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浅析化学试验分析中物质的量浓度计算及基本单元的选取
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作者 刘婷蕊 《中文科技期刊数据库(全文版)自然科学》 2024年第1期0213-0216,共4页
本文简述物质的量浓度及其基本单位的选取以及摩尔与基本单元在化学分析中的应用。使试验计算与分析人员正确的理解与掌握法定计量单位,并了解法定计量单位在化学试验分析中的重要性。法定计量单位的标准化和统一化是关系到我国科技、... 本文简述物质的量浓度及其基本单位的选取以及摩尔与基本单元在化学分析中的应用。使试验计算与分析人员正确的理解与掌握法定计量单位,并了解法定计量单位在化学试验分析中的重要性。法定计量单位的标准化和统一化是关系到我国科技、文化、教育发展和国际学术交流的大事。目前,在化学分析中常使用的法定计量单位为物质的量浓度及其基本单元。由于化学试验操作人员、分析人员和从业人员对物质的量浓度及其基本单元的认定及表示方法仍存在误解,导致在化学分析计算中将产生偏差,甚至影响化学试验分析结果的准确性。因此,正确理解和选取物质的量浓度及基本单元对于从事化学试验分析及相关从业人员而言是至关重要的。 展开更多
关键词 化学试验分析 物质的量浓度 基本单元
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化学免疫分析结核γ-干扰素释放试验在肺结核诊断中的价值探究
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作者 李亮 季秀成 孙素娥 《系统医学》 2024年第11期36-38,共3页
目的 分析化学免疫分析结核γ-干扰素释放试验在肺结核诊断中应用的价值。方法 选取2020年1月—2023年4月江苏省淮安市楚州中医院接受检查的109例疑似肺结核患者作为研究对象,全部研究对象均行结核菌素皮肤试验和化学免疫分析结核γ-干... 目的 分析化学免疫分析结核γ-干扰素释放试验在肺结核诊断中应用的价值。方法 选取2020年1月—2023年4月江苏省淮安市楚州中医院接受检查的109例疑似肺结核患者作为研究对象,全部研究对象均行结核菌素皮肤试验和化学免疫分析结核γ-干扰素释放试验,将抗酸染色试验的结果为金标准,比较两种检测方式在肺结核诊断中的应用结果及诊断效能。结果 结核γ-干扰素释放试验在肺结核诊断中真阳性例数多于结核菌素皮肤试验。化学免疫分析结核γ-干扰素释放试验的灵敏度(94.74%)和准确度(93.58%)高于结核菌素皮肤试验的84.21%、81.65%,差异有统计学意义(χ^(2)=5.588,7.144,P均<0.05)。结论 在肺结核疾病诊断中,应用化学免疫分析结核γ-干扰素释放试验具有较高价值,诊断结果与金标准较为接近,诊断效能较高。 展开更多
关键词 化学免疫分析结核γ-干扰素释放试验 肺结核 诊断 结核菌素皮肤试验 抗酸染色试验
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化学发光免疫分析试验在血液筛查中的应用及评价 被引量:16
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作者 林树波 郑泽旋 张锐 《中国实验血液学杂志》 CAS CSCD 北大核心 2019年第2期569-572,共4页
目的:探讨基于化学发光的免疫分析试验在血液筛查中的应用及效果评价。方法:对3 530例无偿献血者标本应用ELISA法和CLIA法试剂分别筛查HBsAg、抗-HCV、抗-HIV和TP,然后对HBsAg、抗-HCV和抗-HIV ELISA法阴性全部标本和ELISA+/CLIA-标本... 目的:探讨基于化学发光的免疫分析试验在血液筛查中的应用及效果评价。方法:对3 530例无偿献血者标本应用ELISA法和CLIA法试剂分别筛查HBsAg、抗-HCV、抗-HIV和TP,然后对HBsAg、抗-HCV和抗-HIV ELISA法阴性全部标本和ELISA+/CLIA-标本再应用NAT进一步复检;对ELISA法和CLIA法TP单阳性以及双阳性标本采用TPPA法进一步确证。结果:CLIA法与NAT法检测结果的一致性较好,较ELISA法检测重复性好,灵敏度高;对于CLIA+/ELISA-标本,ELISA法存在漏检结果,特别是对于病毒载量浓度较低或处于"窗口期"的献血者容易被漏检。结论:ELISA法与CLIA法在血液筛查中具有优势互补性,可以提高血液筛查检测的灵敏度,减少漏检和缩短检测时间。在血液筛查中引入CLIA法试剂对于保证血液质量和临床输血安全具有重要意义。 展开更多
关键词 化学发光免疫分析试验 酶联免疫吸附试验 血液筛查 核酸检测技术
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碳化硅的化学分析方法试验
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作者 唐月生 郑明 《涟钢科技与管理》 2000年第3期7-8,共2页
本文对碳化硅样品的主成分游离碳和碳化硅的化学分析方法中的灼烧定量法和燃烧定量法进行了平行试验,针对我公司的具体情况确定了燃烧定量法适用于现状。
关键词 碳化硅 化学分析方法试验 脱氧剂 炼钢
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化学分析试验室称重操作过程中的质量保证
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作者 Keny.,AS 林徽 《湖北商检科技》 1996年第2期28-31,共4页
关键词 化学分析试验 称重 质量体证 商品检验
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分析化学实验教学改革总结
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作者 钟梅 彭秧 王吉德 《中国科教创新导刊》 2008年第28期36-36,共1页
在实践教学环节中,不管是教学内容,还是教学形式,教学要求都要适应时代需要。分析化学试验以学校重点课程建设为契机,本着加强基础、培养能力、提高素质、突出创新的教学改革目标。
关键词 分析化学试验 改革 总结
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献血者HIV筛查反应性标本电化学发光检测和确证结果分析 被引量:2
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作者 王全慧 于洋 +3 位作者 李浩龙 潘彤 刘军 樊晶 《中国输血杂志》 CAS 2022年第1期25-28,共4页
