As-cast single crystal （SC） superalloy samples were shot peened and then annealed at different temperatures to investigate the effect of annealing temperature on the surface recrystallization behavior of the SC supe...As-cast single crystal （SC） superalloy samples were shot peened and then annealed at different temperatures to investigate the effect of annealing temperature on the surface recrystallization behavior of the SC superalloy. The results show that the depth of recrystallized layers increases with the increase of annealing temperature. Below 1200 °C, the recrystallization depth climbs slowly with temperature rising. Above 1200 °C, the recrystallization depth increases sharply with the rise of temperature. The morphology of recrystallized grains is significantly affected by annealing temperature. Below the γ′ solvus, cellular recrystallization may be observed. Above the γ′ solvus, recrystallization occurs through the growth of well developed recrystallized grains. In addition, the microstructure evolution of recrystallized grains at the homogenization annealing temperature was studied. It is found that recrystallized grains first nucleate in the dendritic core areas on the shot-peened surface and then grow inwards along the dendritic core areas. With the dissolution of the coarse γ′ precipitates and γ/γ′ eutectics in the interdendritic areas, the recrystallized grain boundaries move through the interdendritic areas. Finally, the fully developed grains nearly have a uniform depth. The dissolution of primary γ′ precipitates is a critical factor influencing the recrystallization behavior of SC superalloys.展开更多
2026 aluminum alloy was compressed in a temperature range of 300-450 ℃ and strain rate range of 0.01-10 s^-1. The correlation between compression conditions and microstructural evolution after solution and aging heat...2026 aluminum alloy was compressed in a temperature range of 300-450 ℃ and strain rate range of 0.01-10 s^-1. The correlation between compression conditions and microstructural evolution after solution and aging heat treatment was investigated. It is found that the recrystallization and precipitation behavior after heat treatment are associated with the temperature compensated strain rate Z value during hot deformation. Under low Z parameter condition, a small quantity of free recrystallized grains are formed, and the well formed subgrains with clean high-angle boundaries and coarse precipitates seem to be remained during heat treatment. Under high Z parameter condition, a large number of fine equiaxed recrystallized grains are produced, and a high dislocation density with poorly developed cellularity and considerable fine dynamic precipitates are replaced by the well formed subgrains and relatively coarse precipitates after heat treatment. The average recrystallized grain size after heat treatment decreases with increasing Z value and a quantitative relation between the average grain size and the Z value is obtained.展开更多
A novel thermomechanical processing was developed for producing fine grained Al-Mg-Li alloy sheets. The influences of static recrystallization annealing on the grain structure and superplastic behavior were investigat...A novel thermomechanical processing was developed for producing fine grained Al-Mg-Li alloy sheets. The influences of static recrystallization annealing on the grain structure and superplastic behavior were investigated. The results show that the refined microstructure has a variation in the distribution of grain size, shape and texture across the normal direction of the sheet. The surface layer （SL） has fine, nearly equiaxed grains with a rotated cUbeND {001 }（310） orientation, whereas the center layer （CL） has coarse, elongated grains with a portion of a fiber orientation. Increasing static recrystallized temperature results in grain growth in the full thickness, decreasing of grain aspect ratio in the center layer, texture sharpening in the surface layer, but weakening in the center layer as well as decreasing of superplastic elongation. Increasing the annealing temperature also produces an sharpening of the rotated cube {001}（310） component and a decreasing of the a fiber texture in the full thickness of the sheet. The formation mechanisms of recrystallization texture at various temperatures and layers were discussed.展开更多
Microstructure and properties of Al-0.30Zr and Al-0.30Zr-0.08Y （mass fraction, %） alloys were investigated by electrical conductivity measurements, microhardness tests, scanning electron microscopy （SEM） and trans...Microstructure and properties of Al-0.30Zr and Al-0.30Zr-0.08Y （mass fraction, %） alloys were investigated by electrical conductivity measurements, microhardness tests, scanning electron microscopy （SEM） and transmission electron microscopy （TEM）. Micron-sized primary Al3Y phases form within grains and at grain boundaries simultaneously as product of eutectic reaction in as-cast Al-Zr--Y alloys. The addition of Y obviously accelerates the precipitation kinetics of Al3Zr （Ll2） in Al-Zr-Y alloys. The Al-Zr-Y alloys exhibit greater electrical conductivity during aging due to formation of increased volume fractions of Al3（Zr, Y） precipitates. In ternary Al-Zr-Y alloys, spheroidal L l2-structured Al3（Zr, Y） precipitates with increased number density and smaller mean radius were observed. The Al-0.30Zr-0.08Y alloys show improved recrystallization resistance compared with Al-0.30Zr alloys展开更多
