以间歇碳化法制备纳米碳酸钙的工艺为基础,以压电超声波辅助合成为方法,以实现工业化生产优质的纳米碳酸钙为目的,确定了超声辐照下纳米碳酸钙的合成反应罐结构及合成装置系统的设计,并探讨了超声波辐照下工艺过程各影响因素与纳米...以间歇碳化法制备纳米碳酸钙的工艺为基础,以压电超声波辅助合成为方法,以实现工业化生产优质的纳米碳酸钙为目的,确定了超声辐照下纳米碳酸钙的合成反应罐结构及合成装置系统的设计,并探讨了超声波辐照下工艺过程各影响因素与纳米碳酸钙粒径的关系。图示了反应体系的传热、传质效果及与粒径的关系。结果表明,影响压电超声在碳化法合成纳米碳酸钙的粒径主要因素有料浆初始温度、C a(O H )2乳液浓度、C O 2的流量。在自制的装置中,制备出10~30nm 优质的纳米碳酸钙产品,为纳米碳酸钙粉料的生产提供了另种方法。展开更多
In order to realize on-line quantitative detection on SF6 and effective control of nlnning state of SF6 high voltage power supply system, a concentrated SF6 quantitative ultrasonic on-line deteetion system has been de...In order to realize on-line quantitative detection on SF6 and effective control of nlnning state of SF6 high voltage power supply system, a concentrated SF6 quantitative ultrasonic on-line deteetion system has been developed based on the actual demand of electric power system consumers. There are four major characteristics in this system. Firstly, the gas of maximum 64 detection points is transferred through the specific air path to the detection devices to he detected and analyzed, thereby the electrical lines and the complicated installation of the collectors can be avoided; secondly, the differential technique is used to shield the influence of environmental factors, which effectively improves the accuracy of the acoustic detection; thirdly, the SF6 coneentration is determined by the speed and phase in the ultrasonic wave trans- mission process, therefore there is no secondary pollution for the purely physical means; finally, the ma- ture embedded technique is applied in this system to improve its intelligence and stability.展开更多
文摘以间歇碳化法制备纳米碳酸钙的工艺为基础,以压电超声波辅助合成为方法,以实现工业化生产优质的纳米碳酸钙为目的,确定了超声辐照下纳米碳酸钙的合成反应罐结构及合成装置系统的设计,并探讨了超声波辐照下工艺过程各影响因素与纳米碳酸钙粒径的关系。图示了反应体系的传热、传质效果及与粒径的关系。结果表明,影响压电超声在碳化法合成纳米碳酸钙的粒径主要因素有料浆初始温度、C a(O H )2乳液浓度、C O 2的流量。在自制的装置中,制备出10~30nm 优质的纳米碳酸钙产品,为纳米碳酸钙粉料的生产提供了另种方法。
基金Supported by the National Natural Science Foundation of China (No. 10574038)
文摘In order to realize on-line quantitative detection on SF6 and effective control of nlnning state of SF6 high voltage power supply system, a concentrated SF6 quantitative ultrasonic on-line deteetion system has been developed based on the actual demand of electric power system consumers. There are four major characteristics in this system. Firstly, the gas of maximum 64 detection points is transferred through the specific air path to the detection devices to he detected and analyzed, thereby the electrical lines and the complicated installation of the collectors can be avoided; secondly, the differential technique is used to shield the influence of environmental factors, which effectively improves the accuracy of the acoustic detection; thirdly, the SF6 coneentration is determined by the speed and phase in the ultrasonic wave trans- mission process, therefore there is no secondary pollution for the purely physical means; finally, the ma- ture embedded technique is applied in this system to improve its intelligence and stability.