Microstructure and hardness of twin-roll casting （TRC） process and direct-chill casting （DC） for A8006 alloy with and without homogenization were investigated by means of scanning electron microscopy （SEM）, X-ra...Microstructure and hardness of twin-roll casting （TRC） process and direct-chill casting （DC） for A8006 alloy with and without homogenization were investigated by means of scanning electron microscopy （SEM）, X-ray diffraction analysis and Vickers hardness measurement. The results show that the eutectic phase of the homogenized TRC alloy becomes fine as the microstructure of the as-cast TRC alloy is refined. The short rodlike eutectic phase of the as-cast TRC alloy is dispersed homogeneously, which is similar to the morphology of eutectic phase of the homogenized DC alloy. After homogenization, elements Fe and Mn in DC and TRC alloys are diffused from eutectic phase to A1 matrix, resulting in the decrease of microhardness. The formability of the as-cast TRC alloy is superior to that of the homogenized DC alloy. For TRC A8006 alloy, the homogenizing cycle can be removed from the subsequent processing.展开更多
The constituent of precipitations phases of aged melt-spun AlMgCu ribbons was characterized by high-resolution transmission electron microscopy and microhardness test. The cooling rate of as melt-spun ribbon was estim...The constituent of precipitations phases of aged melt-spun AlMgCu ribbons was characterized by high-resolution transmission electron microscopy and microhardness test. The cooling rate of as melt-spun ribbon was estimated to be 1.60×105 K/s from the empirical relation. The samples were aged at 200 ＆#176;C for 16 h after solution treatment. Two precipitation phases, i.e. Al2CuMg and abnormal amorphous SiO2 were identified in the T6 melt-spun AlMgCu ribbon. The crystal structure and stoichiometric composition of Al2CuMg phase are in good agreement with the reference results [WANG et al （2007; 2005）]. The combined experiments show that the formation of abnormal amorphous SiO2 appears to be associated with the higher cooling rate in melt-spinning process and has no significant effect on the peak hardness.展开更多
The biocompatibility of orthopedic implants is closely related to their elastic modulus and surface properties.The objective of this study was to determine the effects of cold rolling,recrystallization and laser surfa...The biocompatibility of orthopedic implants is closely related to their elastic modulus and surface properties.The objective of this study was to determine the effects of cold rolling,recrystallization and laser surface melting(LSM)on the microstructure and mechanical properties of a biphase(α″+β)Ti-30Nb-4Sn alloy.X-ray diffraction(XRD)texture analysis of the cold-rolled substrate revealed the[302]α″//ND texture component,while analysis of the recrystallized substrate showed the[302]α″//ND and[110]α″//ND components.Theβ-phase texture could not be directly measured by XRD,but the presence of the[111]β//ND texture component was successfully predicted by considering the orientation relationship between theα″andβphases.Nanoindentation measurements showed that the elastic modulus of the cold-rolled substrate(63GPa)was lower than that of the recrystallized substrate(74GPa).Based on the available literature and the results presented here,it is suggested that this difference is caused by the introduction of crystal defects during cold deformation.The combined nanoindentation/EBSD analysis showed that the nanoindentation results are not affected by crystal orientation.LSM of the deformed alloy produced changes in hardness,elastic modulus and crystallographic texture similar to those produced by recrystallization heat treatment,creating a stiffness gradient between surface and substrate.展开更多
基金Project (42-QP-009) supported by Research Fund of the State Key Laboratory of Solidification Processing,ChinaProject (Z2012019) supported by Graduate Starting Seed Fund of Northwestern Polytechnical University,ChinaProject (B08040) supported by 111 Project
文摘Microstructure and hardness of twin-roll casting （TRC） process and direct-chill casting （DC） for A8006 alloy with and without homogenization were investigated by means of scanning electron microscopy （SEM）, X-ray diffraction analysis and Vickers hardness measurement. The results show that the eutectic phase of the homogenized TRC alloy becomes fine as the microstructure of the as-cast TRC alloy is refined. The short rodlike eutectic phase of the as-cast TRC alloy is dispersed homogeneously, which is similar to the morphology of eutectic phase of the homogenized DC alloy. After homogenization, elements Fe and Mn in DC and TRC alloys are diffused from eutectic phase to A1 matrix, resulting in the decrease of microhardness. The formability of the as-cast TRC alloy is superior to that of the homogenized DC alloy. For TRC A8006 alloy, the homogenizing cycle can be removed from the subsequent processing.
基金Project(42-QP-009)supported by Research Fund of the State Key Laboratory of Solidification Processing,ChinaProject(Z2012019)supported by Graduate Starting Seed Fund of Northwestern Polytechnical University,ChinaProject(B08040)supported by the Program of Introducing Talents of Discipline to Universities("111"Project),China
文摘The constituent of precipitations phases of aged melt-spun AlMgCu ribbons was characterized by high-resolution transmission electron microscopy and microhardness test. The cooling rate of as melt-spun ribbon was estimated to be 1.60×105 K/s from the empirical relation. The samples were aged at 200 ＆#176;C for 16 h after solution treatment. Two precipitation phases, i.e. Al2CuMg and abnormal amorphous SiO2 were identified in the T6 melt-spun AlMgCu ribbon. The crystal structure and stoichiometric composition of Al2CuMg phase are in good agreement with the reference results [WANG et al （2007; 2005）]. The combined experiments show that the formation of abnormal amorphous SiO2 appears to be associated with the higher cooling rate in melt-spinning process and has no significant effect on the peak hardness.
基金supported by the Brazilian Funding Agencies CAPES(Federal Agency for the Support and Improvement of Higher Education)(Grant No.33003017)CNPq(National Council for Scientific and Technological Development)(Grant No.233006/2014-1)FAPESP(Sao Paulo Research Foundation)(Grant No.2011/19982-2)
文摘The biocompatibility of orthopedic implants is closely related to their elastic modulus and surface properties.The objective of this study was to determine the effects of cold rolling,recrystallization and laser surface melting(LSM)on the microstructure and mechanical properties of a biphase(α″+β)Ti-30Nb-4Sn alloy.X-ray diffraction(XRD)texture analysis of the cold-rolled substrate revealed the[302]α″//ND texture component,while analysis of the recrystallized substrate showed the[302]α″//ND and[110]α″//ND components.Theβ-phase texture could not be directly measured by XRD,but the presence of the[111]β//ND texture component was successfully predicted by considering the orientation relationship between theα″andβphases.Nanoindentation measurements showed that the elastic modulus of the cold-rolled substrate(63GPa)was lower than that of the recrystallized substrate(74GPa).Based on the available literature and the results presented here,it is suggested that this difference is caused by the introduction of crystal defects during cold deformation.The combined nanoindentation/EBSD analysis showed that the nanoindentation results are not affected by crystal orientation.LSM of the deformed alloy produced changes in hardness,elastic modulus and crystallographic texture similar to those produced by recrystallization heat treatment,creating a stiffness gradient between surface and substrate.
