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GAP改性单基球形药的热分解性能研究 被引量:5
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作者 吴艳光 罗运军 葛震 《北京理工大学学报》 EI CAS CSCD 北大核心 2013年第6期653-656,共4页
采用热重-微热重(TG-DTG)和差示扫描量热(DSC)实验,研究了纯单基球(NC)、聚叠氮缩水甘油醚(GAP)以及GAP改性的单基球形药的热分解性能,探索了球药中主要组分NC和GAP之间的相互作用.实验结果表明:GAP质量分数分别为20%和30%的改性单基球... 采用热重-微热重(TG-DTG)和差示扫描量热(DSC)实验,研究了纯单基球(NC)、聚叠氮缩水甘油醚(GAP)以及GAP改性的单基球形药的热分解性能,探索了球药中主要组分NC和GAP之间的相互作用.实验结果表明:GAP质量分数分别为20%和30%的改性单基球形药在发生热分解时,存在GAP的热分解过程,且其主链的热分解峰值温度较纯,GAP相应的峰值温度分别提前3.5℃和8.4℃.DSC测试显示,NC的热分解产物和热量使GAP质量分数为20%和30%的改性单基球中—N3基团的放热峰分别降低8.18℃和7.70℃,即发现在GAP改性的单基球中,NC的存在对GAP的热分解具有一定的促进作用. 展开更多
关键词 聚叠氮缩水甘油醚(GAP) 热分解 单基球 改性
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高效液相色谱法测定单基球扁药中钝感剂的含量 被引量:7
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作者 熊立斌 应三九 罗付生 《火炸药学报》 CAS CSCD 2001年第2期54-55,共2页
研究了用高效液相色谱法测定单基球扁药中的钝感剂含量。借助于紫外检测器于波长 2 2 3nm处检测了中定剂和苯二甲酸二丁酯 (DBP)的含量。
关键词 高效液相色谱 紫外检测器 中定剂 钝感剂 单基球扁药 含量 DBP 发射药 苯二甲酸二丁酯
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Preparation and characterization of monodisperse zirconia spherical nanometer powder via lamellar liquid crystal template method
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作者 何伟艳 刘进荣 +2 位作者 曹珍珠 李彩虹 高艳芳 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2015年第10期1721-1727,共7页
Cubic phase spherical zirconia nano-powder was prepared by a direct template route in the lamellar liquid crystal formed by polyoxyethylene tert-octylphenyl ether(Triton X-100)/sodium dodecyl sulfate(SDS)/H_2O.The pre... Cubic phase spherical zirconia nano-powder was prepared by a direct template route in the lamellar liquid crystal formed by polyoxyethylene tert-octylphenyl ether(Triton X-100)/sodium dodecyl sulfate(SDS)/H_2O.The precursor powder and zirconia powder were characterized by XRD,FT-IR,TG/DSC,TEM,and SEM methods.Results show that the stability of the lamellar liquid crystal is controlled by NH_3·H_2O concentration.The size of nanoparticles is greatly affected by NH_3·H_2O and ZrOCl_2·8H_2O concentrations.The zirconia nanoparticles show narrow particle size distribution of 10-30 nm. 展开更多
关键词 ZIRCONIA Spherical nanometer powder Lamellar liquid crystal template
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Brascamp-Lieb inequality for positive double John basis and its reverse 被引量:5
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作者 LI Ai-Jun LENG GangSong 《Science China Mathematics》 SCIE 2011年第2期399-410,共12页
In this paper, we establish the Brascamp-Lieb inequality for positive double John basis and its reverse. As their applications, we estimate the upper and lower bounds for the volume product of two unit balls with the ... In this paper, we establish the Brascamp-Lieb inequality for positive double John basis and its reverse. As their applications, we estimate the upper and lower bounds for the volume product of two unit balls with the given norms. Moreover, the Loomis-Whitney inequality for positive double John basis is obtained. 展开更多
关键词 Brascamp-Lieb inequality and its reverse John basis positive double John basis mass transportation ZONOTOPE
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Approximation of monogenic functions by higher order Szego kernels on the unit ball and half space 被引量:3
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作者 WANG JinXun QIAN Tao 《Science China Mathematics》 SCIE 2014年第9期1785-1797,共13页
We study the adaptive decomposition of functions in the monogenic Hardy spaces H2by higher order Szeg kernels under the framework of Clifford algebra and Clifford analysis,in the context of unit ball and half space.Th... We study the adaptive decomposition of functions in the monogenic Hardy spaces H2by higher order Szeg kernels under the framework of Clifford algebra and Clifford analysis,in the context of unit ball and half space.This is a sequel and a higher-dimensional generalization of our recent study on the complex Hardy spaces. 展开更多
