Hot compression tests were conducted on a homogenized Mg-7Gd-4Y-1Nd-0.5Zr alloy at 450 ℃ and a strain rate of 2 s-1. Dynamic recrystallization （DRX） mechanisms were investigated by optical microscope （OM）, scanni...Hot compression tests were conducted on a homogenized Mg-7Gd-4Y-1Nd-0.5Zr alloy at 450 ℃ and a strain rate of 2 s-1. Dynamic recrystallization （DRX） mechanisms were investigated by optical microscope （OM）, scanning electron microscope （SEM） and transmission electron microscope （TEM） systematically. The crystallographic orientation information is obtained through electron back-scattering diffraction （EBSD）. The result shows that the flow stress firstly reaches a peak rapidly followed by declining to a valley, and then increases gradually again when the alloy is compressed to a strain of-1.88. DRX related to {10]2} tensile twins is extensively observed at small strains, resulting in an evident grain refinement. DRX grains first nucleate along the edges of twin boundaries with about 30~ （0001） off the twin parents. While at large strains, conventional continuous DRX （CDRX） is frequently identified by the formation of small DRX grains along the original grain boundaries and the continuously increasing misorientation from the centre of large original grains to the grain boundaries. Evidence of particle-stimulated nucleation （PSN） is also observed in the present alloy.展开更多
The microstructure and texture evolutions in Mg-Zn-Er alloy during hot compression were investigated by using opticalmicroscope （OM）, field emission scanning electron microscope （EBSD） and transmission electron mi...The microstructure and texture evolutions in Mg-Zn-Er alloy during hot compression were investigated by using opticalmicroscope （OM）, field emission scanning electron microscope （EBSD） and transmission electron microscope （TEM）. The resultsindicate that the temperature plays an important role in dynamic recrystallization （DRX） mechanism. The twin dynamicrecrystallization （TDRX） is induced at a strain of 0.6 because of the activation of non-basal slip （a＋c ） dislocations at 200 ℃.Meanwhile, the continuous DRX （CDRX） occurs at 350℃, which is identified by the typical necklace-like structure around theresidual initial grains. The DRX contributes to the modification of texture significantly. The tension twins are responsible for theweak texture at 200 ℃. Meanwhile, the decrease in the basal texture is ascribed to the DRX sites which transfer from twinboundaries to initial grain boundaries as the temperature is increased from 200 to 350 ℃.展开更多
The creep anisotropy behavior under different stresses at 180℃ of hot-extruded AZ91−2Y magnesium alloy with pre-compression(PC)and without pre-compression(NPC)was studied.Microstructure,texture and mechanical propert...The creep anisotropy behavior under different stresses at 180℃ of hot-extruded AZ91−2Y magnesium alloy with pre-compression(PC)and without pre-compression(NPC)was studied.Microstructure,texture and mechanical properties of the alloy were examined by scanning electron microscopy(SEM),electron backscatter diffraction(EBSD),transmission electron microscopy(TEM)and tensile creep tests.The results revealed that the creep resistance was proportional to the volume fraction of spherical Mg_(17)Al_(12) precipitates.The dynamic precipitation of large volume fraction of lamellar Mg_(17)Al_(12) in NPC samples leads to the basaláañslip as the dominant creep mechanism,and the NPC samples have obvious anisotropy.In the PC samples,dynamic precipitation of large volume fraction of spherical Mg_(17)Al_(12) has inhibitory effect on the basaláañslip.The pyramidalác+añslip and twinning improve the creep anisotropy resistance significantly.展开更多
A Thermecmastor-Z hot deformation simulator,optical microscopy,XRD and TEM were employed to characterize the flow stress behavior and microstructure of twin roll cast ZK60 magnesium alloy during initial stage of hot c...A Thermecmastor-Z hot deformation simulator,optical microscopy,XRD and TEM were employed to characterize the flow stress behavior and microstructure of twin roll cast ZK60 magnesium alloy during initial stage of hot compression at elevated temperature of 300 ℃ and 400 ℃ and a given strain rate of 10-2s-1.The results suggest that flow stress drop during initial stage of hot compression at 300℃,generally led by dynamic recrystallization,is attributed to twinning,correspondingly to dynamic recrystallization as deformation temperature is raised to 400 ℃.展开更多
