利用小麦京771×Pm97034产生的重组自交系(recombinant inbred lines,RIL)群体,对Zeleny沉淀值、谷蛋白膨胀指数(swelling index of glutenin,SIG)、湿面筋含量、面筋指数、面粉膨胀势、碱性水保持力(alkline water retention capac...利用小麦京771×Pm97034产生的重组自交系(recombinant inbred lines,RIL)群体,对Zeleny沉淀值、谷蛋白膨胀指数(swelling index of glutenin,SIG)、湿面筋含量、面筋指数、面粉膨胀势、碱性水保持力(alkline water retention capacity,AWRC)、籽粒硬度、蛋白质含量等8个品质性状在RIL群体中的分离和分布规律进行了研究。结果表明,这些品质性状在重组自交系群体中呈连续变异,分布频率大致接近正态分布,同时存在双向超亲分离现象。多元逐步回归分析表明:SIG值、面筋指数、蛋白质含量和籽粒硬度可以解释Zeleny沉淀值的77.7%的表型变异,其中SIG值与Zeleny沉淀值的关系最密切。展开更多
A resolution method based on Gaussian-like distribution for overlapped linear sweep polarographic peaks was proposed to simultaneously detect the polymetallic components, such as Zn(Ⅱ) and Co(Ⅱ), coexisting in t...A resolution method based on Gaussian-like distribution for overlapped linear sweep polarographic peaks was proposed to simultaneously detect the polymetallic components, such as Zn(Ⅱ) and Co(Ⅱ), coexisting in the leaching solution of zinc hydrometallurgy. A Gaussian-like distribution was constructed as the sub-model of overlapped peaks by analyzing the characteristics of linear sweep polarographic curve. Then, the abscissas of each peak and trough were pinpointed through multi-resolution wavelet decomposition, the curve and its derivative curves were fitted by using nonlinear weighted least squares (NWLS). Finally, overlapped peaks were resolved into independent sub-peaks based on fitted reconstruction parameters. The experimental results show that the relative error of half-wave potential pinpointed by multi-resolution wavelet decomposition is less than 1% and the accuracy of Ip fitted by NWLS is higher than 96%. The proposed resolution method is effective for overlapped linear sweep polarographic peaks of Zn(Ⅱ) and Co(Ⅱ).展开更多
Centered on thetechniques and industrial applications of the reinforced cyclonic separation process, its principles and mechanism for separation ot ions, molecules and their aggregates using polyalsperse aroplets are ...Centered on thetechniques and industrial applications of the reinforced cyclonic separation process, its principles and mechanism for separation ot ions, molecules and their aggregates using polyalsperse aroplets are discussed generally; the characteristics and influential factors of fish-hook phenomenon of the grade efficiency curve in cyclonic separation for both gas and liquid are analyzed; and the influence of shear force on particle be- havior (or that of particle swarm) is also summarized. A novel idea for cyclonic separation is presented here: enhancing the cyclonic seoaration process of ions, molecules and their aggregates with monodisperse microspheres and their surface grafting, rearranging the distribution of particles by size using centrifugal field, reinforcing the cyclonic separation performance with orderly arranged particle swarm. Also the investigation of the shortcut flow, recirculation flow, the asymmetric structure and non-linear characteristics of the cyclonic flow field with a com-bined method of Volumetric 3-component Velocimetry (V3V) and Phase-Doppler Particle Anemometer (PDPA) are elaborated. It is recommended to develop new systems for the separation of heterogeneous phases with cyclonic technology, in accordance with the capture and reuse of CO2, methanol to olefins (MTO) process, coal transfer, andthe exploitation of oil shale.展开更多
We present photoelectron angular distribution of the aligned molecular ion H2^+ by intense ultrashort attosecond extreme ultraviolet laser pulses from numerical solutions of timedependent Schrodinger equations. Photo...We present photoelectron angular distribution of the aligned molecular ion H2^+ by intense ultrashort attosecond extreme ultraviolet laser pulses from numerical solutions of timedependent Schrodinger equations. Photoionization from a superposition state of the ground 1sσg and the excited 2pσu states with pulses at photon energies above the ionization potential, hω〉Ip, and intensity 10^14 W/cm^2, yields pulse duration dependent asymmetry of photoelectron angular distributions. We attribute the asymmetry to the periodical oscillation of the coherent electron wave packets, resulting from the interference of the two electronic states. For the processes with long pulse durations, such duration dependence is absent and symmetric angular distributions are obtained.展开更多
