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FAAS法研究六钛酸钾晶须对Cd(Ⅱ)的动/静态吸附行为 被引量:1
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作者 程永华 《环境科学与技术》 CAS CSCD 北大核心 2009年第8期72-75,共4页
以火焰原子吸收光谱法(FAAS)为检测手段,研究了六钛酸钾晶须对镉的动态、静态吸附性能,考察影响吸附率的相关因素,对比了静态、动态解吸回收率的影响,同时考察了解吸剂的酸度、流速、用量等对回收率的影响,结果表明:在动态实验中,pH7,流... 以火焰原子吸收光谱法(FAAS)为检测手段,研究了六钛酸钾晶须对镉的动态、静态吸附性能,考察影响吸附率的相关因素,对比了静态、动态解吸回收率的影响,同时考察了解吸剂的酸度、流速、用量等对回收率的影响,结果表明:在动态实验中,pH7,流速1.0mL/min.,吸附剂用量0.1g时,Cd(Ⅱ)的吸附效果最佳;以10mL0.1mol/LHNO3为洗脱剂,流速为0.5mL/min时,可将Cd(Ⅱ)完全洗脱。静态实验中,pH7,六钛酸钾晶须用量0.2g,吸附率可达到90%以上。以25mL2mol/L的硝酸溶液对Cd(Ⅱ)进行洗脱,Cd(Ⅱ)的回收率可达99%以上。在优化的试验条件下,本法的检出限为12ng/mL;相对标准偏差为0.7%(Cd(Ⅱ):1μg/mL,n=11)。 展开更多
关键词 FAAS 六钛酸钾 Cd(Ⅱ) 动/静态吸附
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电涡流传感器动/静态自动校验仪的研究 被引量:1
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作者 徐健 《仪表技术》 2014年第9期51-54,共4页
针对当前电涡流传感器实际校验中存在的问题,设计开发了一种电涡流传感器全自动动/静态校验仪。介绍了该校验仪的总体架构,给出了硬件结构框图和软件功能界面。与现有的校验设备相比,该校验仪体现了校验过程的全自动化及对校验数据自动... 针对当前电涡流传感器实际校验中存在的问题,设计开发了一种电涡流传感器全自动动/静态校验仪。介绍了该校验仪的总体架构,给出了硬件结构框图和软件功能界面。与现有的校验设备相比,该校验仪体现了校验过程的全自动化及对校验数据自动生成报表和图形的智能化管理,具有精度高、结构简单、操作灵活、动/静态特性一体化校验的特点。 展开更多
关键词 电涡流传感器 全自 动/静态校验仪
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秋兰姆类促进剂TOTD对硫化胶低动/静态模量比之影响
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作者 王作龄 《世界橡胶工业》 2007年第12期17-22,共6页
应用促进剂TOTD/助剂DS并用体系对橡胶制品的低动/静态模量比的影响进行了研究与阐述。
关键词 促进剂TOTD 助剂DS 动/静态模量比
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动静态载荷下光纤光栅传感器敏感特性研究 被引量:5
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作者 曾捷 王文娟 +3 位作者 王博 王鑫伟 张先辉 宋昊 《南京航空航天大学学报》 EI CAS CSCD 北大核心 2015年第3期397-402,共6页
针对航空航天领域板结构动静态载荷监测需求,研究了基于铝合金板结构的光纤光栅(Fiber Bragg grating,FBG)传感器感知特性。从静载监测角度,得到光纤光栅传感器中心波长偏移量与加载距离、载荷大小和加载角度的对应关系。从动载监测角度... 针对航空航天领域板结构动静态载荷监测需求,研究了基于铝合金板结构的光纤光栅(Fiber Bragg grating,FBG)传感器感知特性。从静载监测角度,得到光纤光栅传感器中心波长偏移量与加载距离、载荷大小和加载角度的对应关系。从动载监测角度,分别得到在不同加载距离和不同加载夹角的载荷作用下,光栅中心波长最大峰值幅度和基于小波包分解的能量谱特征随冲击载荷属性变化的响应特性。研究表明在动静态载荷作用下,光纤光栅传感器中心波长偏移量随加载载荷的增大而呈现良好的单调递增关系。此外,光纤光栅传感器还具有较好的载荷-方向敏感特性,传感器响应灵敏度随着加载夹角增大而逐渐提高。这些特性能够为进一步开展基于光纤光栅传感器的板结构动静态载荷辨识与损伤监测提供有益帮助。 展开更多
关键词 光纤光栅传感器 动/静态载荷 敏感特性 板结构
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基于分布式FBG的钢轨动静态载荷监测研究 被引量:3
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作者 张先辉 史璐 +2 位作者 刘苏州 毛超群 梁大开 《传感器与微系统》 CSCD 2015年第8期39-41,45,共4页
针对铁道领域钢轨应变监测需求,提出一种基于光纤Bragg光栅(FBG)传感器的钢轨应变监测系统。从静态载荷监测角度,研究了不同加载位置的FBG传感器中心波长随加载载荷大小变化的关系。从动态载荷监测角度,研究了循环加载状态下的各FBG传... 针对铁道领域钢轨应变监测需求,提出一种基于光纤Bragg光栅(FBG)传感器的钢轨应变监测系统。从静态载荷监测角度,研究了不同加载位置的FBG传感器中心波长随加载载荷大小变化的关系。从动态载荷监测角度,研究了循环加载状态下的各FBG传感器中心波长偏移量特性。研究表明:在静态载荷作用下,各FBG传感器中心波长偏移量均随加载载荷增大而呈现良好线性变化关系,且传感器对载荷加载距离和角度变化较为敏感。在动态循环载荷作用下,FBG传感器网络能够较好地实现对钢轨应变和温度参量的实时监测。这些研究为钢轨应变与损伤分布式在线监测技术提供了有益借鉴。 展开更多
关键词 光纤BRAGG光栅传感器 动/静态载荷 钢轨 监测
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数控加工中心框架结构动静态性能优化设计方法
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作者 孟祥德 张学玲 满佳 《机械设计》 CSCD 北大核心 2018年第S1期106-110,共5页
为提高数控加工中心的动静态性能,对加工中心的框架结构进行了动态锤击法模态试验测试和有限元分析,针对测试和有限元计算结果分析机床结构的薄弱环节,根据结构优化目标,对框架结构各部件进行改进,提出了整机结构改进方案,并对原结构和... 为提高数控加工中心的动静态性能,对加工中心的框架结构进行了动态锤击法模态试验测试和有限元分析,针对测试和有限元计算结果分析机床结构的薄弱环节,根据结构优化目标,对框架结构各部件进行改进,提出了整机结构改进方案,并对原结构和改进结构进行动态和静态刚度比较。结果表明,优化方案动静态特性均有所提高,优化方法合理可行。 展开更多
关键词 数控加工中心 动/静态性能 结构优化 有限元方法 模态测试