关键词 monogenic Hardy space Szego kernel adaptive decomposition DICTIONARY matching pursuit
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Antimicrobial, anticancer and DNA binding studies of transition metal(Ⅱ)complexes containing 2-phenyl-4-selenazole carboxylic acid 被引量:2
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作者 GUAN QuanYin SHI Xia +1 位作者 SHEN JinBei ZHAO GuoLiang 《Science China Chemistry》 SCIE EI CAS 2013年第5期588-594,共7页
Three novel transition metal complexes [ML2(phen)]'H20 (M= Mn, Co, Zn; HL= C10H702NSe, 2-phenyl-4-selenazole carboxylic acid, phen= 1,10-phenanthroline) 1-3 were synthesized and characterized by elemental analysi... Three novel transition metal complexes [ML2(phen)]'H20 (M= Mn, Co, Zn; HL= C10H702NSe, 2-phenyl-4-selenazole carboxylic acid, phen= 1,10-phenanthroline) 1-3 were synthesized and characterized by elemental analysis, IR spectra. Their crystal structures were deterimined by single-crystal X-ray diffraction method. The antibacterial activities of the complexes against five species of bacteria, Escherichia coli (E. coli), Staphylococcus epidermidis (S. epidermidis), Staphylococcus aureus (S. au- reus), Acinetobacter baumanii (A. baumanii) and Streptococcus viridans (S. viridans), were tested respectively. The anticancer activities of the complexes against human pancreatic cancer line PANC-28 and human hepatocarcinoma line HuH7 were also studied. The interactions between the complexes and DNA were studied by ethidium bromide (EB) fluorescent probe. 展开更多
关键词 2-phenyl-4-selenazole carboxylic acid transition metal complex antibacterial activity anticancer activity DNA binding
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Approaches in extracellular matrix engineering for determination of adhesion molecule mediated single cell function
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作者 Chantal E. AYRES-SANDER Anjelica L. GONZALEZ 《Frontiers in Biology》 CAS CSCD 2013年第1期32-49,共18页
The native extracellular matrix (ECM) and the cells that comprise human tissues are together engaged in a complex relationship; cells alter the composition and structure of the ECM to regulate the material and biolo... The native extracellular matrix (ECM) and the cells that comprise human tissues are together engaged in a complex relationship; cells alter the composition and structure of the ECM to regulate the material and biologic properties of the surrounding environment while the composition and structure of the ECM modulates cellular processes that maintain healthy tissue and repair diseased tissue. This reciprocal relationship occurs via cell adhesion molecules (CAMs) such as integrins, selectins, cadherins and IgSF adhesion molecules. To study these celI-ECM interactions, researchers use two-dimensional substrates or three-dimensional matrices composed of native proteins or bioactive peptide sequences to study single cell function. While two-dimensional snbstrates provide valuable information about cell-ECM interactions, three-dimensional matrices more closely mimic the native ECM; cells cultured in three-dimensional matrices have demonstrated greater cell movement and increased integrin expression when compared to cells cultured on two-dimensional substrates. In this article we review a number of cellular processes (adhesion, motility, phagocytosis, differentiation and survival) and examine the cell adhesion molecules and ECM proteins (or bioactive peptide sequences) that mediate cell functionality. 展开更多
关键词 Extracellular matrix INTEGRINS BIOMATERIALS natural polymers peptide sequences RGD
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