稻米油低度分提关键技术的研究

研究了稻米油的分提技术,关键生产工艺、技术参数、分提自动化设计。通过实验确定了最佳分提条件:脱蜡养晶温度为20℃,养晶时间为20 h;脱脂养晶温度为0~5℃,养晶时间为22 h;搅拌速度为12 r/min;验证了稻米油分提工艺在中试和实际生产中切实可行、效果良好,可大大提高稻米油的品质。

柔性可收分提模技术

结合具体工程实例,介绍了柔性可收分提模技术的工艺原理和施工流程,具体阐述了收分模板制作,提模装置设计,收分模板安装等操作要点和注意事项,并对材料,机具设备,质量要求,安全措施分别作了说明,指出该技术优点众多,具有广泛的应用前景。

Supercritical Fluid Extraction of Essential Oil from Dry Rhizome of Ligusticum chuanxiong Hort and Their Characterization by GC/MS

Supercritical fluid extraction (SFE) of essential oil from dry rhizome ofLigusticum chuanxiong Hort was developed. GC/MS was used for the determination of the composition ofessential oil. Forty-four compounds were identified. The conventional extraction method wasconducted in parallel for comparison. The extracts were qualitatively compared by GC/MS. The yieldsof SFE and steam distillation-extraction were 4.16 % ( v/w) and 0.8 % ( v/w), respectively.Application of SFE of zessential oil from dry rhizome of Ligustiaan chuanxiong Hort was preferable.

Method of Verification for Manufacturing in Sub-Wavelength Design

We describe a post resolution-enhancement-technique verification method for use in manufacturing data flow. The goal of the method is to verify whether designs function as intended,or more precisely, whether the printed images are consistent with the design intent. The process modeling is described for the model-based verifi cation method. The performance of the method is demonstrated by experiment.

Recent Advances in Separation of Bioactive Natural Products

Bioactive natural products are a main source of new drugs,functional foods and food additives.The separation of bioactive natural products plays an important role in transformation and use of biomass.The isolation and purification of bioactive principle from a complex matrix is often inherent bottleneck for the utilization of natural products,so a series of extraction and separation techniques have been developed.This review covers recent advances in the separation of bioactive natural products with an emphasis on their solubility and diffusion coefficients,recent extraction techniques and isolation techniques.This overview of recent technological advances,discussion of pertinent problems and prospect of current methodologies in the separation of bioactive natural products may provide a driving force for development of novel separation techniques.

Separation and Purification of Dodecanedioic Acid from Its Homologous Compounds by Falling Film Crystallization

Separation and purification of dodecanedioic acid (DDDA) from its homologous compounds were studied experimentally by falling film crystallization (FFC). The influences of various operation parameters, including crystallizing time, flow rate of melt and temperature of glycerine bath, on purity of DDDA and crystallizing rate were investigated. Over 99% (by mole) DDDA was obtained for a feed composition of 96% (by mole). The main factors affecting the separation efficiency are flow rate of melt and temperature of glycerine bath. The crystallizing layer of DDDA was further purified by sweating and blasting. A set of optimized operation data are provided for better understanding the mechanism of heat and mass transfer in FFC, and for further industrial application of DDDA purification process.

Isolation of refined solanesol from tobacco extracts by separation integrated technology

A separation integrated technology for isolating refined solanesol from tobacco extracts was provided. Some experimental installations applied in the separation integrated technology were designed. The experimental installations included saponification and extraction installation, cryogenic centrifugation crystallization installation and continuous midium pressure column chromatography separation installation In the paper, a separation integrated technology route was designed： saponification and extraction-crystallization - silica gel column chromatography-recrystallization. Finally, refined solanesol （-95.5%） was successfully got. The new method featured shorter experimental times, as well as lower solvent consumption, compared with the conventional extraction methods. So it showed great potential for efficient sample preparation and large-scale industrial application in the near future.

