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微波合成片状β-SiC的工艺研究 被引量:2
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作者 董陈江 李纪鹏 +6 位作者 王若名 宋勃震 高前程 范书珩 理思远 李文豪 张锐 《现代技术陶瓷》 CAS 2019年第3期199-206,共8页
片状β-SiC可通过使用石墨纸(C)作为碳源、正硅酸乙酯水解制得的SiO2溶胶.凝胶作为硅源、经微波加热合成。本文根据加热过程中微波炉加热温度、输入功率和反射功率的变化曲线,探讨了微波合成片状β-SiC过程中微波加热热效应。分别选择11... 片状β-SiC可通过使用石墨纸(C)作为碳源、正硅酸乙酯水解制得的SiO2溶胶.凝胶作为硅源、经微波加热合成。本文根据加热过程中微波炉加热温度、输入功率和反射功率的变化曲线,探讨了微波合成片状β-SiC过程中微波加热热效应。分别选择1100°C、1200°C、1300°C、1400°C和1500°C五个微波烧结温度,研究了相同保温时间下不同加热温度对微波合成片状β-SiC的影响。在烧结温度1300°C下,选取保温时间分别为0min、10min、30min和60min,探索了同一合成温度下不同保温时间对微波合成片状β-SiC的影响。采用XRD,SEM技术对样品进行了表征。结果发现,烧结温度为1100°C时,产物中合成了片状β-SiC;当烧结温度为1400°C时,片状β-SiC转化为β-SiC颗粒。过高的烧结温度和过长的保温时间都将导致β-SiC的氧化。在1300°C保温30min条件下得到的片状β-SiC生长最好。 展开更多
关键词 片状β-SiC 微波加热 加热热效应
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Momentum-space imaging spectroscopy for the study of nanophotonic materials 被引量:3
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作者 Yiwen Zhang Maoxiong Zhao +12 位作者 Jiajun Wang Wenzhe Liu Bo Wang Songting Hu Guopeng Lu Ang Chen Jing Cui Weiyi Zhang Chia Wei Hsu Xiaohan Liu Lei Shi Haiwei Yin Jian Zi 《Science Bulletin》 SCIE EI CSCD 2021年第8期824-838,M0004,共16页
The novel phenomena in nanophotonic materials, such as the angle-dependent reflection and negative refraction effect, are closely related to the photonic dispersions EepT. EepT describes the relation between energy E ... The novel phenomena in nanophotonic materials, such as the angle-dependent reflection and negative refraction effect, are closely related to the photonic dispersions EepT. EepT describes the relation between energy E and momentum p of photonic eigenmodes, and essentially determines the optical properties of materials. As EepT is defined in momentum space(k-space), the experimental method to detect the energy distribution, that is the spectrum, in a momentum-resolved manner is highly required. In this review, the momentum-space imaging spectroscopy(MSIS) system is presented, which can directly study the spectral information in momentum space. Using the MSIS system, the photonic dispersion can be captured in one shot with high energy and momentum resolution. From the experimental momentumresolved spectrum data, other key features of photonic eigenmodes, such as quality factors and polarization states, can also be extracted through the post-processing algorithm based on the coupled mode theory. In addition, the interference configurations of the MSIS system enable the measurement of coherence properties and phase information of nanophotonic materials, which is important for the study of light-matter interaction and beam shaping with nanostructures. The MSIS system can give the comprehensive information of nanophotonic materials, and is greatly useful for the study of novel photonic phenomena and the development of nanophotonic technologies. 展开更多
关键词 Momentum space imaging Nanophotonic material Photonic dispersion Photonic eigenmode Quality factor Polarization state
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Non-thermal radiation heating synthesis of nanomaterials
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作者 Guowei Xiong Jin Jia +4 位作者 Lili Zhao Xiaoyan Liu Xiaoli Zhang Hong Liu Weijia Zhou 《Science Bulletin》 SCIE EI CSCD 2021年第4期386-406,M0004,共22页
The nanoscale effect enables the unique magnetic,optical,thermal and electrical properties of nanostructured materials and has attracted extensive investigation for applications in catalysis,biomedicine,sensors,and en... The nanoscale effect enables the unique magnetic,optical,thermal and electrical properties of nanostructured materials and has attracted extensive investigation for applications in catalysis,biomedicine,sensors,and energy storage and conversion.The widely used synthesis methods,such as traditional hydrothermal reaction and calcination,are bulk heating processes based on thermal radiation.Differing from traditional heating methods,non-thermal radiation heating technique is a local heating mode.In this regard,this review summarizes various non-thermal radiation heating methods for synthesis of nanomaterials,including microwave heating,induction heating,Joule heating,laser heating and electron beam heating.The advantages and disadvantages of these non-thermal radiation heating methods for the synthesis of nanomaterials are compared and discussed.Finally,the future development and challenges of non-thermal radiation heating method for potential synthesis of nanomaterials are discussed. 展开更多
关键词 Synthesis of nanomaterials Microwave heating Induction heating Joule heating Laser heating
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