Wire-arc additive manufacture(WAAM)has great potential for manufacturing of Al-Cu components.However,inferior mechanical properties of WAAM deposited material restrict its industrial application.Inter-layer cold rolli...Wire-arc additive manufacture(WAAM)has great potential for manufacturing of Al-Cu components.However,inferior mechanical properties of WAAM deposited material restrict its industrial application.Inter-layer cold rolling and thermo-mechanical heat treatment(T8)with pre-stretching deformation between solution and aging treatment were adopted in this study.Their effects on hardness,mechanical properties and microstructure were analyzed and compared to the conventional heat treatment(T6).The results show that cold rolling increases the hardness and strengths,which further increase with T8 treatment.The ultimate tensile strength(UTS)of 513 MPa and yield stress(YS)of 413 MPa can be obtained in the inter-layer cold-rolled sample with T8 treatment,which is much higher than that in the as-deposited samples.The cold-rolled samples show higher elongation than that of as-deposited ones due to significant elimination of porosity in cold rolling;while both the T6 and T8 treatments decrease the elongation.The cold rolling and pre-stretching deformation both contribute to the formation of dense and dispersive precipitatedθ′phases,which inhibits the dislocation movement and enhances the strengths;as a result,T8 treatment shows better strengthening effect than the T6 treatment.The strengthening mechanism was analyzed and it was mainly related to work hardening and precipitation strengthening.展开更多
An integrated low-temperature nitriding process was carried out for Ti6Al4V to investigateitseffect on microstructure and properties.The process was designed to enhance the nitriding kinetics in low-temperature(500℃...An integrated low-temperature nitriding process was carried out for Ti6Al4V to investigateitseffect on microstructure and properties.The process was designed to enhance the nitriding kinetics in low-temperature(500℃) nitriding by deformation, and to strengthen Ti6Al4V alloybydispersionat the same time. Specimens of Ti6Al4V alloyweretreated through the process of solid solutionstrengthening-cold deformation-nitriding at 500℃. The white nitriding layeris formed after some time and then kept stable, changing little withthedeformationdegreeand time. The effect of aging on substrate is significant. Surface hardness and substrate hardnessincrease with deformation increasing. The construction was investigated by XRD.The surface nitridesare TiN, Ti2N, Ti4N3-Xand Ti3N1.29,and thenitridesin cross-section are Ti3N1.29and TiN0.3. The wear tests of specimens after nitriding, aging and deformation were carried out,andthetest data show that the nitrided pieces have the best wear resistance.展开更多
In order to investigate the effects of solid solution atoms, precipitated particles and cold deformation on the microstructures and properties of Al-Sc-Zr alloys, the Al-Sc-Zr alloys prepared by continuous rheo-extrus...In order to investigate the effects of solid solution atoms, precipitated particles and cold deformation on the microstructures and properties of Al-Sc-Zr alloys, the Al-Sc-Zr alloys prepared by continuous rheo-extrusion were treated by thermomechanical treatment, analyzed for conductivity and mechanical properties by tensile and microhardness testing, and characterized using optical microscope, TEM and STEM. A mathematical model was established to quantitatively characterize the contribution of solid solution atoms, precipitates and cold deformation to the conductivity of the alloy. The results show that the strength of Al alloy can be significantly improved by solid solution, aging and cold deformation, and the quantitative impacts of solution atoms, precipitates and cold deformation on the conductivity of Al alloy are 10.5%(IACS), 2.3%(IACS) and 0.5%(IACS), respectively. Aging and cold deformation treatments are the keys to obtain high-strength and high-conductivity aluminum alloy wires.展开更多
Three-layer6009/7050/6009aluminum alloy clad slab was fabricated by an innovative direct-chill casting process.To study the response of the clad slab to plastic deformation and heat treatments,homogenization annealing...Three-layer6009/7050/6009aluminum alloy clad slab was fabricated by an innovative direct-chill casting process.To study the response of the clad slab to plastic deformation and heat treatments,homogenization annealing,hot rolling,solution and aging were successively performed on the as-cast6009/7050/6009clad samples.The results revealed that excellent metallurgical bonding between7050alloy layer and6009alloy layer was achieved under optimal parameters.The clad ratio obviously decreased when the annealed sample was rolled to55%hot reduction level,and then changed slightly with further rolling.Furthermore,the content of rodlike Zn-rich phases increased significantly in7050alloy layer in the homogenized clad samples after rolling at55%,65%and75%hot reduction levels,and the higher level of hot reduction resulted in narrower diffusion layer.Subsequent solution and aging significantly improved the hardness in7050alloy layer,interfaces and6009alloy layers of the rolled samples except for the thin side for the75%hot reduction sample.展开更多
