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利用“自上而下”法评定微生物定量检测方法的不确定度
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作者 李甜甜 王易 +4 位作者 李志君 孙英丽 李彩清 董秀芳 胡敏 《乳业科学与技术》 2024年第5期25-31,共7页
参考ISO 19036标准《食物链中的微生物学定量测定的测量不确定度估算》和RB/T 228—2023《食品微生物定量检测的测量不确定度评估指南》,采用“自上而下”法设计实验方案,以生乳和发酵乳为样品,分别对3种不同定量检测方法进行不确定度... 参考ISO 19036标准《食物链中的微生物学定量测定的测量不确定度估算》和RB/T 228—2023《食品微生物定量检测的测量不确定度评估指南》,采用“自上而下”法设计实验方案,以生乳和发酵乳为样品,分别对3种不同定量检测方法进行不确定度评估。第1种为菌落总数的不确定度评定,包含技术不确定度、基质不确定度和泊松分布不确定度。综合3个分量的数值计算合成不确定度,当结果为9.4×10~4 CFU/m L时,扩展不确定度为0.31(lg(CFU/m L))。第2种为最可能数法的不确定度评定,包含技术不确定度、基质不确定度和基于最可能数的不确定度。综合3个分量的数值计算合成不确定度,当结果为24 MPN/g时,扩展不确定度为0.94(lg(MPN/g))。第3种为需要对目标菌进行确认的菌落总数不确定度评定,包括技术不确定度、基质不确定度、泊松分布不确定度和确证不确定度。综合4个分量的数值计算合成不确定度,当结果为22 CFU/g时,扩展不确定度为0.29(lg(CFU/g))。 展开更多
关键词 不确定评定 “自上而下”法 技术不确定 基质不确定 泊松分布不确定度 基于最可能数不确定 确证不确定
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基于ISO19036:2019评估饮用水中大肠菌群的测量不确定度
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作者 钟文涛 卢琳 +3 位作者 李政 周培华 洪振柏 周丛 《食品与机械》 2024年第10期68-72,共5页
[目的]参考ISO19036:2019对饮用水中大肠菌群的测量不确定度进行评估。[方法]通过设计试验方案,分别评估技术不确定度(u_(tech))、基质不确定度(u_(matrix))和分布不确定度(u_(distrib)),并综合3个分量的数值计算合成不确定度(uc(y))和... [目的]参考ISO19036:2019对饮用水中大肠菌群的测量不确定度进行评估。[方法]通过设计试验方案,分别评估技术不确定度(u_(tech))、基质不确定度(u_(matrix))和分布不确定度(u_(distrib)),并综合3个分量的数值计算合成不确定度(uc(y))和扩展不确定度(U)。[结果]对GB 4789.3—2016第二法进行测量不确定度评估后,得到的技术不确定度为0.1202 log(CFU/mL),基质不确定度为0.1 log(CFU/mL),分布不确定度分别为0.0655,0.0261 log(CFU/mL),当结果为440 CFU/mL时,扩展不确定度为0.34 log(CFU/mL),表示为(2.64±0.34)log(CFU/mL)。[结论]ISO19036:2019对食品中微生物定量检测方法进行测量不确定度评估相较目前国内标准更科学、更便捷。 展开更多
关键词 测量不确定 技术不确定 基质不确定 分布不确定度
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Evaluation of measurement uncertainty based on grey system theory for small samples from an unknown distribution 被引量:18
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作者 HAN LianFu TANG WenYan +2 位作者 LIU YongMeng WANG Jun FU ChangFeng 《Science China(Technological Sciences)》 SCIE EI CAS 2013年第6期1517-1524,共8页
To evaluate measurement uncertainty for small sample size and measurement data from an unknown distribution, we propose a grey evaluation method of measurement uncertainty based on the grey relation coefficient. The u... To evaluate measurement uncertainty for small sample size and measurement data from an unknown distribution, we propose a grey evaluation method of measurement uncertainty based on the grey relation coefficient. The uncertainty of measurement is analyzed using grey system theory, and the defects of the grey evaluation model of measurement uncertainty (GEMU) are studied. We then establish an improved grey evaluation model of measurement uncertainty (IGEMU). Simulations show that the precision of IGEMU is greater than that of GEMU, and that sample size has only a small effect on the precision of IGEVU. In particular, IGEMU is applied to evaluating measurement uncertainty for small sample size and measurement data from an unknown distribution. The measurement uncertainty of total profile deviation, which is measured by the CNC gear measuring center, can be evaluated by a combination of IGEMU and the Monte Carlo method. 展开更多
关键词 grey system theory grey relational coefficient measurement uncertainty tooth profile gear measuring center
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Effect of the uncertainty in soil-water characteristic curve on the estimated shear strength of unsaturated soil 被引量:2
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作者 Qian ZHAI Harianto RAHARDJO +2 位作者 Alfrendo SATYANAGA Guo-liang DAI Yan-jun DU 《Journal of Zhejiang University-Science A(Applied Physics & Engineering)》 SCIE EI CAS CSCD 2020年第4期317-330,共14页
Most failures or instabilities of geotechnical structures commonly result from shear failure in soil. In addition, many infrastructures are constructed within the unsaturated zone. Therefore, the determination of shea... Most failures or instabilities of geotechnical structures commonly result from shear failure in soil. In addition, many infrastructures are constructed within the unsaturated zone. Therefore, the determination of shear strength of unsaturated soil is crucial in geotechnical design. The soil-water characteristic curve(SWCC) is commonly used to estimate the shear strength of unsaturated soil because the direct measurement is time-consuming and costly. However, the uncertainty associated with the determined SWCC is rarely considered in the estimation of the shear strength. In this paper, the uncertainties of SWCC resulted from different factors are reviewed and discussed. The variability of the estimated shear strength for the unsaturated soil due to the uncertainty of SWCC associated with the best fit process is quantified by using the upper and lower bounds of the determined SWCC. On the other hand, the uncertainties of the estimated shear strength due to different initial void ratios or different confining pressures are quantified by adopting different SWCCs. As a result, it is recommended that the measured SWCC from the conventional Tempe cell or pressure plate needs to be corrected by considering different stress levels in the estimation of the shear strength of unsaturated soil. 展开更多
关键词 Unsaturated shear strength Pore-size distribution function VARIABILITY Soil-water characteristic curve (SWCC) Confidence limits
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