目的对HIV筛查反应性标本进行ECLIA和WB确证试验,比较分析ELISA(酶联免疫法)、ECLIA检测结果与确证感染的关系,为化学发光检测在血液筛查领域的应用提供数据支持。方法收集2019年2~10月本实验室检测的HIV筛查反应性标本177份,ELISA单试... 目的对HIV筛查反应性标本进行ECLIA和WB确证试验,比较分析ELISA(酶联免疫法)、ECLIA检测结果与确证感染的关系,为化学发光检测在血液筛查领域的应用提供数据支持。方法收集2019年2~10月本实验室检测的HIV筛查反应性标本177份,ELISA单试剂反应性137份;双试剂反应性39份;窗口期标本1份;所有项目均为阴性标本10份,总计187份进行ECLIA检测;HIV筛查反应性标本送CDC(疾病预防控制中心)进行确证试验,并对检测结果分析比较。结果177份标本中ECLIA反应性66份,阴性111份,10份阴性标本全部检测为阴性。检测指标比较分析:ECLIA检测的灵敏度97.1%,特异度81.1%,阳性预期值55%,阴性预期值99.1%,总符合率84.2%。除灵敏度相同外均大于2种ELSIA试剂。阳性预期值、特异度分别进行χ;检验,ECLIA与试剂2比较有差异(P<0.05)。ECLIA与确证结果显著相关,Kappa检验2者一致性良好。检测准确度分析:3种试剂ECLIA准确度最高、Youden指数最大。结论ECLIA具有较高的检测灵敏度,能提高早期感染标本的检出能力,缩短HIV检测的窗口期;准确度、特异性均优于ELISA试剂。ECLIA可在血液筛查中加以推广充分发挥其优势。 展开更多
关键词 化学发光免疫分析试验(ECLIA) 血液筛查 确证结果 窗口期
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煤化工厂分析化验筹建过程中应考虑的因素分析
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作者 刘蓓 王光辉 《化工管理》 2016年第29期92-,共1页
在煤化工厂分析化验室的筹建过程中,本文对煤化工厂分析化验室的设计要求、设施配置、仪器配置、人员配置以及信息管理等方面的要素进行了具体分析,希望能够以此保证煤化工厂分析化验室筹建的顺利进行。
关键词 煤化工厂 分析化学试验 筹建
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Sex Pheromone Components of the Female Black Cutworm Moth in China: Identification and Field Trials 被引量:5
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作者 向玉勇 杨茂发 李子忠 《Zoological Research》 CAS CSCD 北大核心 2009年第1期59-64,共6页
The sex pheromone blend of a China strain of the black cutworm moth Agrotis ypsilon (Rottemberg) (Lepidoptera: Noctuidae) was investigated. Chemical analysis of pheromone gland extracts of 3-day-old females showe... The sex pheromone blend of a China strain of the black cutworm moth Agrotis ypsilon (Rottemberg) (Lepidoptera: Noctuidae) was investigated. Chemical analysis of pheromone gland extracts of 3-day-old females showed that individual isolated glands contained only very small amounts of pheromone. The high-resolution gas chromatography combined with mass spectrometry (GC-MS) analysis showed the presence of Cis-7-dodecenyl acetate (Z7-12:Ac, A), Cis-9-tetradecenyl acetate (Z9-14:Ac, B), Cis- 11-hexadecenyl acetate (Z 11 - 16 :Ac, C), Cis-8-dodecenyl acetate (Z8-12:Ac, E) and Cis-5-decenyl acetate (Z5-10:Ac, D) in biologically active pheromone gland extracts. An extract of one gland from a day 3 female gave the following values for the gland components: 0.245±0.098ng for Z7-12:Ac, 0.080±0.031ng for Z9-14:Ac, 0.089±0.033ng for Z11-16:Ac, 0.085±0.031ng for Z5-10:Ac, 0.105±0.065ng for Z8-12:Ac per female. The percentages of Z7-12:Ac, Z9-14:Ac, Z11-16:Ac, Z5-10:Ac and ZS-12:Ac in pheromone gland extracts from individual females were (meaniSE) 40.451±13.66, 13.176±5.279, 14.943±5.142, 14.392±6.10 and 17.225±9.792 respectively, and the percentages of Z7-12:Ac, Z9-14:Ac and Z11-16:Ac were 58.75±9.429, 18.91±7.539 and 22.34±7.209. Field trials indicated that each single component of sex pheromone was non-effective and captured no males. The lures baited with duality compound of AB (3 : 1) had a certain attraction to males, the mean captured number was 2.6. The attraction ability of the lures baited with ternary compound of ABC (3 : 1 :1) to males added significantly, the mean captured number per trap was 7.40, which was 2.8 times of duality compound of AB (3 : 1). The contents of sex pheromone could obviously affect its capture ability to males, the mean captured number was the highest at the dosage of 200 μg. 展开更多
关键词 Agrotis ypsilon Chemical analysis Field trial Gas chromatography/High-resolution mass spectrometry Internal standard Sex pheromone Standard chemicals
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Grave's病患者血清中IFN-γ、TNF-α和IL-6的变化 被引量:2