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浮选颗粒条栅结构表面润湿行为特性研究
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作者 张锐 于锋 +1 位作者 邢耀文 桂夏辉 《选煤技术》 CAS 2024年第4期13-21,共9页
矿物颗粒间表面润湿性差异是浮选成功的关键,受表面化学性质与物理形貌结构的双重影响。为进一步明确表面物理形貌结构对液滴在矿物颗粒表面上润湿行为的影响,采用光刻显影技术制备了5种具有不同粗糙度系数和表面面积分数的条栅结构聚... 矿物颗粒间表面润湿性差异是浮选成功的关键,受表面化学性质与物理形貌结构的双重影响。为进一步明确表面物理形貌结构对液滴在矿物颗粒表面上润湿行为的影响,采用光刻显影技术制备了5种具有不同粗糙度系数和表面面积分数的条栅结构聚二甲基硅氧烷(PDMS)表面,并利用自制的动/静态接触角测量系统及润湿三相接触线行为测试系统对液滴在PDMS表面上的润湿行为进行了测试。动/静态接触角测试结果表明:当表面粗糙度系数相同时,固体表面面积分数增加,条栅结构表面不同润湿方向上的接触角均呈减小趋势,而当表面面积分数相同时,条栅结构表面不同润湿方向上的接触角则与固体表面粗糙度系数呈正相关;此外,各样品表面垂直于条栅结构方向的动/静态接触角均大于平行方向(即θ_(⊥)>θ_(∥)),且不同润湿方向上接触角的差异随样品表面润湿性的增强而减小。动态接触角测试结果还表明:表面接触角滞后(Δθ=θ_(a)-θ_(r))与表面面积分数呈正相关,而与表面粗糙度系数呈负相关,且前进与后退接触角的预测值与试验值基本吻合,说明动态接触角能够真实地反映固体表面润湿性;此外,在液滴滚动时,其运动行为总是周期性地发生后端接触线先从固体表面分离,而后液滴重新与固体表面发生黏附形成新的前端接触线的过程,这种运动特性在不同条栅结构表面上完全相同。润湿三相接触线行为测试结果表明:液滴在条栅结构表面优先沿着条栅结构方向润湿或去润湿,而跨越条栅结构润湿时,受表面微结构的“钉扎”作用,润湿半径远小于平行润湿方向,且三相接触线在不同条栅结构表面的移动均呈现“解钉—钉扎—再解钉—再钉扎”的一种断续周期性过程。研究结果深化了矿物颗粒表面物理形貌结构对其润湿行为特性的影响,可为后续通过表面形貌调控颗粒表面润湿性起到一定的理论支撑作用。 展开更多
关键词 浮选 润湿行为 条栅结构 表面形貌 动/静态接触角测量 三相接触线行为测试 各向异性 断续周期性
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级配碎石动态CBR试验研究 被引量:5
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作者 谢远勇 李改 《公路工程》 北大核心 2014年第2期5-8,共4页
针对不同级配类型进行静态和动态CBR试验,得出级配碎石结构类型对CBR的影响:在悬浮密实型、骨架密实型和骨架空隙型3种类型中,骨架密实型的CBR值最大,力学性能最优。主要对动态CBR进行研究,气动伺服系统的运用更加具有说服力。动态CBR... 针对不同级配类型进行静态和动态CBR试验,得出级配碎石结构类型对CBR的影响:在悬浮密实型、骨架密实型和骨架空隙型3种类型中,骨架密实型的CBR值最大,力学性能最优。主要对动态CBR进行研究,气动伺服系统的运用更加具有说服力。动态CBR通过应变的变化率反应级配碎石的力学性能,变化率越小,性能越好。通过动态CBR试验数据的进一步处理,得出级配碎石的蠕变模量,能更有效地说明不同级配类型对级配碎石强度特性的影响。 展开更多
关键词 级配类型 力学性能 蠕变模量 强度特性
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热轧H型钢厚度自动控制系统模型研究与实现
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作者 王业涛 《信息技术与信息化》 2013年第6期75-77,83,共4页
随着H型钢应用范围的不断扩大,人们对相应的产品尺寸要求也越来越高。本文以莱钢H型钢生产线精轧控制系统为原型,介绍了厚度自动控制系统的原理、AGC自动控制系统数学模型的建立,以及影响H型钢产品尺寸的主要因素。着重分析了精轧控制... 随着H型钢应用范围的不断扩大,人们对相应的产品尺寸要求也越来越高。本文以莱钢H型钢生产线精轧控制系统为原型,介绍了厚度自动控制系统的原理、AGC自动控制系统数学模型的建立,以及影响H型钢产品尺寸的主要因素。着重分析了精轧控制系统中静态AGC厚度控制系统与动态AGC厚度控制系统的区别和实现的效果。 展开更多
关键词 AGC控制系统 弹性曲线 塑性曲线
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基于Labview的ADC综合性能测试系统 被引量:10
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作者 邓若汉 余金金 +3 位作者 王洪彬 徐星 陈世军 陈永平 《科学技术与工程》 北大核心 2012年第19期4653-4658,共6页
近年来,在电路设计领域高性能的模数转换器(ADC)一直是研究热点。相应的ADC测试评价技术也同样一直受到重点关注。阐述了ADC的参数及其测试的原理和方法,并基于Labview软件和数据采集卡构建了ADC的软硬件测试平台,实现了低成本、高可靠... 近年来,在电路设计领域高性能的模数转换器(ADC)一直是研究热点。相应的ADC测试评价技术也同样一直受到重点关注。阐述了ADC的参数及其测试的原理和方法,并基于Labview软件和数据采集卡构建了ADC的软硬件测试平台,实现了低成本、高可靠性的高速高精度ADC计算机辅助测试的测试系统。最后,使用该测试系统对TI公司的ADS805进行了测试,并给出了测试结果。 展开更多
关键词 ADC测试 LABVIEW 动/静态参数 码密度 FFT 直方图
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基于Matlab的高速高精度ADC测试研究 被引量:14
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作者 戴澜 姜岩峰 刘文楷 《计算机测量与控制》 CSCD 北大核心 2010年第9期2044-2045,2049,共3页
高速高精度模数转换器(ADC)一直是研究热点,相应地ADC的测试技术显得尤为重要;文章首先对ADC动静态参数进行研究,利用概率统计理论得到性能参数的数学表示;然后提出一种ADC动静态参数测试电路实现方案,利用上述性能参数的研究成果和提... 高速高精度模数转换器(ADC)一直是研究热点,相应地ADC的测试技术显得尤为重要;文章首先对ADC动静态参数进行研究,利用概率统计理论得到性能参数的数学表示;然后提出一种ADC动静态参数测试电路实现方案,利用上述性能参数的研究成果和提出的测试电路,对所设计的一种12位50MHz流水线ADC性能参数进行测试,并基于Matlab工具对测试数据进行分析,得到SFDR为65dB,ENOB为9.1位,SNR为56.9 dB,SNDR为56 dB,INL为1.8LSB,试验数据证明了测试方案的可行性。 展开更多
