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水溶性人工合成色素的聚苯胺分散相固相萃取 被引量:4
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作者 胡骢 严付华 +1 位作者 汪琼 孙边成 《中国卫生检验杂志》 CAS 2017年第14期1977-1979,共3页
目的通过化学氧化法制备聚苯胺,并将其作为分散相固相萃取的吸附材料,用于实际样品中水溶性人工色素的提取。方法采用化学氧化法制备聚苯胺,优化仪器参数和提取反应条件后,将聚苯胺用于人工合成色素胭脂红、苋菜红、柠檬黄和日落黄的提... 目的通过化学氧化法制备聚苯胺,并将其作为分散相固相萃取的吸附材料,用于实际样品中水溶性人工色素的提取。方法采用化学氧化法制备聚苯胺,优化仪器参数和提取反应条件后,将聚苯胺用于人工合成色素胭脂红、苋菜红、柠檬黄和日落黄的提取,同时应用于实际饮料样品中人工合成色素的检测。结果水溶性人工合成色素标准品提取前后对比图以及高效液相色谱图均显示出该提取法对4种水溶性人工合成色素具有极好的提取效率,可以基本实现完全提取,方法用于复杂基体样品的检测时同样具有良好的提取效率。结论新提取方法对水溶性人工色素萃取效率高,抗干扰能力强,同时还具有操作简单、成本低廉和环境友好等优点,具有良好的应用前景。 展开更多
关键词 聚苯胺 分散相固相萃取 水溶性人工合成色素
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Development of new solid phase extraction techniques in the last ten years 被引量:4
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作者 范惠霞 邓志鹏 +1 位作者 仲浩 姚庆强 《Journal of Chinese Pharmaceutical Sciences》 CAS CSCD 2013年第4期293-302,共10页
Solid phase extraction (SPE) is a widely used sample pretreatment method for separation, purification and enrichment, which has been established due to its significant advantages of time-saving, low consumption of s... Solid phase extraction (SPE) is a widely used sample pretreatment method for separation, purification and enrichment, which has been established due to its significant advantages of time-saving, low consumption of solvent, high enrichment factor, high accuracy, etc. In recent years, a variety of new SPE methods such as molecularly imprinted solid phase extraction (MISPE), magnetic solid phase extraction (MSPE), solid phase micro-extraction (SPME), etc., which are superior to the conventional SPE, have been developed and been widely applied to food, drugs, and environmental monitoring. In this paper, the basic principles and methods of SPE and its new applications in different areas are reviewed. 展开更多
关键词 Solid phase extraction Molecularly imprinted solid phase extraction Magnetic solid phase extraction Solid phase micro-extraction
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