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作者 梁驰 何凤屏 +2 位作者 曾建业 潘革 宋艳芳 《广西医学》 CAS 2008年第8期1146-1148,共3页
目的研究细胞因子在Grave's病发病机制的作用。方法Grave's病未治疗组、临床缓解组各40例,健康体检者39例,用酶联免疫试验法测定血清中IL-6、TNF-α和IFN-γ的水平,用化学发光免疫分析法测定各组的FT3、FT4和TSH的水平。结果Gra... 目的研究细胞因子在Grave's病发病机制的作用。方法Grave's病未治疗组、临床缓解组各40例,健康体检者39例,用酶联免疫试验法测定血清中IL-6、TNF-α和IFN-γ的水平,用化学发光免疫分析法测定各组的FT3、FT4和TSH的水平。结果Grave's病未治疗组患者血清中TNF-α、IFN-γ和IL-6的水平均明显高于健康对照组(P<0.01)。缓解组患者血清中TNF-a、IFN-γ的水平与未治疗组的相比降低均不明显(P>0.05),且均明显高于对照组(P<0.01);缓解组患者血清中IL-6的水平与未治疗组的相比明显降低(P<0.01),且与对照组相比无明显变化(P>0.05)。结论Grave's病患者血清TNF-α、IFN-γ和IL-6发生变化,这些因子可能共同参与Grave's病的发病过程,但是TNF-α、IFN-γ和IL-6的水平不能很好地反映Grave's病病情的严重程度。 展开更多
关键词 Grave's病 白细胞介素-6 干扰素-Γ 肿瘤坏死因子-α 酶联免疫试验 化学发光免疫分析
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HBsAg弱阳性标本4种检测方法敏感性的比较 被引量:3
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作者 谷娅楠 程艳杰 +1 位作者 朱鸿 曹华军 《医学与哲学(B)》 2013年第8期31-33,共3页
比较电化学发光免疫分析(ECLIA)、酶联免疫吸附试验(ELISA)、胶体金免疫层析技术(GICA)、HBsAg确认试验4种方法检测HBsAg弱阳性标本的检出率;探讨ELISA法不同孵育时间条件下,HBsAg弱阳性标本的检出率,为临床工作中降低HBsAg弱阳性标本... 比较电化学发光免疫分析(ECLIA)、酶联免疫吸附试验(ELISA)、胶体金免疫层析技术(GICA)、HBsAg确认试验4种方法检测HBsAg弱阳性标本的检出率;探讨ELISA法不同孵育时间条件下,HBsAg弱阳性标本的检出率,为临床工作中降低HBsAg弱阳性标本的漏检提供参考。用上述4种方法平行检测HBsAg弱阳性血清68份(ECLIA法结果1.0<吸光度/临界值(S/CO)<20.0);ELISA法分别设立孵育时间为30min、45min、60min三个组别。对检出率进行统计学比较。结果显示,ECLIA法阳性率100%,ELISA法阳性率83.82%,GICA法阳性率7.35%,HBsAg确认试验阳性率79.41%。ELISA法孵育60min的检出率高于孵育30min和45min,但检出率的差异无统计学意义。因此,为降低弱阳性标本的漏检,可以采用灵敏性高的ECLIA方法;若采用ELISA方法检测HBsAg,建议按照说明书要求,孵育60min。 展开更多
关键词 化学发光免疫分析 酶联免疫吸附试验 胶体金免疫层析技术 HBsAg确认试验 乙型肝炎病毒表面抗原
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化验室废液的处理与某些试剂的回收 被引量:6
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作者 夏芳 《化工环保》 CAS CSCD 北大核心 2003年第3期180-181,共2页
关键词 化验室废液 废液处理 试剂 回收 分析化学试验
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Indoor Particle Contamination in Airlaid Papermaking Workshop
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作者 刘俊杰 王萌 裴晶晶 《Transactions of Tianjin University》 EI CAS 2006年第4期277-280,共4页
An onsite testing based on eight-site air sampling was carried out in an airlaid papermaking workshop in Tianjin, China. By theoretical calculation, super absorbent polymer (SAP) size and its existent state in indoo... An onsite testing based on eight-site air sampling was carried out in an airlaid papermaking workshop in Tianjin, China. By theoretical calculation, super absorbent polymer (SAP) size and its existent state in indoor static airflow were obtained. SAP content in the sampled air was tested through chemical analysis method and found to be 3.0-7.2 times that of the human health limit in production areas. The concentrations of total suspending particles (TSP) and respirable particles were achieved by weighing. Particles of the most concern differ for varied function areas. Particles smaller than 10μm are mostly produced in the main production process, and 73%-90% particles generated in packing areas are larger than 10μm. SAP raw material particles can easily changed to suspending form by inevitable extrusion and frication. Correlation between respirable particles and TSP agrees well with that in atmospheric environment. 展开更多
关键词 industrial pollution PAPERMAKING TESTING PARTICLES chemical analysis
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Similar fecal immunochemical test results in screening and referral colorectal cancer