An integrated low temperature nitriding process for TC4(Ti6Al4V) has been developed and the effect on wear resistance has been investigated. Through the process of solid solution strengthening—cold deformation—nit...An integrated low temperature nitriding process for TC4(Ti6Al4V) has been developed and the effect on wear resistance has been investigated. Through the process of solid solution strengthening—cold deformation—nitriding at 400℃, the TC4 alloy is nitrided on surface and dispersion strengthened in bulk at the same time. The white nitriding layer is formed after some time of nitriding. The nitriding speed increases with the deformation degree. The construction was investigated by XRD and the nitride is Ti3N(2-X). The wear test was carried out and results exhibit that the nitrided samples have better wear resistance.展开更多
The Ti-35Nb-2Zr-0.3O(mass fraction,%)alloy was melted under a high-purity argon atmosphere in a high vacuumnon-consumable arc melting furnace,followed by cold deformation.The effects of cold deformation process on mic...The Ti-35Nb-2Zr-0.3O(mass fraction,%)alloy was melted under a high-purity argon atmosphere in a high vacuumnon-consumable arc melting furnace,followed by cold deformation.The effects of cold deformation process on microstructure andmechanical properties were investigated using the OM,XRD,TEM,Vicker hardness tester and universal material testing machine.Results indicated that the alloy showed multiple plastic deformation mechanisms,including stress-inducedα'martensite(SIMα')transformation,dislocation slipping and deformation twins.With the increase of cold deformation reduction,the tensile strength andhardness increased owing to the increase of dislocation density and grain refinement,and the elastic modulus slightly increasedowing to the increase of SIMα'phase.The90%cold deformed alloy exhibited a great potential to become a new candidate forbiomedical applications since it possessed low elastic modulus(56.2GPa),high tensile strength(1260MPa)and highstrength-to-modulus ratio(22.4×10-3),which are superior than those of Ti-6Al-4V alloy.展开更多
The solution heat treatment,cold deformation and subsequent aging were performed on CuMoCr alloy.And the influence of deformation and aging treatment on the electrical conductivity of CuMoCr alloy was studied through ...The solution heat treatment,cold deformation and subsequent aging were performed on CuMoCr alloy.And the influence of deformation and aging treatment on the electrical conductivity of CuMoCr alloy was studied through metallograph,transmission electron microscopy(TEM) and electrical conductivity measurement.Results show that deformation without subsequent aging can reduce the electrical conductivity of CuMoCr alloy,but deformation followed by the optimum aging treatment can effectively improve the electrical conductivity of CuMoCr alloy.Aging at 500 ℃ for 4 h after 80% deformation,the much better electrical conductivity of CuMoCr alloy can be obtained.Reduction of Cr content in the Cu matrix could be the reason for the enhancement of electrical conductivity.展开更多
How to model the permeability evolution of rock subjected to liquid nitrogen cooling is a key issue. This paper proposes a simple but practical method to study the permeability evolution of rocks subject to liquid nit...How to model the permeability evolution of rock subjected to liquid nitrogen cooling is a key issue. This paper proposes a simple but practical method to study the permeability evolution of rocks subject to liquid nitrogen cooling. FLAC with FISH function was employed to numerically model the rock behavior under cooling. The enhanced perme- ability of the volumetric strain was defined, and the permeability was directly evaluated based on element's volumetric strain. Detailed procedures for implementing the evolution model of permeability in this paper were presented. A case study was carried out to simulate a coal bed where liquid nitrogen was injected in the bore hole. And a semi-submerged test of liquid nitrogen was performed. The method to model the permeability evolution of rocks subject to liquid nitrogen shock in this paper was proved to be right by the test results. This simulation results are discussed with the hope to provide some insight into understanding the nitrogen cooling practice.展开更多
Cold orbital forging is an advanced spur bevel gear forming technology. Generally, the spur bevel gear in the cold orbital forging process is formed by two steps: the preforming step and the final step. Due to the gre...Cold orbital forging is an advanced spur bevel gear forming technology. Generally, the spur bevel gear in the cold orbital forging process is formed by two steps: the preforming step and the final step. Due to the great importance of the final step to gear forming and its complication with interactive factors, this work aims at examining the influence of key factors on the final step in cold orbital forging of a spur bevel gear. Using the finite element(FE) method and control variate method, the influence rules of four key factors, rotation velocity of the upper tool, n, feeding velocity of the lower tool, v, tilted angle of the upper tool, γ, friction factor between the tools and the billet, m, on the geometry and the deformation inhomogeneity of the cold orbital forged gear are thoroughly clarified. The research results show that the flash becomes more homogeneous with increasing v, increasing m, decreasing n or decreasing γ. And the deformation of the gear becomes more homogeneous with increasing v, decreasing n or decreasing γ. Finally, a corresponding experiment is conducted, which verifies the accuracy of FE simulation conclusions.展开更多