The pulsed power is a potential means for energy saving and presents an alternative to the conventional mechanical communication for minerals.The effect of magnetic pulse treatment on grindability of a magnetite ore w...The pulsed power is a potential means for energy saving and presents an alternative to the conventional mechanical communication for minerals.The effect of magnetic pulse treatment on grindability of a magnetite ore was investigated by grindability tests.The results of the investigation show that the pulsed treatment has little effect on the particle size distribution of the magnetite ore.Significant micro-cracks or fractures are not found by SEM analysis in magnetic pulse treated sample.Magnetic separation of magnetic pulse treated and untreated magnetite ore indicates that iron recovery increases from 81.3% in the untreated sample to 87.7% in the magnetic pulse treated sample,and the corresponding iron grade increases from 42.1% to 44.4%.The results demonstrate that the magnetic pulse treatment does not significantly weaken the mineral grain boundaries or facilitate the liberation of minerals,but is beneficial to magnetic separation.展开更多
Eye observation was used to evaluate the segregation degree of asphalt pavement, which was not much creditable. To the asphalt pavement, road surface texture measuring method which has appeared recently can identify g...Eye observation was used to evaluate the segregation degree of asphalt pavement, which was not much creditable. To the asphalt pavement, road surface texture measuring method which has appeared recently can identify gradational segregation; but it can’t reflect the influence of the temperature segregation. However, using infrared temperature detector to evaluate the segregation must be taken during paving, which brings much inconvenience. In this paper, measuring the air voids distribution using non-nuclear density gauge to evaluate asphalt pavement segregation was introduced. Result shows that this method can directly reflect the comprehensive results of the two types of segregation in a high efficient and accurate way. Moreover, using the sketch map of segregation area can help to analyze the segregation reason visually.展开更多
Liquid Fe35Cu35Si30alloy has achievedthemaximum undercooling of 328 K (0.24TL) with glass fluxing method, and it displayed triple solidification mechanisms. A critical undercooling of 24 K was determined for metasta...Liquid Fe35Cu35Si30alloy has achievedthemaximum undercooling of 328 K (0.24TL) with glass fluxing method, and it displayed triple solidification mechanisms. A critical undercooling of 24 K was determined for metastable liquid phase separation. At lower undercoolings,α-Fe phase was the primary phase and the solidification microstructure appeared as homogeneous well-defined dendrites. When the undercooling exceeded 24 K, the sample segregated into Fe-rich and Cu-rich zones. In the Fe-rich zone, FeSi intermetallic compound was the primary phase within the undercooling regime below 230 K, while Fe5Si3intermetallic compound replaced FeSi phase as the primary phase at larger undercoolings. The growth velocity of FeSi phase increased whereas that ofFe5Si3 phase decreased with increasing undercooling. For the Cu-rich zone, FeSi intermetallic compound was always the primary phase. Energy-dispersive spectrometry analyses showed that the average compositions of separated zones have deviated substantially from the original alloycomposition.展开更多
Dry coal separation has been the most significant process in the field of coal beneficiation to date, because of its special advantage of operation with no water consumption. Mineral dry separation research has receiv...Dry coal separation has been the most significant process in the field of coal beneficiation to date, because of its special advantage of operation with no water consumption. Mineral dry separation research has received wide attention, particularly in countries and regions experiencing drought and water shortages. During the process of dense coal gas-solid fluidized bed beneficiation, the material is stratified according to its density; the high density material layer remains at the bed bottom, and thus the high density coarse particle bed becomes an important infuencing factor in fluidized bed stability. In the steady fluidization stage, a small number of large radius bubbles are the direct cause of unsteady fluidization in the tradi- tional fluidized bed. The dispersion effect of the secondary air distribution bed for air flow is mainly apparent in the gas region; when the particle size exceeds 13 mm, the secondary air distribution bed has a synergistic effect on the density stability of the upper fluidized layer. When the particle size is small, especially when less than 6 ram, particles will constantly move, accounting for instability of the secondary air distribution bed and distorting the stability of the upper fluidized bed. Under optimum operation conditions, the probable deviation E of gas-solid separation fluidized with a high density coarse particle layer can be as low as 0.085 g/cm3.展开更多