Zonal extraction technology and numerical simulation analysis in open pit coal mine

In order to enhance coal recovery ratio of open pit coal mines, a new extraction method called zonal mining system for residual coal around the end-walls is presented. The mining system can improve economic benefits by exploiting haulage and ventilation roadways from the exposed position of coal seams by uti- lizing the existing transportation systems. Moreover, the main mining parameters have also been dis- cussed. The outcome shows that the load on coal seam roof is about 0.307 MPa and the drop step of the coal seam roof about 20.3 m when the thickness of cover and average volume weight are about 120 m and 0.023 MN/m~ respectively. With the increase of mining height and width, the coal recovery ratio can be improved. However, when recovery ratio is more than 0.85, the average stress on the coal pillar will increase tempestuously, so the recovery ratio should also be controlled to make the coal seam roof safe. Based on the numerical simulation results, it is concluded that the ratio of coal pillar width to height should be more than 1.0 to make sure the coal pillars are steady, and there are only minor dis- placements on the end-walls.

Simultaneous Cell Disruption and Aqueous Two-Phase Extraction for Isolation of Intracellular Recombinant Proteins

A new technique was developed for the integrated processing of cell disruption and aqueous two-phase extraction in a high-speed bead mill to separate intracellular proteins from microbial cells. The process was named as simultaneous cell disruption and aqueous two-phase extraction (SDATE). Advantages, such as high cell disruption efficiency, biochemical activities preservation of proteins, cell debris elimination, and prelimiary purification of the target protein were being claimed. When this technique was employed for isolating recombinant Tumor Necrosis Factor (TNF) from E. coli, overall protein concentration and TNF activity were found to have been increased. More than 95% of TNF was partitioned into the top phase and all cell debris were in the bottom phase. The partition coefficient was greater than 3 and the TNF purification factor was greater than 6. It is shown that less separation steps were being utilized in the new technique, meaning a reduction in separation time and less process extractors required.

Mild Extraction Technique for Flavonoids from Leaves of Nypa fruiticans and Chemical Analysis of Its Components

Eight flavonoid derivatives： rutin, quercetin-3-glucoside, quercetin, luteolin-7-glucoside, isorhmnetin-3-sulphate, kaempferol-3,7-diglucoside,＇luteolin and kaempferol have been extracted and characterized from Nipa palm. Mild extraction technique involving the use of HPLC-DAD-MS was used. The structures of the flavonoids were determined on the basis of mass spectroscopy. Separation of the crude extract by paper chromatography （PC） on forestall as solvent system gave one major yellowish brown spot which had Rf value of 3.9. The Rf value and maximum absorption from UV spectroscopy were the same as those of quercetin standard. The most prominent compound was quercetin followed by three others： kaempferol-3,7-diglucoside, luteolin-7-glucoside, and isorhmnetin-3 -sulphate.

Research on A Web Intelligent Information Extraction Method

The paper introduce segmentation ideas in the pretreatment process of web page. By page segmentation technique to extract the accurate information in the extract region, the region was processed to extract according to the rules of ontology extraction, and ultimately get the information you need. Through experiments on two real datasets and compare with related work, experimental results show that this method can achieve good extraction results.

Automatic extraction of floating ice at Antarctic continental margin from remotely sensed imagery using object-based segmentation

Information of Antarctic iceberg and sea ice are valuable to Antarctic ice melting patterns studies which are helpful to understand climate conditions and general trends of our planet.This paper presents an automatic floating ice extraction method based on image segmentation technology using region growing.It effectively solves the over-segmentation and under-segmentation problems by merging the gray,contour,location and other information of each ice-object.A pixel-based extraction method is proposed to extract the small ices within 5 pixels.LANDSAT TM data,Chinese environment disaster satellite HJ1B data,and MODIS 1B data used to detect Floating ice at Antarctic continental margin respectively.The results showed that the extraction accuracies of the three kinds of data were all higher than 81 percent,while the accuracies of both TM data and HJ1B data were higher than 90%.Object-based information extraction methods can not only obtain the total area and number of floating ice objects in the whole region,but also provide precise details of single objects,including area,perimeter,contour,average brightness.

Abstract principal component analysis

We present the basic idea of abstract principal component analysis(APCA)as a general approach that extends various popular data analysis techniques such as PCA and GPCA.We describe the mathematical theory behind APCA and focus on a particular application to mode extractions from a data set of mixed temporal and spatial signals.For illustration,algorithmic implementation details and numerical examples are presented for the extraction of a number of basic types of wave modes including,in particular,dynamic modes involving spatial shifts.