基金Project(ZZYJKT2024-08)supported by the State Key Laboratory of Precision Manufacturing for Extreme Service Performance,ChinaProject(2022JB11GX004)supported by Selection of the best Candidates to Undertake Key Research Projects by Dalian City,ChinaProject(201806835007)supported by China Scholarship Council。
文摘Wire-arc additive manufacture(WAAM)has great potential for manufacturing of Al-Cu components.However,inferior mechanical properties of WAAM deposited material restrict its industrial application.Inter-layer cold rolling and thermo-mechanical heat treatment(T8)with pre-stretching deformation between solution and aging treatment were adopted in this study.Their effects on hardness,mechanical properties and microstructure were analyzed and compared to the conventional heat treatment(T6).The results show that cold rolling increases the hardness and strengths,which further increase with T8 treatment.The ultimate tensile strength(UTS)of 513 MPa and yield stress(YS)of 413 MPa can be obtained in the inter-layer cold-rolled sample with T8 treatment,which is much higher than that in the as-deposited samples.The cold-rolled samples show higher elongation than that of as-deposited ones due to significant elimination of porosity in cold rolling;while both the T6 and T8 treatments decrease the elongation.The cold rolling and pre-stretching deformation both contribute to the formation of dense and dispersive precipitatedθ′phases,which inhibits the dislocation movement and enhances the strengths;as a result,T8 treatment shows better strengthening effect than the T6 treatment.The strengthening mechanism was analyzed and it was mainly related to work hardening and precipitation strengthening.
基金Projects(51275105,51375106)supported by the National Natural Science Foundation of China
文摘An integrated low-temperature nitriding process was carried out for Ti6Al4V to investigateitseffect on microstructure and properties.The process was designed to enhance the nitriding kinetics in low-temperature(500℃) nitriding by deformation, and to strengthen Ti6Al4V alloybydispersionat the same time. Specimens of Ti6Al4V alloyweretreated through the process of solid solutionstrengthening-cold deformation-nitriding at 500℃. The white nitriding layeris formed after some time and then kept stable, changing little withthedeformationdegreeand time. The effect of aging on substrate is significant. Surface hardness and substrate hardnessincrease with deformation increasing. The construction was investigated by XRD.The surface nitridesare TiN, Ti2N, Ti4N3-Xand Ti3N1.29,and thenitridesin cross-section are Ti3N1.29and TiN0.3. The wear tests of specimens after nitriding, aging and deformation were carried out,andthetest data show that the nitrided pieces have the best wear resistance.
基金Project(51674077) supported by the National Natural Science Foundation of ChinaProject(2018YFB2001800) supported by the National Research and Development Program of China
文摘In order to investigate the effects of solid solution atoms, precipitated particles and cold deformation on the microstructures and properties of Al-Sc-Zr alloys, the Al-Sc-Zr alloys prepared by continuous rheo-extrusion were treated by thermomechanical treatment, analyzed for conductivity and mechanical properties by tensile and microhardness testing, and characterized using optical microscope, TEM and STEM. A mathematical model was established to quantitatively characterize the contribution of solid solution atoms, precipitates and cold deformation to the conductivity of the alloy. The results show that the strength of Al alloy can be significantly improved by solid solution, aging and cold deformation, and the quantitative impacts of solution atoms, precipitates and cold deformation on the conductivity of Al alloy are 10.5%(IACS), 2.3%(IACS) and 0.5%(IACS), respectively. Aging and cold deformation treatments are the keys to obtain high-strength and high-conductivity aluminum alloy wires.
基金Projects(51375070,51574058) supported by the National Natural Science Foundation of China
文摘Three-layer6009/7050/6009aluminum alloy clad slab was fabricated by an innovative direct-chill casting process.To study the response of the clad slab to plastic deformation and heat treatments,homogenization annealing,hot rolling,solution and aging were successively performed on the as-cast6009/7050/6009clad samples.The results revealed that excellent metallurgical bonding between7050alloy layer and6009alloy layer was achieved under optimal parameters.The clad ratio obviously decreased when the annealed sample was rolled to55%hot reduction level,and then changed slightly with further rolling.Furthermore,the content of rodlike Zn-rich phases increased significantly in7050alloy layer in the homogenized clad samples after rolling at55%,65%and75%hot reduction levels,and the higher level of hot reduction resulted in narrower diffusion layer.Subsequent solution and aging significantly improved the hardness in7050alloy layer,interfaces and6009alloy layers of the rolled samples except for the thin side for the75%hot reduction sample.
