Semi-solid squeeze casting(SSSC) and liquid squeeze casting(LSC) processes were used to fabricate a ZL104 connecting rod, and the influences of the process parameters on the microstructures and mechanical properti...Semi-solid squeeze casting(SSSC) and liquid squeeze casting(LSC) processes were used to fabricate a ZL104 connecting rod, and the influences of the process parameters on the microstructures and mechanical properties were investigated. Results showed that the tensile strength and elongation of the SSSC-fabricated rod were improved by 22% and 17%, respectively, compared with those of the LSC-fabricated rod. For SSSC, the average particle size(APS) and the shape factor(SF) increased with the increase of re-melting temperature(Tr), whereas the tensile strength and elongation increased first and then decreased. The APS increased with increasing the mold temperature(Tm), whereas the SF increased initially and then decreased, which caused the tensile strength and elongation to increase initially and then decrease. The APS decreased and the SF increased as squeezing pressure(ps) increased, and the mechanical properties were enhanced. Moreover, the optimal Tr, ps and Tm are 848 K, 100 MPa and 523 K, respectively.展开更多
Near-liquidus cast ingot was reheated to semi-solid firstly, and then a bracket of motor was prepared by die casting the semi-solid ingot into mould. The microstructural characteristics of AZ91D alloy in these process...Near-liquidus cast ingot was reheated to semi-solid firstly, and then a bracket of motor was prepared by die casting the semi-solid ingot into mould. The microstructural characteristics of AZ91D alloy in these processes were investigated. In the process of near-liquidus casting, primary α-Mg grains tend to be rosette-like because of the increase of plentiful quasi-solid atom clusters in molten alloy with the decrease of pouring temperature. These rosette-like a-Mg grains in ingots fabricated by near-liquidus casting are fused off and refined into near-globular structure owing to the solute diffusion mechanism and the minimum surface energy mechanism during reheating. After semi-solid die-casting, a-Mg grains, located in biscuit, impact and connect with each other; α-Mg grains, located in inner gate, congregate together; while α-Mg grains, located in component, distribute uniformly and become into globularity or strip. Because the inner gate limits the flowing of semi-solid slurry, and the pressure acted on the semi-solid slurry decreases gradually along the filling direction of semi-solid slurry in Cavity, microstructural segregation of unmelted a-Mg grains appears along this direction. Shrinkage holes in casting are caused by two different reasons. For biscuit, the shrinkage holes are caused by the blocked access of feeding liquid to the shrinkage zone for the agglomerated unmelted α-Mg grains. For component, the shrinkage holes are caused by the lack of feeding of liquid alloy.展开更多
A new Mg-14Al-0.5Mn alloy that exhibits a wide solidification range and sufficient fluidity for semi-solid forming was designed. And the rnicrostructure evolution of semi-solid Mg-14Al-0.5Mn alloy during isothermal he...A new Mg-14Al-0.5Mn alloy that exhibits a wide solidification range and sufficient fluidity for semi-solid forming was designed. And the rnicrostructure evolution of semi-solid Mg-14Al-0.5Mn alloy during isothermal heat treatment was investigated. The mechanism of the microstructure evolution and the processing conditions for isothermal heat treatment were also discussed. The results show that the microstructures of cast alloys consist of α-Mg,β-Mg17Al12 and a small amount of Al-Mn compounds. After holding at 520 ℃ for 3 min, the phases of β-Mg17Al12 and eutectic mixtures in the Mg-14Al-0.5Mn alloy melt and the microstructures of α-Mg change from developed dendrites to irregular solid particles. With increasing the isothermal time, the amount of liquid increases, and the solid particles grow large and become spherical. When the holding time lasts for 20 min or even longer, the solid and liquid phases achieve a state of dynamic equilibrium.展开更多
Cooling slope casting has been applied to aluminium casting alloys for producing ingots with non-dendritic microstructure.Semi-solid forming of the AA7075 was studied via cooling slope casting,reheating and thixoforgi...Cooling slope casting has been applied to aluminium casting alloys for producing ingots with non-dendritic microstructure.Semi-solid forming of the AA7075 was studied via cooling slope casting,reheating and thixoforging processes in order to determine the effect of semi-solid casting on the microstructure of the alloy.AA7075 ingots with non-dendritic microstructure were produced with cooling slope pouring.Castings were characterized by light microscopy,image analysis,scanning electron microscopy and EDS analysis.The resulting structures are promising in terms of grain size and sphericity.It was realized that grain coarsening may occur very suddenly in the reheating process.Cooling slope castings were obtained with 30°and 60°inclination angles,and in comparison,60°castings showed better results.Moreover,by using short reheating periods,semi-solid forging causes trace formation in the solid grains.展开更多