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作者 Sietze T van Turenhout Leo GM van Rossum +10 位作者 Frank A Oort Robert JF Laheij Anne F van Rijn Jochim S Terhaar sive Droste Paul Fockens René WM van der Hulst Anneke A Bouman Jan BMJ Jansen Gerrit A Meijer Evelien Dekker Chris JJ Mulder 《World Journal of Gastroenterology》 SCIE CAS CSCD 2012年第38期5397-5403,共7页
AIM: To improve the interpretation of fecal immunochemical test (FIT) results in colorectal cancer (CRC) cases from screening and referral cohorts. METHODS: In this comparative observational study, two prospective coh... AIM: To improve the interpretation of fecal immunochemical test (FIT) results in colorectal cancer (CRC) cases from screening and referral cohorts. METHODS: In this comparative observational study, two prospective cohorts of CRC cases were compared. The first cohort was obtained from 10 322 average risk subjects invited for CRC screening with FIT, of which, only subjects with a positive FIT were referred for colonoscopy. The second cohort was obtained from 3637 subjects scheduled for elective colonoscopy with a positive FIT result. The same FIT and positivity threshold (OC sensor; ≥ 50 ng/mL) was used in both cohorts. Colonoscopy was performed in all referral subjects and in FIT positive screening subjects. All CRC cases were selected from both cohorts. Outcome measurements were mean FIT results and FIT scores per tissue tumor stage (T stage). RESULTS: One hundred and eighteen patients with CRC were included in the present study: 28 cases obtained from the screening cohort (64% male; mean age 65 years, SD 6.5) and 90 cases obtained from the referral cohort (58% male; mean age 69 years, SD 9.8). The mean FIT results found were higher in the referral cohort (829 ± 302 ng/mLvs 613 ± 368 ng/mL,P = 0.02). Tissue tumor stage (T stage) distribution was dif-ferent between both populations [screening population: 13 (46%) T1, eight (29%) T2, six (21%) T3, one (4%) T4 carcinoma; referral population: 12 (13%) T1, 22 (24%) T2, 52 (58%) T3, four (4%) T4 carcinoma], and higher T stage was significantly associated with higher FIT results (P < 0.001). Per tumor stage, no significant difference in mean FIT results was observed (screening vs referral: T1 498 ± 382 ng/mL vs 725 ± 374 ng/mL, P = 0.22; T2 787 ± 303 ng/mL vs 794 ± 341 ng/mL, P = 0.79; T3 563 ± 368 ng/mLvs 870 ± 258 ng/mL,P = 0.13; T4 not available). After correction for T stage in logistic regression analysis, no significant differences in mean FIT results were observed between both types of cohorts (P = 0.10). CONCLUSION: Differences in T stage distribution largely explain differences in FIT results between screening and referral cohorts. Therefore, FIT results should be reported according to T stage. 展开更多
关键词 Screening population Referral cohort Fecal immunochemical test Tumor stage distribution Colorectal cancer
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Study on Using Mixed Fuel of Jet Fuel/Gasoline as Fuel of Gasoline Engine
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作者 L.L. Ren B. Su J. Qu 《Journal of Energy and Power Engineering》 2011年第4期300-307,共8页
