Surface modification of Diamond-like carbon (DLC) films was carried out in order to estimate the reliability of the ultra thin DLC films. The wear resistance, conductivity and mechatronic reliability of the films were...Surface modification of Diamond-like carbon (DLC) films was carried out in order to estimate the reliability of the ultra thin DLC films. The wear resistance, conductivity and mechatronic reliability of the films were studied by contact atomic force microscope (AFM), electric force microscope (EFM) and conductive AFM. The failure mechanism of pits formed and the reason for conductivity changed of DLC films were examined.展开更多
CVD polycrystalline diamond surfaces were etched using reactive ion etching system with either a conventional stainless steel electrode or MgO sintered ceramic containing electrode. The micro-needle array of high aspe...CVD polycrystalline diamond surfaces were etched using reactive ion etching system with either a conventional stainless steel electrode or MgO sintered ceramic containing electrode. The micro-needle array of high aspect on diamond substrate surfaces obtained with MgO electrode was fabricated by using back-sputtering from MgO electrode. The RMS roughness of diamond substrate surfaces obtained with MgO electrode is higher than those obtained with stainless steel electrode. The secondary electron emission coefficient in Ne gas of the diamond obtained with MgO electrode was twice that obtained with the stainless steel electrode.展开更多
Cathode samples of nano-diamond by graphitization pretreatment with different temperatures were fabricated by electrophoresis, then the structures and morphologies of the cathode samples were characterized by scanning...Cathode samples of nano-diamond by graphitization pretreatment with different temperatures were fabricated by electrophoresis, then the structures and morphologies of the cathode samples were characterized by scanning electron microscope(SEM) and X-ray diffraction(XRD), and the field emission tests were conducted. The effects of graphitization pretreatment on the field emission characteristics of nano-diamond cathode surface on titanium substrate are studied. The results indicate that the surface morphologies of nano-diamond cathode samples after graphitization pretreatment change a lot, and the field emission characteristics in low-voltage area are improved obviously. However, in high-voltage area, the curve distortion happens, and it doesn't conform the mechanism of field emission characteristics.展开更多
文摘Surface modification of Diamond-like carbon (DLC) films was carried out in order to estimate the reliability of the ultra thin DLC films. The wear resistance, conductivity and mechatronic reliability of the films were studied by contact atomic force microscope (AFM), electric force microscope (EFM) and conductive AFM. The failure mechanism of pits formed and the reason for conductivity changed of DLC films were examined.
文摘CVD polycrystalline diamond surfaces were etched using reactive ion etching system with either a conventional stainless steel electrode or MgO sintered ceramic containing electrode. The micro-needle array of high aspect on diamond substrate surfaces obtained with MgO electrode was fabricated by using back-sputtering from MgO electrode. The RMS roughness of diamond substrate surfaces obtained with MgO electrode is higher than those obtained with stainless steel electrode. The secondary electron emission coefficient in Ne gas of the diamond obtained with MgO electrode was twice that obtained with the stainless steel electrode.
基金supported by the PH.D Start-up Foundation of Yan’an University(No.YD 2010-04)the Special Foundation of Yan’an University(No.YDZD 2011-01)+3 种基金the 2014 Education and Innovation Project of Yan’an University for Graduate Studentthe 2014 Local University National Training Project of Innovation and Entrepreneurship for Undergraduates(No.201410719023)the Special Research Funds for Discipline Construction of High Level University Construction(No.2015SXTS02)the Natural Science Foundation of Shaanxi Province(No.2014JM2-5058)
文摘Cathode samples of nano-diamond by graphitization pretreatment with different temperatures were fabricated by electrophoresis, then the structures and morphologies of the cathode samples were characterized by scanning electron microscope(SEM) and X-ray diffraction(XRD), and the field emission tests were conducted. The effects of graphitization pretreatment on the field emission characteristics of nano-diamond cathode surface on titanium substrate are studied. The results indicate that the surface morphologies of nano-diamond cathode samples after graphitization pretreatment change a lot, and the field emission characteristics in low-voltage area are improved obviously. However, in high-voltage area, the curve distortion happens, and it doesn't conform the mechanism of field emission characteristics.