Tensile fracture behaviors of thixocast, artificially aged thixocast (thixocast+T6) and as-extruded AA7075 alloys were investigated. The microstructural and fractographic observations were carried out using optical...Tensile fracture behaviors of thixocast, artificially aged thixocast (thixocast+T6) and as-extruded AA7075 alloys were investigated. The microstructural and fractographic observations were carried out using optical microscope (OM) and scanning electron microscope (SEM). Experimental studies showed that as-extruded and thixocast+T6 specimens exhibited considerably more excellent mechanical properties than as-thixocast AA7075 specimen. T6 artificial heat treatment with prolonged solution treatment significantly improved the tensile properties of the thixocast AA7075 alloy. The tensile properties of as-extruded and thixocast+T6 specimens were close to each other. In as-thixocast specimen having remarkable micro-cracks, fracture was intergranular brittle type. The ductile fracture surfaces were observed in as-extruded and thixocast+T6 specimens. In as-thixocast specimens, decohesion started between the eutectic-matrix interfaces and propagated through grains. Micro-void coalescence was the dominant form of fracture in thixocast+T6 heat treated specimens. The micro-voids nucleation was initiated at the interface between the matrix and multinary eutectic structure.展开更多
The semi-solid antiburning AZ61-1.0%Y magnesium alloy slurry with fine circular solid phase was fabricated by a novel type continuous mechanical stirring in this work.The microstructure of the semisolid slurry was cha...The semi-solid antiburning AZ61-1.0%Y magnesium alloy slurry with fine circular solid phase was fabricated by a novel type continuous mechanical stirring in this work.The microstructure of the semisolid slurry was characterized by a metallography microscope.The results show that the fine circular solid phase distributes uniformly in the slurry when the stirring temperature ranges from 600 to 605℃.With the increase of the stirring velocity,the size of the solid phase becomes smaller and smaller.With the increase of the stirring time,the size of solid phase gets finer,but if the stirring time is longer than the critical time,it will be coarsened abnormally.The mechanical properties of semi-solid AZ61-1.0%Y alloy are superior to those of the normally casting magnesium alloy.展开更多
基金Project(51335009)supported by the National Natural Science Foundation of ChinaProject(2014JQ7273)supported by the Natural Science Foundation of Shaanxi Province of ChinaProject(CXY1514(1))supported by the Xi’an Science and Technology Plan Projects,China
文摘Semi-solid squeeze casting(SSSC) and liquid squeeze casting(LSC) processes were used to fabricate a ZL104 connecting rod, and the influences of the process parameters on the microstructures and mechanical properties were investigated. Results showed that the tensile strength and elongation of the SSSC-fabricated rod were improved by 22% and 17%, respectively, compared with those of the LSC-fabricated rod. For SSSC, the average particle size(APS) and the shape factor(SF) increased with the increase of re-melting temperature(Tr), whereas the tensile strength and elongation increased first and then decreased. The APS increased with increasing the mold temperature(Tm), whereas the SF increased initially and then decreased, which caused the tensile strength and elongation to increase initially and then decrease. The APS decreased and the SF increased as squeezing pressure(ps) increased, and the mechanical properties were enhanced. Moreover, the optimal Tr, ps and Tm are 848 K, 100 MPa and 523 K, respectively.
基金Project(2008BB4177) supported by the Natural Science Foundation of Chongqing City, China
文摘Near-liquidus cast ingot was reheated to semi-solid firstly, and then a bracket of motor was prepared by die casting the semi-solid ingot into mould. The microstructural characteristics of AZ91D alloy in these processes were investigated. In the process of near-liquidus casting, primary α-Mg grains tend to be rosette-like because of the increase of plentiful quasi-solid atom clusters in molten alloy with the decrease of pouring temperature. These rosette-like a-Mg grains in ingots fabricated by near-liquidus casting are fused off and refined into near-globular structure owing to the solute diffusion mechanism and the minimum surface energy mechanism during reheating. After semi-solid die-casting, a-Mg grains, located in biscuit, impact and connect with each other; α-Mg grains, located in inner gate, congregate together; while α-Mg grains, located in component, distribute uniformly and become into globularity or strip. Because the inner gate limits the flowing of semi-solid slurry, and the pressure acted on the semi-solid slurry decreases gradually along the filling direction of semi-solid slurry in Cavity, microstructural segregation of unmelted a-Mg grains appears along this direction. Shrinkage holes in casting are caused by two different reasons. For biscuit, the shrinkage holes are caused by the blocked access of feeding liquid to the shrinkage zone for the agglomerated unmelted α-Mg grains. For component, the shrinkage holes are caused by the lack of feeding of liquid alloy.