The aim of this work is evaluate the intergranular corrosion on UNS S31803 steel, with heat treatments at 800 ℃, varying treatment times of 30 mins, 360 mins and 1,440 mins. The results confirm the formation of o pha...The aim of this work is evaluate the intergranular corrosion on UNS S31803 steel, with heat treatments at 800 ℃, varying treatment times of 30 mins, 360 mins and 1,440 mins. The results confirm the formation of o phases and secondary austenite （γ2）. For the analysis of the influence of o and γ2 phases, metallographic analysis were conducted through optical microscopy, potentiokinetic reactivation electrochemical techniques and potentiodynamic polarization in NaCI 3.5% solution. Microstructural analysis has shown a formation of γ2 and o phase in heat treatment, due to diffusion of chromium and molybdenum from δ phase to y phase, precipitating on δ/γ and δ/δ interfaces. The DL-EPR （Double loop electrochemical potentiokinetic reactivation） results have shown an increase of the DOS （degree of sensitization） for long periods of time on heat treatment. The results of potentiodynamic polarization showed a reduction of the corrosion and pitting potentials, followed by an increase of the current density when the UNS S31830 steel is heat treated during long periods of time.展开更多
Magnesium alloy is the lightest structural metal material. As its ductility is usually limited because of its hexagonal closest packing (hcp) structure, it is significant to improve its forming performance. The primar...Magnesium alloy is the lightest structural metal material. As its ductility is usually limited because of its hexagonal closest packing (hcp) structure, it is significant to improve its forming performance. The primary way to achieve this goal is by grain refinement. This study explores new ways of grain refinement for cold-rolled sheet of magnesium alloy AZ31B by probing into its structural evolvement in heat treatment. It is found that recrystallization mostly takes place in the cold-rolled sheet in heat-treatment, and refined and equiaxial recrystallization grains with an average diameter of (14 to 15) mm can be obtained by heat-treatment at 260 C for (60 to 90) min, which is an effective method to obtain refined symmetrical grains of magnesium alloy by heat treatment at a lower recrystallization temperature after cold-rolling.展开更多
The fiber Bragg grating （FBG） is a passive optical fiber component with the refractive index modulated along the fiber length and has been widely applied in fiber sensing systems. High-temperature stable fiber grati...The fiber Bragg grating （FBG） is a passive optical fiber component with the refractive index modulated along the fiber length and has been widely applied in fiber sensing systems. High-temperature stable fiber gratings are promising for uses at high temperatures and attract extensive attention. In this paper, FBGs were inscribed in hydrogen loaded standard single mode fibers with the 248-nm excimer laser, and regenerated gratings were obtained through heat treatment. The shift of the central wavelength of the regenerated FBG had a good linearity with temperature, and the reflectivity of the regenerated FBG could almost keep unchanged at 800 ℃.展开更多
基金Project(2010ZF21007)supported by the Aeronautical Science Foundation of China
文摘As-cast single crystal （SC） superalloy samples were shot peened and then annealed at different temperatures to investigate the effect of annealing temperature on the surface recrystallization behavior of the SC superalloy. The results show that the depth of recrystallized layers increases with the increase of annealing temperature. Below 1200 °C, the recrystallization depth climbs slowly with temperature rising. Above 1200 °C, the recrystallization depth increases sharply with the rise of temperature. The morphology of recrystallized grains is significantly affected by annealing temperature. Below the γ′ solvus, cellular recrystallization may be observed. Above the γ′ solvus, recrystallization occurs through the growth of well developed recrystallized grains. In addition, the microstructure evolution of recrystallized grains at the homogenization annealing temperature was studied. It is found that recrystallized grains first nucleate in the dendritic core areas on the shot-peened surface and then grow inwards along the dendritic core areas. With the dissolution of the coarse γ′ precipitates and γ/γ′ eutectics in the interdendritic areas, the recrystallized grain boundaries move through the interdendritic areas. Finally, the fully developed grains nearly have a uniform depth. The dissolution of primary γ′ precipitates is a critical factor influencing the recrystallization behavior of SC superalloys.
基金Projects (2008CB617608, 2009CB623704) supported by the National Basic Research Program of China
文摘2026 aluminum alloy was compressed in a temperature range of 300-450 ℃ and strain rate range of 0.01-10 s^-1. The correlation between compression conditions and microstructural evolution after solution and aging heat treatment was investigated. It is found that the recrystallization and precipitation behavior after heat treatment are associated with the temperature compensated strain rate Z value during hot deformation. Under low Z parameter condition, a small quantity of free recrystallized grains are formed, and the well formed subgrains with clean high-angle boundaries and coarse precipitates seem to be remained during heat treatment. Under high Z parameter condition, a large number of fine equiaxed recrystallized grains are produced, and a high dislocation density with poorly developed cellularity and considerable fine dynamic precipitates are replaced by the well formed subgrains and relatively coarse precipitates after heat treatment. The average recrystallized grain size after heat treatment decreases with increasing Z value and a quantitative relation between the average grain size and the Z value is obtained.
