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冻析法从杉木油中分离柏木醇的研究 被引量:16
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作者 杨静 陆顺忠 +2 位作者 李秋庭 刘洁 李娜 《广西林业科学》 2009年第1期39-41,共3页
采用冻析法从杉木油中分离柏木醇,通过结晶温度、结晶时间及是否添加晶种对柏木醇纯度及得率的影响的试验,确定从杉木油中分离柏木醇的最佳结晶时间及结晶温度。结果表明,不加晶种的条件下,杉木油(柏木醇含量为31.96%)在2℃下冷冻120 h... 采用冻析法从杉木油中分离柏木醇,通过结晶温度、结晶时间及是否添加晶种对柏木醇纯度及得率的影响的试验,确定从杉木油中分离柏木醇的最佳结晶时间及结晶温度。结果表明,不加晶种的条件下,杉木油(柏木醇含量为31.96%)在2℃下冷冻120 h,柏木醇的得率为59%以上,纯度大于95%。 展开更多
关键词 杉木油 柏木醇 冻析法
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10—钨铈(Ⅳ)酸及其盐的制备与性质研究
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作者 赵曙辉 顾翼东 《中国纺织大学学报》 CSCD 1994年第2期9-14,共6页
本文用10—钨铈(Ⅳ)酸钠溶液通过阳离子交换树脂制得了10—钨铈(Ⅳ)酸溶液,并用冻析法制得了固体10—钨铈(Ⅳ)酸。通过化学分析,得知其组成为H_6[CeW_(10)O_(35)]19H_2O。并对10—钨铈(Ⅳ)酸及其盐的性质进行了测试。红外(IR)分析显... 本文用10—钨铈(Ⅳ)酸钠溶液通过阳离子交换树脂制得了10—钨铈(Ⅳ)酸溶液,并用冻析法制得了固体10—钨铈(Ⅳ)酸。通过化学分析,得知其组成为H_6[CeW_(10)O_(35)]19H_2O。并对10—钨铈(Ⅳ)酸及其盐的性质进行了测试。红外(IR)分析显示,10—钨铈(Ⅳ)酸与10—钨铈(Ⅳ)酸纳相比,在生成10—钨铈(Ⅳ)酸的过程中,聚合杂多阴离子的结构有些变形。此外,10—钨铈(Ⅳ)酸及其盐与其它杂多酸相比,性质上差异较大,稳定性也较差。 展开更多
关键词 杂多酸 稀土元素 离子交换 冻析法
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Synthesis and properties of physically crosslinked poly (vinyl alcohol) hydrogels 被引量:1
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作者 MA Ru-yin XIONG Dang-sheng 《Journal of China University of Mining and Technology》 EI 2008年第2期271-274,共4页
The present study is an investigation of the properties of poly(vinyl alcohol),which would be a better contact lens mate- rial than conventional HEMA in some ways.A transparent PVA hydrogel was prepared from a PVA sol... The present study is an investigation of the properties of poly(vinyl alcohol),which would be a better contact lens mate- rial than conventional HEMA in some ways.A transparent PVA hydrogel was prepared from a PVA solution in a mixed solvent consisting of water and a water-miscible organic solvent,DMSO,by the freezing-thawing method.The water content,visible light transmittance,mechanical and swelling properties of the hydrogels were evaluated as a function of PVA concentration and number of freeze-thaw cycles.The results show that the properties of PVA hydrogels depend on the polymer concentration,the number of freeze-thaw cycles and the addition of the organic solvent. 展开更多
关键词 poly (vinyl alcohol) HYDROGEL freezing-thawing method swelling property
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STRESS ANALYSIS OF FREEZING PIPES BY MODELLING
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作者 崔广心 杨维好 《Journal of China University of Mining and Technology》 1992年第1期83-92,共10页
Using the simulation test facility designed on the basis of similitude principle, the authors of the paper carry out a series of simulation tests and study the influence of effective factors on the stress in the freez... Using the simulation test facility designed on the basis of similitude principle, the authors of the paper carry out a series of simulation tests and study the influence of effective factors on the stress in the freezing pipes during hoth periods of active freezing and excavating-lining. They obtain preliminarily the regularity of stress variation and discuss the causes of freezing pipe fracture. 展开更多
关键词 freezing pipe STRESS MODELLING
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