A series of organosilica sols are prepared by the polymeric sol–gel method using 1,2-bis(triethoxysilyl)ethane(BTESE)as the precursor.Particle size distributions of the BTESE-derived sols are systematically investiga...A series of organosilica sols are prepared by the polymeric sol–gel method using 1,2-bis(triethoxysilyl)ethane(BTESE)as the precursor.Particle size distributions of the BTESE-derived sols are systematically investigated by carefully adjusting the synthesis parameters(i.e.,water ratios,acid ratios and solvent ratios)in the sol process.In certain conditions,increasing the water ratio or the acid ratio tends to cause larger sol sizes and bimodal particle size distributions.However,higher solvent ratios lead to smaller sol sizes and unimodal particle size distributions.The organosilica membranes prepared from the optimized sols show excellent H_2 permeances(up to 4.2×10^(-7)mol·m^(-2)·s^(-1)·Pa^(-1))and gas permselectitivies(H_2/CO_2 is 9.5,H_2/N_2 is 50 and H_2/CH_4 is 68).This study offers significant insights into the relationship between the sol synthesis parameters,sol sizes and membrane performance.展开更多
Separation density is one of the most concerned operating parameters in gravity beneficiation.Although equal-errors cut point or distribution density is usually used as practical separation density in gravity benefici...Separation density is one of the most concerned operating parameters in gravity beneficiation.Although equal-errors cut point or distribution density is usually used as practical separation density in gravity beneficiation, the gravity separating process complexly affected by many kinds of factors is actually carried out at a fluctuant density; namely, the practical separation density is essentially a random variable.The studied results show that the equal-errors cut point is the mathematical expectation of this random variable, and the distribution density corresponds to the highest separation efficiency in the gravity separation process.This shows that the distribution density is the best working point of the gravity separation equipment under a particular operating condition.Therefore,in order to fully develop the function of the gravity separation equipment, the distribution density should be close to the theoretical separation density unlimitedly in the range of minimum fluctuation.展开更多
Solution properties of 7S globulins (7S), 11S globulins (11S) and soy protein isolates (SPI) in dimethylsulfoxide (DMSO)/urea solvent system were studied by intrinsic viscosity and particle size distributions. The res...Solution properties of 7S globulins (7S), 11S globulins (11S) and soy protein isolates (SPI) in dimethylsulfoxide (DMSO)/urea solvent system were studied by intrinsic viscosity and particle size distributions. The results showed that the existence of urea was the main reason for the denaturation and solubility of soy protein in the system, and the effects were more obvious with increasing of urea concentration in solutions. Suitably dissolution temperature and time contributed to the solubility of soy proteins.展开更多
文摘利用小麦京771×Pm97034产生的重组自交系(recombinant inbred lines,RIL)群体,对Zeleny沉淀值、谷蛋白膨胀指数(swelling index of glutenin,SIG)、湿面筋含量、面筋指数、面粉膨胀势、碱性水保持力(alkline water retention capacity,AWRC)、籽粒硬度、蛋白质含量等8个品质性状在RIL群体中的分离和分布规律进行了研究。结果表明,这些品质性状在重组自交系群体中呈连续变异,分布频率大致接近正态分布,同时存在双向超亲分离现象。多元逐步回归分析表明:SIG值、面筋指数、蛋白质含量和籽粒硬度可以解释Zeleny沉淀值的77.7%的表型变异,其中SIG值与Zeleny沉淀值的关系最密切。
基金Project(2012BAF03B05)supported by the National Key Technology R&D Program of ChinaProject(61025015)supported by the National Natural Science Foundation for Distinguished Young Scholars of China+1 种基金Project(61273185)supported by the National Natural Science Foundation of ChinaProject(2012CK4018)supported by the Science and Technology Project of Hunan Province,China
文摘A resolution method based on Gaussian-like distribution for overlapped linear sweep polarographic peaks was proposed to simultaneously detect the polymetallic components, such as Zn(Ⅱ) and Co(Ⅱ), coexisting in the leaching solution of zinc hydrometallurgy. A Gaussian-like distribution was constructed as the sub-model of overlapped peaks by analyzing the characteristics of linear sweep polarographic curve. Then, the abscissas of each peak and trough were pinpointed through multi-resolution wavelet decomposition, the curve and its derivative curves were fitted by using nonlinear weighted least squares (NWLS). Finally, overlapped peaks were resolved into independent sub-peaks based on fitted reconstruction parameters. The experimental results show that the relative error of half-wave potential pinpointed by multi-resolution wavelet decomposition is less than 1% and the accuracy of Ip fitted by NWLS is higher than 96%. The proposed resolution method is effective for overlapped linear sweep polarographic peaks of Zn(Ⅱ) and Co(Ⅱ).
