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基于多指标权重分析和单因素-正交实验优选前列爽颗粒醇提工艺 被引量:6
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作者 赵婷婷 何承辉 +1 位作者 谭梅娥 孙玉华 《化学与生物工程》 CAS 2020年第12期45-50,共6页
对前列爽颗粒醇提工艺进行了优化。在单因素实验的基础上,以醇提液中盐酸小檗碱、王不留行黄酮苷、毛蕊花糖苷的转移率及醇浸膏得率为评价指标,对指标权重系数计算方法进行比较分析,设计L9(34)正交实验对乙醇体积分数、料液比、提取时... 对前列爽颗粒醇提工艺进行了优化。在单因素实验的基础上,以醇提液中盐酸小檗碱、王不留行黄酮苷、毛蕊花糖苷的转移率及醇浸膏得率为评价指标,对指标权重系数计算方法进行比较分析,设计L9(34)正交实验对乙醇体积分数、料液比、提取时间等条件进行优化。结果表明,AHP-CRITIC混合加权法融合主观和客观两种方法的优点,综合评分结果更为合理、可靠;最佳醇提工艺如下:乙醇体积分数70%、料液比1∶10(g∶mL)、提取时间1.5 h、提取次数2次,在此条件下,盐酸小檗碱、王不留行黄酮苷、毛蕊花糖苷的平均转移率分别为81.57%、64.49%、88.15%,醇浸膏平均得率为39.38%,平均综合评分为97.67(RSD=1.98%,n=3)。该提取工艺重复性好、稳定可行,可用于工业化生产。 展开更多
关键词 前列爽颗粒 醇提 单因素-正交实验 多指标权重分析
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Ultrasonic-assisted extraction of pectin from chaenomeles 被引量:2
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作者 李新社 刘争艳 陆步诗 《Journal of Central South University》 SCIE EI CAS 2014年第11期4115-4120,共6页
Ultrasound was applied for the extraction of pectin from chaenomeles. The content of pectin was evaluated by carbazole colorimetric method. Based on the results of the single factor experiment and the orthogonal tests... Ultrasound was applied for the extraction of pectin from chaenomeles. The content of pectin was evaluated by carbazole colorimetric method. Based on the results of the single factor experiment and the orthogonal tests, the optimum extraction parameters are as follows: the solid-to-liquid ratio is 1:4 g/m L, the ultrasonic power is 320 W, the ultrasonic-assisted extraction temperature is 60 °C, the ultrasonic-assisted extraction time is 50 min, and p H value is 2.0. Compared with acid hydrolyze methods, the extraction time of the present technique decreases from 70 min to 50 min, and the extraction yield increases from 1.39% to 2.61%. The results show that ultrasonic-assisted extraction is time-saving and highly efficient, so it provides a new way to extract pectin from chaenomeles. 展开更多
关键词 chaenomeles pectin orthogonal experiments
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莜麦淀粉的提取工艺优化及其相关特性研究 被引量:5
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作者 王娜 肖云峰 +1 位作者 钱新宇 韩运祺 《中国粮油学报》 EI CAS CSCD 北大核心 2020年第9期47-53,共7页
确定应用脱脂碱提复合法进行莜麦淀粉提取的最佳工艺,并对其相关特性进行研究。以莜麦种子为原料,通过单因素以及正交实验确定莜麦淀粉提取的最佳工艺并对莜麦淀粉相关特性进行研究。最佳工艺为:当固液比为1∶10,摇床温度为50℃,振摇时... 确定应用脱脂碱提复合法进行莜麦淀粉提取的最佳工艺,并对其相关特性进行研究。以莜麦种子为原料,通过单因素以及正交实验确定莜麦淀粉提取的最佳工艺并对莜麦淀粉相关特性进行研究。最佳工艺为:当固液比为1∶10,摇床温度为50℃,振摇时间为2 h,测得莜麦淀粉的提取率为73.26%。在最优条件下,提取的莜麦淀粉中水分含量为7.56 g/100 g,灰分含量为0.13 g/100 g,脂肪含量为0.17 g/100 g,蛋白质残留量为0.56 g/100 g,符合国家食品安全标准;SEM和光学显微镜图像显示,莜麦淀粉颗粒较小,且粒径大小不一致,呈多角型或椭圆形,属于小颗粒淀粉;红外光谱与核磁共振分析发现,莜麦淀粉的谱图为典型的淀粉图谱。应用脱脂碱提复合法进行莜麦淀粉的提取,并对其相关特性进行研究。 展开更多
关键词 莜麦淀粉 提取工艺 因素实验-设计 物质组成 微观结构
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Study on Microcapsulation of Onion Oil with Complex Coacervation and Spray Drying Method 被引量:1
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作者 LIU Nan-nan 《Chinese Food Science》 2012年第4期4-6,8,共4页
[Objective] The aim was to study the microcapsulation of onion oil with double place separation-coacevation and spray drying. [Method] The effect of processing parameters which included the different wall material com... [Objective] The aim was to study the microcapsulation of onion oil with double place separation-coacevation and spray drying. [Method] The effect of processing parameters which included the different wall material combination,the ratio between the wall material,the core material content and the feed concentration on the efficiency and yield of microencapsulated was evaluated by single factor experiments. [Result] Through orthogonal optimization experiments, the optimum condition was as follows: the ratio of Arabic gum and maltodextrin ration was 1∶1, the core content was 25%, feed composition was 18%, and the microencapsulation efficiency and yield can reach 80.7% and 95.3% respectively. [Conclusion] The microcapsulaiton of onion oil with complex coacervation spray drying method can increase membrane thickness, improve core stability and prolong shelf life of products. 展开更多
关键词 Spray drying Onion oil flavor MICROENCAPSULATION China
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