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应用X射线衍射-红外光谱等技术研究滑石在机械力研磨中的形貌和晶体结构变化及影响机制 被引量:3
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作者 任叶叶 张俭 +3 位作者 严俊 林剑 陈思杭 盛嘉伟 《岩矿测试》 CAS CSCD 北大核心 2015年第2期181-186,共6页
滑石的颗粒粒径、形貌、晶型等对其应用的实效性、终端产品的性能产生极大影响,目前主要研究其表面改性,而有关微观形貌及晶体结构研究较少。本文利用X射线荧光光谱、X射线衍射分析、红外光谱、粒度分析仪结合高分辨场发射扫描电镜(FE-S... 滑石的颗粒粒径、形貌、晶型等对其应用的实效性、终端产品的性能产生极大影响,目前主要研究其表面改性,而有关微观形貌及晶体结构研究较少。本文利用X射线荧光光谱、X射线衍射分析、红外光谱、粒度分析仪结合高分辨场发射扫描电镜(FE-SEM)技术对辽宁滑石粉在高强度机械力研磨作用下的微形貌和晶体结构变化特征进行系统研究。结果表明滑石粉原矿混合物中MgO与SiO2的分子个数比约为0.45,该数值明显低于纯滑石粉晶体中MgO与SiO2的分子个数比0.75。此类滑石为典型的单斜晶系,研磨作用使滑石粉由晶态转变为非晶态结构,其层状结构的有序化和键合作用发生了明显的变化。滑石粒度随研磨时间变化呈现减小-增大-减小的循环过程。研磨后粉体形貌存在差异,细化的小颗粒粉体因团聚而呈"准球体",且随着研磨的进行出现细化-团聚-细化的反复过程。此结论对于滑石的深加工与应用及其相关矿物粉体的研究具有一定的参考价值。 展开更多
关键词 滑石粉 研磨 团聚 准球体 X射线衍射法 红外光谱法 粒度分析仪 高分辨场发射扫描电镜
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General formulas for drag coefficient and settling velocity of sphere based on theoretical law 被引量:3
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作者 Yang Hongli Fan Minqiang +1 位作者 Liu Airong Dong Lianping 《International Journal of Mining Science and Technology》 SCIE EI CSCD 2015年第2期219-223,共5页
The settlement of particles is of great importance in many areas. The accurate determination of drag coefficient and settling velocity in wide Reynolds number (Re) range remains a problem. In this paper, a series of... The settlement of particles is of great importance in many areas. The accurate determination of drag coefficient and settling velocity in wide Reynolds number (Re) range remains a problem. In this paper, a series of new formulas for drag coefficient of spherical particles based on theoretical laws, such as the Stokes law, the Oseen law, and the Goldstein law, were developed and fitted using 480 groups of experimental data (Re 〈 2 × 10^5). The results show that the 2nd approximation of a rational function containing only one parameter can describe Co-Re relationship accurately over the whole Re range of 0-2× 10^5. The new developed formulas containing five parameters show higher goodness over wide Re range than presently existing equations. The introduction of the Oseen law is helpful for improving the fitting goodness of the empirical formulas. On the basis of one of the Oseen-based Co-Re formulas giving the lowest sum of squared relative errors Qover the whole Re range (Re 〈 2 × 10^5), a general formula for settling velocity ut based on dimensionless parameters was proposed showing high goodness. 展开更多
关键词 Sphere Drag coefficient Settling velocity Reynolds number Theoretical equation
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