基金Project(51205419)supported by the National Natural Science Foundation of China
文摘A novel thermomechanical processing was developed for producing fine grained Al-Mg-Li alloy sheets. The influences of static recrystallization annealing on the grain structure and superplastic behavior were investigated. The results show that the refined microstructure has a variation in the distribution of grain size, shape and texture across the normal direction of the sheet. The surface layer （SL） has fine, nearly equiaxed grains with a rotated cUbeND {001 }（310） orientation, whereas the center layer （CL） has coarse, elongated grains with a portion of a fiber orientation. Increasing static recrystallized temperature results in grain growth in the full thickness, decreasing of grain aspect ratio in the center layer, texture sharpening in the surface layer, but weakening in the center layer as well as decreasing of superplastic elongation. Increasing the annealing temperature also produces an sharpening of the rotated cube {001}（310） component and a decreasing of the a fiber texture in the full thickness of the sheet. The formation mechanisms of recrystallization texture at various temperatures and layers were discussed.
基金Project(2012CB619505)supported by the Basic Research Program of ChinaProject(51274141)supported by the National Natural Science Foundation of China
文摘Microstructure and properties of Al-0.30Zr and Al-0.30Zr-0.08Y （mass fraction, %） alloys were investigated by electrical conductivity measurements, microhardness tests, scanning electron microscopy （SEM） and transmission electron microscopy （TEM）. Micron-sized primary Al3Y phases form within grains and at grain boundaries simultaneously as product of eutectic reaction in as-cast Al-Zr--Y alloys. The addition of Y obviously accelerates the precipitation kinetics of Al3Zr （Ll2） in Al-Zr-Y alloys. The Al-Zr-Y alloys exhibit greater electrical conductivity during aging due to formation of increased volume fractions of Al3（Zr, Y） precipitates. In ternary Al-Zr-Y alloys, spheroidal L l2-structured Al3（Zr, Y） precipitates with increased number density and smaller mean radius were observed. The Al-0.30Zr-0.08Y alloys show improved recrystallization resistance compared with Al-0.30Zr alloys
文摘The aim of this work is evaluate the intergranular corrosion on UNS S31803 steel, with heat treatments at 800 ℃, varying treatment times of 30 mins, 360 mins and 1,440 mins. The results confirm the formation of o phases and secondary austenite （γ2）. For the analysis of the influence of o and γ2 phases, metallographic analysis were conducted through optical microscopy, potentiokinetic reactivation electrochemical techniques and potentiodynamic polarization in NaCI 3.5% solution. Microstructural analysis has shown a formation of γ2 and o phase in heat treatment, due to diffusion of chromium and molybdenum from δ phase to y phase, precipitating on δ/γ and δ/δ interfaces. The DL-EPR （Double loop electrochemical potentiokinetic reactivation） results have shown an increase of the DOS （degree of sensitization） for long periods of time on heat treatment. The results of potentiodynamic polarization showed a reduction of the corrosion and pitting potentials, followed by an increase of the current density when the UNS S31830 steel is heat treated during long periods of time.
基金the National "863"Foundation (Grant No. 2001AA351050).
文摘Magnesium alloy is the lightest structural metal material. As its ductility is usually limited because of its hexagonal closest packing (hcp) structure, it is significant to improve its forming performance. The primary way to achieve this goal is by grain refinement. This study explores new ways of grain refinement for cold-rolled sheet of magnesium alloy AZ31B by probing into its structural evolvement in heat treatment. It is found that recrystallization mostly takes place in the cold-rolled sheet in heat-treatment, and refined and equiaxial recrystallization grains with an average diameter of (14 to 15) mm can be obtained by heat-treatment at 260 C for (60 to 90) min, which is an effective method to obtain refined symmetrical grains of magnesium alloy by heat treatment at a lower recrystallization temperature after cold-rolling.
基金This work was supported by the Major Program of the National Natural Science Foundation of China （Grant No. 61290311）.
文摘The fiber Bragg grating （FBG） is a passive optical fiber component with the refractive index modulated along the fiber length and has been widely applied in fiber sensing systems. High-temperature stable fiber gratings are promising for uses at high temperatures and attract extensive attention. In this paper, FBGs were inscribed in hydrogen loaded standard single mode fibers with the 248-nm excimer laser, and regenerated gratings were obtained through heat treatment. The shift of the central wavelength of the regenerated FBG had a good linearity with temperature, and the reflectivity of the regenerated FBG could almost keep unchanged at 800 ℃.
