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Properties of Surface Film on X70 Pipeline Steel in CO_3^(2-)-/HCO_3^- Environment

The electrochemical behavior of X70 pipeline steel in (0.5mol·L-1 Na2CO3+1 mol·L-1 NaHCO3) solution was studied by potentiodynamic polarization and electrochemical impedance spectroscopy (EIS). X-ray photoelectron spectroscopy (XPS) and scanning electron microscopy (SEM) were used to analyze the composition and microstructure of the surface film. The results showed that there were two anodic peaks at -600 mV and -350 mV. The surface film formed at -600 mV mainly consisted of ferrous carbonates and ferrous hydroxycarbonates. It had a small reaction resistance. It was metastable and possessed poor protective property. Numerous pits and microcracks existed on the film, which could be the active paths for the initiation of stress corrosion cracking. The surface film formed at -350 mV, mainly consisted of ferric oxides. It has high reaction resistance and offered good protection for the substrate.

Cyclic oxidation behavior of Fe-9Cr-1Mo steel in water vapor atmosphere

The cyclic oxidation behavior of Fe-9Cr-1Mo steel (9Cr-1Mo) in 10%H2O+90%Ar (volume fraction) atmosphere at 600, 650 and 700 ℃ for various time was studied. The oxidation mechanism of 9Cr-1Mo steel in 10%H2O+90%Ar atmosphere was discussed. The thermal stress was evaluated in two oxide layers to illustrate the spallation of the oxide layer. The experimental results indicate that there exists a duplex oxide scale with an outer layer of Fe2O3 and an inner layer of mixed (Fe, Cr)3O4 formed on 9Cr-1Mo steel during cyclic oxidation. Some cracks generated in both inner and outer oxide layers. Parts of oxide scales spalled from substrate during the cyclic oxidation. A higher tensile stress in the oxide layer is formed at the early oxidation stage than at the later oxidation stage during heating. This tensile stress results in the formation of cracks in the oxide layer.

Variation in the temperature field of rocks overlying a high-temperature cavity during underground coal gasification

High temperature affects rocks in a way that changes the physical and mechanical properties of them. The temperature field in rock overlying a high temperature zone has been estimated using experimental research on thermal conductivity of the overlying strata. Numerical analysis software was used to esti- mate rock thermal conductivity at different temperatures. These estimates were then used with COMSOL Multiphysics to perform a numerical analysis with the heat conduction model. The results show that rock thermal conductivity decreases as the temperature increases and that various lithologies show similar behavior. The thermal conductivity of each rock type differs from the others at a given temperature. Exact values for the temperature distribution in the overlying strata during the process of underground coal gasification are obtained from the numerical simulation. The temperature in the rock changes with the height and direction from the gasifier. Temperature gradients vary for different types of rock. This result provides an important reference for further study of the strength of overlying strata subject to the process of underground coal gasification.

Growth of Semi-Insulating GaN Using N2 as Nucleation Layer Carrier Gas Combining with an Optimized Annealing Time

Semi-insulating （SI） GaN is grown using N2 as the nucleation layer （NL） carrier gas combined with an optimized annealing time by metalorganic chemical vapour deposition. Influence of using 1-12 and N2 as the NL carrier gas is investigated in our experiment. It is found that the sheet resistance of unintentionally doped GaN can be increased from 10^4 Ω/sq to 10^10 Ω/sq by changing the NL carrier gas from 1-12 to N2 while keeping the other growth parameters to be constant, however crystal quality and roughness of the tilm are degraded unambiguously. This situation can be improved by optimizing the NL annealing time. The high resistance of GaN grown on NL using N2 as the carrier gas is due to higher density of threading dislocations caused by the higher density of nucleation islands and small statistic diameter grain compared to the one using 1-12 as carrier gas. Annealing the NL for an optimized annealing time can decrease the density of threading dislocation and improve the tilm roughness and interface of AlGaN/GaN without degrading the sheet resistance of as-grown GaN signiticantly. High-quality SI GaN is grown after optimizing the annealing time, and AlGaN/GaN high electron mobility transistors are also prepared.

Numerical Study of the Mixing of Density-Stratified Fluid with a Jet

Density stratification of LNG （liquefied natural gas） is produced in a storage tank when one LNG is loaded on top of another LNG in the same tank. Mixing LNG by a jet issued from a nozzle on the tank wall is considered to a promising technique to prevent and eliminate stratification in LNG storage tanks. This study is concerned with the numerical simulation of a jet flow issued into a two-layer density-stratified fluid in a tank and the resultant mixing phenomena. The jet behavior was investigated with the laboratory-based experiment of the authors＇ previous study. A numerical method proposed by the authors is employed for the simulation. The upper and lower fluids are water and a NaCl-water solution, respectively, and the lower fluid is issued vertically upward from a nozzle on the bottom of the tank. The Reynolds number （Re） defined by the jet velocity and the nozzle diameter ranges from 95 to 2,378, and the mass concentration of the NaCl-water solution Co is set at 0.02 and 0.04. The simulation highlights the jet-induced mixing between the upper and lower fluids. It also clarifies the effects of Re and C0 on the height and horizontal spread of the jet.