基金Supported by the National Natural Science Foundation of China (21076073)the Shanghai Foundation for Development of Science and Technology (10DZ1201300)Sci-Tech Development Plan of SINOPEC (109070)
文摘Centered on thetechniques and industrial applications of the reinforced cyclonic separation process, its principles and mechanism for separation ot ions, molecules and their aggregates using polyalsperse aroplets are discussed generally; the characteristics and influential factors of fish-hook phenomenon of the grade efficiency curve in cyclonic separation for both gas and liquid are analyzed; and the influence of shear force on particle be- havior (or that of particle swarm) is also summarized. A novel idea for cyclonic separation is presented here: enhancing the cyclonic seoaration process of ions, molecules and their aggregates with monodisperse microspheres and their surface grafting, rearranging the distribution of particles by size using centrifugal field, reinforcing the cyclonic separation performance with orderly arranged particle swarm. Also the investigation of the shortcut flow, recirculation flow, the asymmetric structure and non-linear characteristics of the cyclonic flow field with a com-bined method of Volumetric 3-component Velocimetry (V3V) and Phase-Doppler Particle Anemometer (PDPA) are elaborated. It is recommended to develop new systems for the separation of heterogeneous phases with cyclonic technology, in accordance with the capture and reuse of CO2, methanol to olefins (MTO) process, coal transfer, andthe exploitation of oil shale.
基金This work was supported by the National Natural Science Foundation of China (No.21222308, No.21103187, and No.21133006), the Chinese Academy of Sciences, and the National Basic Research Program of China (No. 2013CB922200).
文摘We present photoelectron angular distribution of the aligned molecular ion H2^+ by intense ultrashort attosecond extreme ultraviolet laser pulses from numerical solutions of timedependent Schrodinger equations. Photoionization from a superposition state of the ground 1sσg and the excited 2pσu states with pulses at photon energies above the ionization potential, hω〉Ip, and intensity 10^14 W/cm^2, yields pulse duration dependent asymmetry of photoelectron angular distributions. We attribute the asymmetry to the periodical oscillation of the coherent electron wave packets, resulting from the interference of the two electronic states. For the processes with long pulse durations, such duration dependence is absent and symmetric angular distributions are obtained.
基金Projects(N140108001,N150106003)supported by the Fundamental Research Funds for National University of China
文摘The pulsed power is a potential means for energy saving and presents an alternative to the conventional mechanical communication for minerals.The effect of magnetic pulse treatment on grindability of a magnetite ore was investigated by grindability tests.The results of the investigation show that the pulsed treatment has little effect on the particle size distribution of the magnetite ore.Significant micro-cracks or fractures are not found by SEM analysis in magnetic pulse treated sample.Magnetic separation of magnetic pulse treated and untreated magnetite ore indicates that iron recovery increases from 81.3% in the untreated sample to 87.7% in the magnetic pulse treated sample,and the corresponding iron grade increases from 42.1% to 44.4%.The results demonstrate that the magnetic pulse treatment does not significantly weaken the mineral grain boundaries or facilitate the liberation of minerals,but is beneficial to magnetic separation.
文摘Eye observation was used to evaluate the segregation degree of asphalt pavement, which was not much creditable. To the asphalt pavement, road surface texture measuring method which has appeared recently can identify gradational segregation; but it can’t reflect the influence of the temperature segregation. However, using infrared temperature detector to evaluate the segregation must be taken during paving, which brings much inconvenience. In this paper, measuring the air voids distribution using non-nuclear density gauge to evaluate asphalt pavement segregation was introduced. Result shows that this method can directly reflect the comprehensive results of the two types of segregation in a high efficient and accurate way. Moreover, using the sketch map of segregation area can help to analyze the segregation reason visually.
基金Projects(51271150,51327901,51371150)supported by the National Natural Science Foundation of China
文摘Liquid Fe35Cu35Si30alloy has achievedthemaximum undercooling of 328 K (0.24TL) with glass fluxing method, and it displayed triple solidification mechanisms. A critical undercooling of 24 K was determined for metastable liquid phase separation. At lower undercoolings,α-Fe phase was the primary phase and the solidification microstructure appeared as homogeneous well-defined dendrites. When the undercooling exceeded 24 K, the sample segregated into Fe-rich and Cu-rich zones. In the Fe-rich zone, FeSi intermetallic compound was the primary phase within the undercooling regime below 230 K, while Fe5Si3intermetallic compound replaced FeSi phase as the primary phase at larger undercoolings. The growth velocity of FeSi phase increased whereas that ofFe5Si3 phase decreased with increasing undercooling. For the Cu-rich zone, FeSi intermetallic compound was always the primary phase. Energy-dispersive spectrometry analyses showed that the average compositions of separated zones have deviated substantially from the original alloycomposition.