关键词 频谱分析 MATLAB 动/静态参数 信噪比
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高速公路称重系统布置 被引量:2
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作者 徐刚 《公路交通科技》 CAS CSCD 北大核心 2003年第z1期65-68,共4页
按照交通部《超限运输车辆行驶公路管理规定》分析在高速公路上设置动 /静态称重系统的必要性 。
关键词 超限 高速公路 动/静态 设置
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Effect of hot deformation conditions on grain structure and properties of 7085 aluminum alloy 被引量:12
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作者 陈送义 陈康华 +1 位作者 贾乐 彭国胜 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2013年第2期329-334,共6页
The influences of deformation conditions on grain structure and properties of 7085 aluminum alloy were investigated by optical microscopy and transmission electron microscopy in combination with tensile and fracture t... The influences of deformation conditions on grain structure and properties of 7085 aluminum alloy were investigated by optical microscopy and transmission electron microscopy in combination with tensile and fracture toughness tests. The results show that the volume fraction of dynamic recrystallization increased with the decrease of Zener-Hollomon (Z) parameter, and the volume fraction of static recrystallization increased with the increasing of Z parameter. The strength and fracture toughness of the alloy after solution and aging treatment first increased and then decreased with the increase of Z parameter. The microstructure map was established on the basis of microstructure evolution during deformation and solution heat treatment. The optimization deformation conditions were acquired under Z parameters of 1.2×10^10-9.1×10^12. 展开更多
关键词 7085 aluminum alloy Zener-Hollomon parameter hot deformation grain structure dynamic recrystallization static recrystallization
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Static and dynamic mechanical behaviour of ECO-RPC 被引量:2
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作者 赖建中 孙伟 +1 位作者 林玮 金祖权 《Journal of Southeast University(English Edition)》 EI CAS 2005年第2期197-202,共6页
Ecological reactive powder concrete (ECO-RPC) with small sized and differentvolume fraction steel fibers was prepared by substitution of ultra-fine industrial waste powder for50% to 60% cement by weight and replacemen... Ecological reactive powder concrete (ECO-RPC) with small sized and differentvolume fraction steel fibers was prepared by substitution of ultra-fine industrial waste powder for50% to 60% cement by weight and replacement of ground fine quartz sand with natural fine aggregate.The effect of steel fiber volume fraction and curing ages on the static mechanical behaviour ofECO-RPC was studied. Using the split Hopkinson pressure bar technique, the dynamic mechanicalbehaviour of ECO-RPC was investigated under different strain rates. The results show that the staticmechanical behaviour of ECO-RPC increases with the increase of steel fiber volume fraction andcuring ages. The type of ECO-RPC with the substitution of 25% ultra-fine slag, 25% ultra-fine flyash and 10% silica fume is better than the others with compressive strength, flexural strength, andfracture energy more than 200 MPa, 60 MPa and 30 kJ/m^2, respectively. ECO-RPC has excellent strainrate stiffening effects under dynamic load. Its peak stress, peak strain and the area understrain-stress curve increase with the increase of strain rate. Its fracture pattern changes frombrittleness to toughness under high strain rates. 展开更多