基金Projects(51275105,51375106)supported by the National Natural Science Foundation of China
文摘An integrated low temperature nitriding process for TC4(Ti6Al4V) has been developed and the effect on wear resistance has been investigated. Through the process of solid solution strengthening—cold deformation—nitriding at 400℃, the TC4 alloy is nitrided on surface and dispersion strengthened in bulk at the same time. The white nitriding layer is formed after some time of nitriding. The nitriding speed increases with the deformation degree. The construction was investigated by XRD and the nitride is Ti3N(2-X). The wear test was carried out and results exhibit that the nitrided samples have better wear resistance.
基金Project(20133069014)supported by the National Aerospace Science Foundation of China
文摘The Ti-35Nb-2Zr-0.3O(mass fraction,%)alloy was melted under a high-purity argon atmosphere in a high vacuumnon-consumable arc melting furnace,followed by cold deformation.The effects of cold deformation process on microstructure andmechanical properties were investigated using the OM,XRD,TEM,Vicker hardness tester and universal material testing machine.Results indicated that the alloy showed multiple plastic deformation mechanisms,including stress-inducedα'martensite(SIMα')transformation,dislocation slipping and deformation twins.With the increase of cold deformation reduction,the tensile strength andhardness increased owing to the increase of dislocation density and grain refinement,and the elastic modulus slightly increasedowing to the increase of SIMα'phase.The90%cold deformed alloy exhibited a great potential to become a new candidate forbiomedical applications since it possessed low elastic modulus(56.2GPa),high tensile strength(1260MPa)and highstrength-to-modulus ratio(22.4×10-3),which are superior than those of Ti-6Al-4V alloy.
文摘The solution heat treatment,cold deformation and subsequent aging were performed on CuMoCr alloy.And the influence of deformation and aging treatment on the electrical conductivity of CuMoCr alloy was studied through metallograph,transmission electron microscopy(TEM) and electrical conductivity measurement.Results show that deformation without subsequent aging can reduce the electrical conductivity of CuMoCr alloy,but deformation followed by the optimum aging treatment can effectively improve the electrical conductivity of CuMoCr alloy.Aging at 500 ℃ for 4 h after 80% deformation,the much better electrical conductivity of CuMoCr alloy can be obtained.Reduction of Cr content in the Cu matrix could be the reason for the enhancement of electrical conductivity.
文摘How to model the permeability evolution of rock subjected to liquid nitrogen cooling is a key issue. This paper proposes a simple but practical method to study the permeability evolution of rocks subject to liquid nitrogen cooling. FLAC with FISH function was employed to numerically model the rock behavior under cooling. The enhanced perme- ability of the volumetric strain was defined, and the permeability was directly evaluated based on element's volumetric strain. Detailed procedures for implementing the evolution model of permeability in this paper were presented. A case study was carried out to simulate a coal bed where liquid nitrogen was injected in the bore hole. And a semi-submerged test of liquid nitrogen was performed. The method to model the permeability evolution of rocks subject to liquid nitrogen shock in this paper was proved to be right by the test results. This simulation results are discussed with the hope to provide some insight into understanding the nitrogen cooling practice.
基金Project(51105287)supported by the National Natural Science Foundation of ChinaProject(IRT13087)supported by Innovative Research Team Development Program of Ministry of Education of China+2 种基金Project(2012-86)supported by High-End Talent Leading Program of Hubei Province,ChinaProject(2014CFB876)supported by Natural Science Foundation of Hubei ProvinceChina
文摘Cold orbital forging is an advanced spur bevel gear forming technology. Generally, the spur bevel gear in the cold orbital forging process is formed by two steps: the preforming step and the final step. Due to the great importance of the final step to gear forming and its complication with interactive factors, this work aims at examining the influence of key factors on the final step in cold orbital forging of a spur bevel gear. Using the finite element(FE) method and control variate method, the influence rules of four key factors, rotation velocity of the upper tool, n, feeding velocity of the lower tool, v, tilted angle of the upper tool, γ, friction factor between the tools and the billet, m, on the geometry and the deformation inhomogeneity of the cold orbital forged gear are thoroughly clarified. The research results show that the flash becomes more homogeneous with increasing v, increasing m, decreasing n or decreasing γ. And the deformation of the gear becomes more homogeneous with increasing v, decreasing n or decreasing γ. Finally, a corresponding experiment is conducted, which verifies the accuracy of FE simulation conclusions.