This paper has integrated various methods such as laboratory physical and chemical analysis, engine bench test and actual road test, etc. to conduct a feasibility study on the emergency alternative fuel of gasoline by... This paper has integrated various methods such as laboratory physical and chemical analysis, engine bench test and actual road test, etc. to conduct a feasibility study on the emergency alternative fuel of gasoline by mixed jet fuel and gasoline. The study shows that both the evaporability and anti-knock quality decrease after mixing jet fuel with gasoline. While the mixing proportion increases, the engine power decreases and the fuel consumption increases gradually. When the proportion reaches 40%, the engine power drops by 5.3% to 11.7%, the fuel consumption rises by an average of 3.8%, and meantime the oil dilution and emission of the engine power become worse. Therefore, as for the gasoline engine, the mixed oil can only be used as emergency alternative fuel due to its harm to the engine. 展开更多
关键词 Auto gasoline jet fuel EMERGENCY SUBSTITUTE engine.
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Durum Wheat Bread: Old Sicilian Varieties and Improved Ones
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作者 G. Gallo M. Lo Bianco R. Bognanni G. Saimbene A. Orlando O. Grillo R. Saccone G. Venora 《Journal of Agricultural Science and Technology》 2010年第4期10-17,共8页
In Mediterranean countries and particularly in Southern Italy, durum wheat (Triticum durum Desf.) is traditionally used for bread production. Market globalization has created, also in these regions, the spread of br... In Mediterranean countries and particularly in Southern Italy, durum wheat (Triticum durum Desf.) is traditionally used for bread production. Market globalization has created, also in these regions, the spread of bread made with soft wheat flour (Triticum aestivum L.) standardizing this product flattening consumers' taste. With the aim of re-evaluating the old Sicilian local varieties, some landraces, chosen from the genebank of the institute, have been multiplied on farmers' fields to have enough material for making bread and for comparing this product with bread made by improved new varieties. Before milling in the pilot plant, the different wheats were characterized for their merceological indexes. The semolina obtained was analyzed for its chemical parameters. Rheological tests were conducted on dough and, finally, using standardized methods, one-variety breads were produced. On the bread slices, computerized image analysis was performed to measure colour and morphological parameters of crumb and crust. Sensory analysis, achieved through a descriptive profiling test, was conducted with trained judges using touch, fragrance and taste attributes for the different bread types. The different merceological, chemical and theological properties of raw material, grain and semolina were reflected in the breads prepared using old or improved varieties. Finally, the data obtained pointed out that the bread prepared with old and improved varieties can be clearly distinguished both by objective morphological parameters (image analysis) and by sensorial evaluations, for a potential traceability of typical product. 展开更多
关键词 Durum wheat (Triticum durum Desf.) old and improved varieties biodiversity BREAD image analysis sensory evaluation
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