关键词 ecological reactive powder concrete (ECO-RPC) industrial waste powder interfacial bond strength fracture energy static and dynamic mechanical behaviour high strainrate
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Separation of macro amounts of tungsten and molybdenum by ion exchange with D309 resin 被引量:13
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作者 卢晓颖 霍广生 廖春华 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2014年第9期3008-3013,共6页
Based on the difference in tendency to polymerize between tungsten and molybdenum, a new method using D309 resin was propounded. The batch tests indicate that the optimum pH value and contact time for the separation a... Based on the difference in tendency to polymerize between tungsten and molybdenum, a new method using D309 resin was propounded. The batch tests indicate that the optimum pH value and contact time for the separation are 7.0 and 4 h respectively, the maxium separation factor of W and Mo is 9.29. And the experimental resules show that isothermal absorbing tungsten and molybdenum belongs to Langmuir model and Freundlich model respectively, and the absorbing kinetics for tungsten is controlled by intra-particle diffusion. With a solution containing 70 g/L WO3 and 28.97 g/L Mo, the effluent with a mass ratio of Mo to WO3 of 76 and the eluate with a mass ratio of WO3 to Mo of 53.33 are obtained after column test. 展开更多
关键词 high concentrated tungstate and molybdenum solution ion exchange batch tests column tests
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Research on measuring time constant of NANMAC thermocouple 被引量:4
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作者 冯浩 张志杰 +1 位作者 黄晓敏 张晋文 《Journal of Measurement Science and Instrumentation》 CAS 2014年第4期1-4,共4页
The theory for measuring the time constant of thermocouple was introduced, and the method for measuring the time constant of NANMAC thermocouple by using dynamic calibration system of transient surface temperature sen... The theory for measuring the time constant of thermocouple was introduced, and the method for measuring the time constant of NANMAC thermocouple by using dynamic calibration system of transient surface temperature sensor was proposed. In this system, static and dynamic calibrations were conducted for infrared detectors and thermocouples, and then both temperature-time curves were obtained. Since the frequency response of infrared detector is superior to that of calibrat- ed thermocouple, the values measured by infrared detectors are taken as true values. Through dividing the values measured with thermocouples by those with infrared detectors, a normalized curve was obtained, based on which the time constant of thermocouple was measured. With this method, the experiments were carried out with NANMAC thermocouple to obtain its time constant. The results show that the method for measuring the time constant is feasible and the dynamic calibration of thermocouples can be achieved at microsecond and millisecond level. This research has a certain reference value for research and application of NANMAC thermocouple temperature sensor. 展开更多
