gastric dissemination. 展开更多
关键词 Diffuse large B-cell lymphoma Non-Hodgkin's lymphoma Gastric infiltration
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Intraluminal versus infiltrating gallbladder carcinoma:Clinical presentation,ultrasound and computed tomography 被引量:7
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作者 Tze-Yu Lee Sheung-Fat Ko +5 位作者 Chung-Cheng Huang Shu-Hang Ng Jiun-Lung Liang Hsuan-Ying Huang Min-Chi Chen Shyr-Ming Sheen-Chen 《World Journal of Gastroenterology》 SCIE CAS CSCD 2009年第45期5662-5668,共7页
AIM: To compare clinical presentation and ultrasound (US) and computed tomography (CT) sensitivity between intraluminal and infiltrating gallbladder carcinoma (GBCA). METHODS: This retrospective study evaluate... AIM: To compare clinical presentation and ultrasound (US) and computed tomography (CT) sensitivity between intraluminal and infiltrating gallbladder carcinoma (GBCA). METHODS: This retrospective study evaluated 65 cases of GBCA that were categorized morphologically into the intraluminaI-GBCA (n = 37) and infiltrating-GBCA (n = 28) groups. The clinical and laboratory findings, presence of gallstones, gallbladder size, T-staging, nodal status, sensitivity of preoperative US and CT studies, and outcome were compared between the two groups. RESULTS: There were no significant differences between the two groups with respect to female predominance, presence of abdominal pain, serum aminotransferases level, T2-T4 staging, and regional metastatic nodes. Compared with the patients with intraluminaI-GBCA, those with infiltrating-GBCA were significantly older (65.49 ± 1.51 years vs 73.07 ± 1.90 years), had a higher frequency of jaundice (3/37 patients vs 13/28 patients) and fever (3/37 patients vs 10/28 patients), higher alkaline phosphatase (119.36 ± 87.80 IU/L vs 220.68 ± 164.84 IU/L) and total bilirubin (1.74 ± 2.87 mg/L vs 3.50 ± 3.51 mg/L) levels, higher frequency of gallstones (12/37 patients vs 22/28 patients), smaller gallbladder size (length, 7.47± 1.70 cm vs 6.47 ± 1.83 cm; width, 4.21 ± 1.43 cm vs 2.67 ± 0.93 cm), and greater proportion of patients with 〈 12 mo survival (16/37 patients vs 18/28 patients). The sensitivity for diagnosing intraluminal- GBCA with and without gallstones was 63.6% and 91.3% by US, and 80% and 100% by CT, respectively. The sensitivity for diagnosing infiltrating-GBCA with and without gallstones was 12.5% and 25% by US, and 71.4% and 75% by c-r, respectively. CONCLUSION: In elderly women exhibiting small gallbladder and gallstones on US, especially those with jaundice, fever, high alkaline phosphatase and bilirubin levels, CT may reveal concurrent infiltrating-GBCA. 展开更多
关键词 Gallbladder neoplasms CARCINOMA ULTRASOUND Computed tomography
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Reflecting on the English Immersion in the Mainland of China
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作者 LIANG Xiaohua 《International English Education Research》 2014年第9期63-66,共4页
Launched in the late 1990s in Xi'an, the first and the most influential English immersion programs - CCUEI were carried out in some big cities in the mainland of China. Fifteen years of implementation witnessed the s... Launched in the late 1990s in Xi'an, the first and the most influential English immersion programs - CCUEI were carried out in some big cities in the mainland of China. Fifteen years of implementation witnessed the success as well as the challenges, which need reflect and draw the implications for pedagogy and teacher education. 展开更多
关键词 English immersion CCUE1 ACTIVITY
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The Extension of Infinitesimal Prolongation Theorem and Its Application
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作者 陈东立 《Journal of Mathematical Research and Exposition》 CSCD 北大核心 2003年第2期221-224,共4页
Infinitesimal prolongation theorem is extended from sequences to nets based on κ-saturated nonstandard model. As its an application, a main property about topology of uniform convergence is proved. The proof is much ... Infinitesimal prolongation theorem is extended from sequences to nets based on κ-saturated nonstandard model. As its an application, a main property about topology of uniform convergence is proved. The proof is much simpler than it was, meanwhile the nonstandard characteristics of convergence with respect to u.c. topology is given. 展开更多
关键词 Infinitesimal Prolongation Theorem κ-saturation monad of uniformity topology of uniform convergence.
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