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减压条件下氯化锌活化油茶果壳活性炭的制备工艺 被引量:14
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作者 周琴 邱会华 +1 位作者 沈健 黄敏 《精细化工》 EI CAS CSCD 北大核心 2015年第5期500-504,共5页
以油茶果壳为原料,以氯化锌为活化剂,在减压条件下热裂解制备活性炭。探讨氯化锌溶液的质量分数、体系压力、活化温度、活化时间对活性炭吸附性能的影响;通过低温氮气吸-脱附表征了样品的比表面积及孔结构,采用红外光谱仪分析了样品的... 以油茶果壳为原料,以氯化锌为活化剂,在减压条件下热裂解制备活性炭。探讨氯化锌溶液的质量分数、体系压力、活化温度、活化时间对活性炭吸附性能的影响;通过低温氮气吸-脱附表征了样品的比表面积及孔结构,采用红外光谱仪分析了样品的表面官能团。得到制备该活性炭的最佳工艺条件为:氯化锌溶液的质量分数为60%、料液比1∶3(即每毫克固体物料加入3 m L液体物料,下同)、体系压力为0.05 MPa、活化温度为450℃、活化时间为1 h,在该条件下得到的活性炭碘吸附值为1 120 mg/g,亚甲基蓝吸附值为373.16 mg/g,比表面积为2 023.15 m2/g,总孔体积为2.34 cm3/g,平均孔径为4.63 nm。减压条件下制备的活性炭具有优良的吸附性能。 展开更多
关键词 减压条件 氯化锌 油茶果壳 活性炭 功能材料
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减压条件下深水圆柱附近气泡的运动特性
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作者 崔杰 陈志鹏 +1 位作者 周陶然 郭建廷 《船舶工程》 CSCD 北大核心 2019年第9期131-137,共7页
为深入探究气泡与附近潜艇的相互作用规律,采用电火花气泡发生装置与高速摄像分析系统,在减压环境中对近似潜艇的深水圆柱周围不同位置的气泡进行研究。并以气泡通过圆柱结构中心的铅垂线为界的分类情况讨论深水圆柱周围气泡的动态变化... 为深入探究气泡与附近潜艇的相互作用规律,采用电火花气泡发生装置与高速摄像分析系统,在减压环境中对近似潜艇的深水圆柱周围不同位置的气泡进行研究。并以气泡通过圆柱结构中心的铅垂线为界的分类情况讨论深水圆柱周围气泡的动态变化。试验结果表明:圆柱结构附近的气泡的运动主要取决于气泡与圆柱结构间相对的攻角以及气泡质心到就近圆柱壁面的无量纲距离这两种因素的影响。在此基础上同时考虑减压环境中浮力的因素分析了浮力参数及攻角和爆距半径比对气泡第一周期运动时间和位移的影响,并总结圆柱下侧气泡不同爆距半径比下射流宽度的作用范围变化规律。研究结论为圆柱状的潜艇结构在水下受到攻击时的毁伤状态提供了参考。 展开更多
关键词 深水 圆柱结构 减压条件 气泡 运动特性
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Estimation of the Isotherms of Phenol on Activated Carbons and Polymeric Adsorbents under Supercritical Condition 被引量:2
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作者 奚红霞 谢兰英 +1 位作者 李祥斌 李忠 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2003年第3期253-256,共4页
A method named as 'volume-expanding and pressure-reducing adsorption' is proposed. It can be used to measure the isotherms under supercritical condition. The adsorption isotherms of phenol on activated carbons... A method named as 'volume-expanding and pressure-reducing adsorption' is proposed. It can be used to measure the isotherms under supercritical condition. The adsorption isotherms of phenol on activated carbons and polymeric adsorbents are estimated and compared respectively for the systems of 'phenol-activated carbon-supercritical fluid CO2' and 'phenol-polymeric adsorbent-supercritical fluid CO2'. The results show that the amount of phenol adsorbed on the activated carbons and the polymeric adsorbents under the supercritical condition is much less than that under the general condition, which can be utilized to develop a technology regenerating the activated carbon with supercritical fluid. Moreover, the effects of ethyl alcohol, used as the third component, on the isotherms of phenol on the activated carbons and polymeric adsorbents under the supercritical condition are also investigated. 展开更多
关键词 volume-expanding and pressure-reducing adsorption adsorption isotherm activated carbon polymeric adsorbent supercritical fluid
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Numerical simulation of flow field of single-hole oxygen lance jet
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作者 LIU Kun HAN Ren-zhi BAO Li-ming 《Journal of Energy and Power Engineering》 2007年第1期22-28,共7页
The numerical simulation of jet flow field in Laval tube was carried out first by commercial software CFX4.4, and it is used to determine inlet pressure condition out of nozzle in order to its numerical simulation. Th... The numerical simulation of jet flow field in Laval tube was carried out first by commercial software CFX4.4, and it is used to determine inlet pressure condition out of nozzle in order to its numerical simulation. The decay rule of jet middle line velocity of axial symmetry turbulence jet and cross section's expand situation out of the tube in different stagnation pressure and surrounding temperature were analyzed systematically. The result showed that K-e model is suitable for numerical simulation. The conclusion will have important guide and referent function to research of two important craft parameters, impact depth and the impact area which are related to steel-making production practice. 展开更多
关键词 Laval tube axis symmetry turbulence jet simulation
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