A stripping batch distillation column is preferred when the amount of the light component in the feed is small and the products are to be recovered at high purity. The operation modes of a batch stripping are believed...A stripping batch distillation column is preferred when the amount of the light component in the feed is small and the products are to be recovered at high purity. The operation modes of a batch stripping are believed to be the same as those of a rectifier. However, the control system of a stripper is different. In this paper, we explore three different control methods with Hysys (Hyprotech Ltd. 1997) for a batch stripper. The main difference is the control scheme for reboiler liquid level: (a) controlled by reflux flow; (b) controlled by reboiler heat duty; (c) controlled by bottom product flow. The main characteristics of operating a batch stripper with different control scheme are presented in this paper. Guidelines are provided for the startup of a batch stripper, the effects of somecontrol tuning parameters on the column performance are discussed.展开更多
分离纯度较高的 NK 细胞对在体外研究 NK 细胞对靶细胞的杀伤作用有着重要的意义。本文研究了利用流式细胞仪分离 NK 细胞的技术方法,主要分析了细胞的流速、喷嘴驱动频率、液滴形成的中断距离等因素对分离细胞纯度的影响,并分离出纯度...分离纯度较高的 NK 细胞对在体外研究 NK 细胞对靶细胞的杀伤作用有着重要的意义。本文研究了利用流式细胞仪分离 NK 细胞的技术方法,主要分析了细胞的流速、喷嘴驱动频率、液滴形成的中断距离等因素对分离细胞纯度的影响,并分离出纯度较高的 NK 细胞。展开更多
In this article,we review the advancement in nanoseparation and concomitant purification of nanoparticles(NPs) by using density gradient ultracentrifugation technique(DGUC) and demonstrated by taking several typical e...In this article,we review the advancement in nanoseparation and concomitant purification of nanoparticles(NPs) by using density gradient ultracentrifugation technique(DGUC) and demonstrated by taking several typical examples.Study emphasizes the conceptual advances in classification,mechanism of DGUC and synthesis-structure-property relationships of NPs to provide the significant clue for the further synthesis optimization.Separation,concentration,and purification of NPs by DGUC can be achieved at the same time by introducing the water/oil interfaces into the separation chamber.We can develop an efficient method ‘‘lab in a tube" by introducing a reaction zone or an assembly zone in the gradient to find the surface reaction and assembly mechanism of NPs since the reaction time can be precisely controlled and the chemical environment change can be extremely fast.Finally,to achieve the best separation parameters for the colloidal systems,we gave the mathematical descriptions and computational optimized models as a new direction for making practicable and predictable DGUC separation method.Thus,it can be helpful for an efficient separation as well as for the synthesis optimization,assembly and surface reactions as a potential cornerstone for the future development in the nanotechnology and this review can be served as a plethora of advanced notes on the DGUC separation method.展开更多
基金Supported by CONICET (Consejo Nacional de Investigaciones Cientificas y Tecnicas, Argentina) (No. 778) and the Scientific Research Foundation of the State Education Ministry for Returned Overseas Chinese Scholar.
文摘A stripping batch distillation column is preferred when the amount of the light component in the feed is small and the products are to be recovered at high purity. The operation modes of a batch stripping are believed to be the same as those of a rectifier. However, the control system of a stripper is different. In this paper, we explore three different control methods with Hysys (Hyprotech Ltd. 1997) for a batch stripper. The main difference is the control scheme for reboiler liquid level: (a) controlled by reflux flow; (b) controlled by reboiler heat duty; (c) controlled by bottom product flow. The main characteristics of operating a batch stripper with different control scheme are presented in this paper. Guidelines are provided for the startup of a batch stripper, the effects of somecontrol tuning parameters on the column performance are discussed.
基金supported by the National Natural Science Foundation of China(NSFC)the National Key Research and Development Project of China(2016YFF0204402)+1 种基金the Program for Changjiang Scholars and Innovative Research Team in the University(IRT1205)the Fundamental Research Funds for the Central Universities,the Long-Term Subsidy Mechanism from the Ministry of Finance and the Ministry of Education of PRC
文摘In this article,we review the advancement in nanoseparation and concomitant purification of nanoparticles(NPs) by using density gradient ultracentrifugation technique(DGUC) and demonstrated by taking several typical examples.Study emphasizes the conceptual advances in classification,mechanism of DGUC and synthesis-structure-property relationships of NPs to provide the significant clue for the further synthesis optimization.Separation,concentration,and purification of NPs by DGUC can be achieved at the same time by introducing the water/oil interfaces into the separation chamber.We can develop an efficient method ‘‘lab in a tube" by introducing a reaction zone or an assembly zone in the gradient to find the surface reaction and assembly mechanism of NPs since the reaction time can be precisely controlled and the chemical environment change can be extremely fast.Finally,to achieve the best separation parameters for the colloidal systems,we gave the mathematical descriptions and computational optimized models as a new direction for making practicable and predictable DGUC separation method.Thus,it can be helpful for an efficient separation as well as for the synthesis optimization,assembly and surface reactions as a potential cornerstone for the future development in the nanotechnology and this review can be served as a plethora of advanced notes on the DGUC separation method.
