For the test of rotation speed of high spinning projectile, the general formula of the motional electromotive force （MEMF） of planar magnetic induction coil （PMIC） is derived in case of 3D rotation in a stable mag...For the test of rotation speed of high spinning projectile, the general formula of the motional electromotive force （MEMF） of planar magnetic induction coil （PMIC） is derived in case of 3D rotation in a stable magnetic field. Under a reasona-ble assumption, the MEMF of PMIC is simplified after the aforementioned general formula is used to calculate high spinning PMIC in the geomagnetic field environment. The determination approach of half-cycle is discussed and the method of rotation speed test is studied, and a test is conducted in the paper. The rotation speed curve obtained by the approach in this paper is consistent with the curve by telemetry.展开更多
A simple and sensitive high performance liquid chromatography-chemical vapour generation-atom fluorescent spectrometry （HPLC-CVG-AFS） method was developed and validated for simultaneous determination mercury species...A simple and sensitive high performance liquid chromatography-chemical vapour generation-atom fluorescent spectrometry （HPLC-CVG-AFS） method was developed and validated for simultaneous determination mercury species in Su-He-Xiang-Wan （SHXW） and in tissues of rats, respectively. The species of mercury were separated by a Venusil MP-C 18 （5μm, 150 mm×4.6 ram） column with the optimized mobile phase containing 5% （w/v） acetonitrile, 0.01 mol/L L-cysteine and 0.06 moL/L ammonium acetate. The tissues of rats were freeze-dried after giving the medicine for 10 d, and then added into the solution containing 10% （w/v） HC1, 1% （w/v） sulfocarbamide and 0.15% （w/v） KC1 for increasing extraction rate. The resolutions of Hg2＋, MeHg and EtHg were 1.5 and 2.9, respectively. The detection limits of Hg2＋, MeHg and EtHg were 2.0, 1.0 and 0.9 ng/mL, respectively. The relative standard deviation （RSD） of inter- and intra-day precisions ranged from 1.56% to 2.86%. The recovery rates of three different adding level were 87%-101% （n=6）, and the RSDs were smaller than 8.2%. The results show that no MeHg and EtHg were detected in rat tissues. Only soluble mercury （Hg2＋） was determined for the mercury species of SHXW in rat tissues.展开更多
基金National Key Lab for Electronic Measurement and Technology,North University of China(No.9140C120401080C12)
文摘For the test of rotation speed of high spinning projectile, the general formula of the motional electromotive force （MEMF） of planar magnetic induction coil （PMIC） is derived in case of 3D rotation in a stable magnetic field. Under a reasona-ble assumption, the MEMF of PMIC is simplified after the aforementioned general formula is used to calculate high spinning PMIC in the geomagnetic field environment. The determination approach of half-cycle is discussed and the method of rotation speed test is studied, and a test is conducted in the paper. The rotation speed curve obtained by the approach in this paper is consistent with the curve by telemetry.
基金Projects(20875104, 21075138) supported by the National Natural Science Foundation of China
文摘A simple and sensitive high performance liquid chromatography-chemical vapour generation-atom fluorescent spectrometry （HPLC-CVG-AFS） method was developed and validated for simultaneous determination mercury species in Su-He-Xiang-Wan （SHXW） and in tissues of rats, respectively. The species of mercury were separated by a Venusil MP-C 18 （5μm, 150 mm×4.6 ram） column with the optimized mobile phase containing 5% （w/v） acetonitrile, 0.01 mol/L L-cysteine and 0.06 moL/L ammonium acetate. The tissues of rats were freeze-dried after giving the medicine for 10 d, and then added into the solution containing 10% （w/v） HC1, 1% （w/v） sulfocarbamide and 0.15% （w/v） KC1 for increasing extraction rate. The resolutions of Hg2＋, MeHg and EtHg were 1.5 and 2.9, respectively. The detection limits of Hg2＋, MeHg and EtHg were 2.0, 1.0 and 0.9 ng/mL, respectively. The relative standard deviation （RSD） of inter- and intra-day precisions ranged from 1.56% to 2.86%. The recovery rates of three different adding level were 87%-101% （n=6）, and the RSDs were smaller than 8.2%. The results show that no MeHg and EtHg were detected in rat tissues. Only soluble mercury （Hg2＋） was determined for the mercury species of SHXW in rat tissues.