关键词 THERMOCOUPLE time constant static calibration dynamic calibration normalized curve
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Static and dynamic collaborative optimization of ship hull structure 被引量:4
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作者 黄海燕 王德禹 《Journal of Marine Science and Application》 2009年第1期77-82,共6页
The goal of this effort was to provide a static and dynamic collaborative optimization (CO) model for the design of ship hull structure. The CO model integrated with static, mode and dynamic analyses. In the system-... The goal of this effort was to provide a static and dynamic collaborative optimization (CO) model for the design of ship hull structure. The CO model integrated with static, mode and dynamic analyses. In the system-level optimization model, a new objective function was advised, integrating all the subsystem-levels' objective functions, so as to eliminate the effects of dimensions and magnitude order. The proposed CO architecture enabled multi-objectives of the system and subsystem-level to be considered at both levels during optimization. A bi-level optimization strategy was advised, using the multi-island genetic algorithm. The proposed model was demonstrated with a deck optimization problem of container ship stern. The analysis progress and results of example show that the CO strategy is not only feasible and reliable, but also well suited for use in actual optimization problems of ship design. 展开更多
关键词 collaborative optimization multi-island genetic algorithm static analysis dynamic analysis
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Computer Aided Analysis of the Performances of a Tilting Pad Gas Journal Bearing
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作者 周勇 李振清 毛谦德 《Journal of Beijing Institute of Technology》 EI CAS 1993年第1期38-48,共11页
Tilting pad gas journal bearing is one of the most widely used types of aerodynamic bearings due to its inherent excellent stability in high speed applications.A practical method for analyzing and calculating the per-... Tilting pad gas journal bearing is one of the most widely used types of aerodynamic bearings due to its inherent excellent stability in high speed applications.A practical method for analyzing and calculating the per- formances of such bearings is presented as well as its rotordynamics based on the computer aided technique.The method of calculation and the philosophy of programming with a microcomputer for the computer aided analysis are highlighted. 展开更多
关键词 hydrodynamic gas lubricated bearing static characteristics dynamic properties STABILITY
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Quasi-static and dynamic tensile behaviors in electron beam welded Ti-6Al-4V alloy
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作者 张静 谭成文 +2 位作者 任宇 王富耻 才鸿年 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2011年第1期39-44,共6页