基金Projects(2006BA104B04-1,2006BAE04B07-3)supported by the National Science and Technology Supporting Program of ChinaProject(2007KZ05)supported by the Science and Technology Supporting Project of Changchun City,China+1 种基金Project(2008)supported by the Open Subject of State Key Laboratory of Rare Earth Resource Utilization,ChinaProject supported by the"985 Project"of Jilin University,China
文摘A new Mg-14Al-0.5Mn alloy that exhibits a wide solidification range and sufficient fluidity for semi-solid forming was designed. And the rnicrostructure evolution of semi-solid Mg-14Al-0.5Mn alloy during isothermal heat treatment was investigated. The mechanism of the microstructure evolution and the processing conditions for isothermal heat treatment were also discussed. The results show that the microstructures of cast alloys consist of α-Mg,β-Mg17Al12 and a small amount of Al-Mn compounds. After holding at 520 ℃ for 3 min, the phases of β-Mg17Al12 and eutectic mixtures in the Mg-14Al-0.5Mn alloy melt and the microstructures of α-Mg change from developed dendrites to irregular solid particles. With increasing the isothermal time, the amount of liquid increases, and the solid particles grow large and become spherical. When the holding time lasts for 20 min or even longer, the solid and liquid phases achieve a state of dynamic equilibrium.
文摘Cooling slope casting has been applied to aluminium casting alloys for producing ingots with non-dendritic microstructure.Semi-solid forming of the AA7075 was studied via cooling slope casting,reheating and thixoforging processes in order to determine the effect of semi-solid casting on the microstructure of the alloy.AA7075 ingots with non-dendritic microstructure were produced with cooling slope pouring.Castings were characterized by light microscopy,image analysis,scanning electron microscopy and EDS analysis.The resulting structures are promising in terms of grain size and sphericity.It was realized that grain coarsening may occur very suddenly in the reheating process.Cooling slope castings were obtained with 30°and 60°inclination angles,and in comparison,60°castings showed better results.Moreover,by using short reheating periods,semi-solid forging causes trace formation in the solid grains.
基金the financial supports of the State Planning Organization of Turkey (DPT Project Number: 2003K120470-27)Gazi University Scientific Research Fund (GUBAP Project Number: 07/2013-01)
文摘Tensile fracture behaviors of thixocast, artificially aged thixocast (thixocast+T6) and as-extruded AA7075 alloys were investigated. The microstructural and fractographic observations were carried out using optical microscope (OM) and scanning electron microscope (SEM). Experimental studies showed that as-extruded and thixocast+T6 specimens exhibited considerably more excellent mechanical properties than as-thixocast AA7075 specimen. T6 artificial heat treatment with prolonged solution treatment significantly improved the tensile properties of the thixocast AA7075 alloy. The tensile properties of as-extruded and thixocast+T6 specimens were close to each other. In as-thixocast specimen having remarkable micro-cracks, fracture was intergranular brittle type. The ductile fracture surfaces were observed in as-extruded and thixocast+T6 specimens. In as-thixocast specimens, decohesion started between the eutectic-matrix interfaces and propagated through grains. Micro-void coalescence was the dominant form of fracture in thixocast+T6 heat treated specimens. The micro-voids nucleation was initiated at the interface between the matrix and multinary eutectic structure.
基金Project(50765005)supported by the National Natural Science Foundation of China
文摘The semi-solid antiburning AZ61-1.0%Y magnesium alloy slurry with fine circular solid phase was fabricated by a novel type continuous mechanical stirring in this work.The microstructure of the semisolid slurry was characterized by a metallography microscope.The results show that the fine circular solid phase distributes uniformly in the slurry when the stirring temperature ranges from 600 to 605℃.With the increase of the stirring velocity,the size of the solid phase becomes smaller and smaller.With the increase of the stirring time,the size of solid phase gets finer,but if the stirring time is longer than the critical time,it will be coarsened abnormally.The mechanical properties of semi-solid AZ61-1.0%Y alloy are superior to those of the normally casting magnesium alloy.