基金the Key Project of National Fundamental Research and Development of China (No. 2012CB214904)the National Natural Science Foundation of China for Innovative Research Group (No. 51221462)+1 种基金the National Natural Science Foundation of China (Nos. 51134022 and 51174203)Specialized Research Fund for the Doctoral Program of Higher Education (No. 20120095130001)
文摘Dry coal separation has been the most significant process in the field of coal beneficiation to date, because of its special advantage of operation with no water consumption. Mineral dry separation research has received wide attention, particularly in countries and regions experiencing drought and water shortages. During the process of dense coal gas-solid fluidized bed beneficiation, the material is stratified according to its density; the high density material layer remains at the bed bottom, and thus the high density coarse particle bed becomes an important infuencing factor in fluidized bed stability. In the steady fluidization stage, a small number of large radius bubbles are the direct cause of unsteady fluidization in the tradi- tional fluidized bed. The dispersion effect of the secondary air distribution bed for air flow is mainly apparent in the gas region; when the particle size exceeds 13 mm, the secondary air distribution bed has a synergistic effect on the density stability of the upper fluidized layer. When the particle size is small, especially when less than 6 ram, particles will constantly move, accounting for instability of the secondary air distribution bed and distorting the stability of the upper fluidized bed. Under optimum operation conditions, the probable deviation E of gas-solid separation fluidized with a high density coarse particle layer can be as low as 0.085 g/cm3.
基金Supported by the National Natural Science Foundation of China(21276123,21490581)the National High Technology Research and Development Program of China(2012AA03A606)+1 种基金the "Summit of the Six Top Talents" Program of Jiangsu Province(2011-XCL-021)the Open Research Fund Program of Collaborative Innovation Center of Membrane Separation and Water Treatment(2016YB01)
文摘A series of organosilica sols are prepared by the polymeric sol–gel method using 1,2-bis(triethoxysilyl)ethane(BTESE)as the precursor.Particle size distributions of the BTESE-derived sols are systematically investigated by carefully adjusting the synthesis parameters(i.e.,water ratios,acid ratios and solvent ratios)in the sol process.In certain conditions,increasing the water ratio or the acid ratio tends to cause larger sol sizes and bimodal particle size distributions.However,higher solvent ratios lead to smaller sol sizes and unimodal particle size distributions.The organosilica membranes prepared from the optimized sols show excellent H_2 permeances(up to 4.2×10^(-7)mol·m^(-2)·s^(-1)·Pa^(-1))and gas permselectitivies(H_2/CO_2 is 9.5,H_2/N_2 is 50 and H_2/CH_4 is 68).This study offers significant insights into the relationship between the sol synthesis parameters,sol sizes and membrane performance.
基金Supported by the Young Science Foundation of China(50025411)the Doctoral Science Research Foundation of University(20030290015)
文摘Separation density is one of the most concerned operating parameters in gravity beneficiation.Although equal-errors cut point or distribution density is usually used as practical separation density in gravity beneficiation, the gravity separating process complexly affected by many kinds of factors is actually carried out at a fluctuant density; namely, the practical separation density is essentially a random variable.The studied results show that the equal-errors cut point is the mathematical expectation of this random variable, and the distribution density corresponds to the highest separation efficiency in the gravity separation process.This shows that the distribution density is the best working point of the gravity separation equipment under a particular operating condition.Therefore,in order to fully develop the function of the gravity separation equipment, the distribution density should be close to the theoretical separation density unlimitedly in the range of minimum fluctuation.
基金National Natural Science Foundation of China (No.50303003)
文摘Solution properties of 7S globulins (7S), 11S globulins (11S) and soy protein isolates (SPI) in dimethylsulfoxide (DMSO)/urea solvent system were studied by intrinsic viscosity and particle size distributions. The results showed that the existence of urea was the main reason for the denaturation and solubility of soy protein in the system, and the effects were more obvious with increasing of urea concentration in solutions. Suitably dissolution temperature and time contributed to the solubility of soy proteins.