The quasi-static and dynamic tensile behaviors in electron beam welded(EBW) Ti-6Al-4V alloy were investigated at strain rates of 10-3 and 103 s-1,respectively,by materials test system(MTS) and reconstructive Hopki... The quasi-static and dynamic tensile behaviors in electron beam welded(EBW) Ti-6Al-4V alloy were investigated at strain rates of 10-3 and 103 s-1,respectively,by materials test system(MTS) and reconstructive Hopkinson bars apparatus.The microstructures of the base metal(BM) and the welded metal(WM) were observed with optical microscope.The fracture characteristics of the BM and WM were characterized with scanning electronic microscope.In Ti-6Al-4V alloy joint,the flow stress of WM is higher than that of BM,while the fracture strain of WM is less than that of BM at strain rates of 103 and 10-3 s-1,respectively.The fracture strain of WM has apparent improvement when the strain rate rises from 10-3 to 103 s-1,while the fracture strain of BM almost has no change.At the same time,the fracture mode of WM alters from brittle to ductile fracture,which causes improvement of the fracture strain of WM. 展开更多
关键词 Ti-6Al-4V alloy electron beam welding quasi-static tensile behavior dynamic behavior fracture mode
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Risk evaluation of rock burst through theory of static and dynamic stresses superposition 被引量:22
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作者 李振雷 窦林名 +3 位作者 王桂峰 蔡武 何江 丁言露 《Journal of Central South University》 SCIE EI CAS CSCD 2015年第2期676-683,共8页
Rock burst is one of the most catastrophic dynamic hazards in coal mining. A static and dynamic stresses superposition-based(SDSS-based) risk evaluation method of rock burst was proposed to pre-evaluate rock burst ris... Rock burst is one of the most catastrophic dynamic hazards in coal mining. A static and dynamic stresses superposition-based(SDSS-based) risk evaluation method of rock burst was proposed to pre-evaluate rock burst risk. Theoretical basis of this method is the stress criterion incurring rock burst and rock burst risk is evaluated according to the closeness degree of the total stress(due to the superposition of static stress in the coal and dynamic stress induced by tremors) with the critical stress. In addition, risk evaluation criterion of rock burst was established by defining the "Satisfaction Degree" of static stress. Furthermore,the method was used to pre-evaluate rock burst risk degree and prejudge endangered area of an insular longwall face in Nanshan Coal Mine in China. Results show that rock burst risk is moderate at advance extent of 97 m, strong at advance extent of 97-131 m,and extremely strong(i.e. inevitable to occur) when advance extent exceeds 131 m(mining is prohibited in this case). The section of two gateways whose floor abuts 15-3 coal seam is a susceptible area prone to rock burst. Evaluation results were further compared with rock bursts and tremors detected by microseismic monitoring. Comparison results indicate that evaluation results are consistent with microseismic monitoring, which proves the method's feasibility. 展开更多
关键词 rock burst HAZARD MINING STRESS risk evaluation microseismic monitoring
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