The influence of free-end torsion on compressive behavior of an extruded AZ31 rod at various temperatures was studied.Pre-torsion generates a high density of dislocations and a large number of{1012}twins in the matrix...The influence of free-end torsion on compressive behavior of an extruded AZ31 rod at various temperatures was studied.Pre-torsion generates a high density of dislocations and a large number of{1012}twins in the matrix,which can largely enhance the compressive yield strength at RT and 100℃.However,with increasing temperature,hardening effect via pre-torsion gradually decreases.When the compressive temperature reaches 300℃,pre-torsion reduces the compressive yield strength.Moreover,initial dislocations and twins via torsion help to refine the sub-structure and accelerate the continuous dynamic recrystallization during compression at 200℃.Thus,twisted sample exhibits more rapid flow softening behavior than the as-extruded sample at 200℃.When compressed at 300℃,the twins and dislocations via torsion were largely eliminated during the holding time,and the discontinuous dynamic recrystallization was enhanced.It is found that the compression curves of twisted sample and as-extruded sample tended to be coincident at 300℃.Related mechanisms were discussed in detail.展开更多
文摘Hot compression tests were conducted on a homogenized Mg-7Gd-4Y-1Nd-0.5Zr alloy at 450 ℃ and a strain rate of 2 s-1. Dynamic recrystallization （DRX） mechanisms were investigated by optical microscope （OM）, scanning electron microscope （SEM） and transmission electron microscope （TEM） systematically. The crystallographic orientation information is obtained through electron back-scattering diffraction （EBSD）. The result shows that the flow stress firstly reaches a peak rapidly followed by declining to a valley, and then increases gradually again when the alloy is compressed to a strain of-1.88. DRX related to {10]2} tensile twins is extensively observed at small strains, resulting in an evident grain refinement. DRX grains first nucleate along the edges of twin boundaries with about 30~ （0001） off the twin parents. While at large strains, conventional continuous DRX （CDRX） is frequently identified by the formation of small DRX grains along the original grain boundaries and the continuously increasing misorientation from the centre of large original grains to the grain boundaries. Evidence of particle-stimulated nucleation （PSN） is also observed in the present alloy.
基金Project(2172013)supported by the Natural Science Foundation of Beijing,ChinaProject(2016YFB0301101)supported by the National Key Research and Development Program,ChinaProject(KZ201810005005)supported by Key Science and Technology Program of Beijing Municipal Commission of Education,China
文摘The microstructure and texture evolutions in Mg-Zn-Er alloy during hot compression were investigated by using opticalmicroscope （OM）, field emission scanning electron microscope （EBSD） and transmission electron microscope （TEM）. The resultsindicate that the temperature plays an important role in dynamic recrystallization （DRX） mechanism. The twin dynamicrecrystallization （TDRX） is induced at a strain of 0.6 because of the activation of non-basal slip （a＋c ） dislocations at 200 ℃.Meanwhile, the continuous DRX （CDRX） occurs at 350℃, which is identified by the typical necklace-like structure around theresidual initial grains. The DRX contributes to the modification of texture significantly. The tension twins are responsible for theweak texture at 200 ℃. Meanwhile, the decrease in the basal texture is ascribed to the DRX sites which transfer from twinboundaries to initial grain boundaries as the temperature is increased from 200 to 350 ℃.
基金the National Natural Science Foundation of China(Nos.52075048,52171099 and 52105140)the Natural Science Foundation of Hunan Province,China(No.2021JJ40583)+2 种基金the Science and Technology Innovation Project of Hunan Province,China(No.2018RS3073)the Scientific Research Innovation Project for Graduate Student of Changsha University of Science&Technology,China(No.CX2021SS55)the Double First-class Scientific Research International Cooperation Project of Changsha University of Science and Technology,China(No.2019IC15).
文摘The creep anisotropy behavior under different stresses at 180℃ of hot-extruded AZ91−2Y magnesium alloy with pre-compression(PC)and without pre-compression(NPC)was studied.Microstructure,texture and mechanical properties of the alloy were examined by scanning electron microscopy(SEM),electron backscatter diffraction(EBSD),transmission electron microscopy(TEM)and tensile creep tests.The results revealed that the creep resistance was proportional to the volume fraction of spherical Mg_(17)Al_(12) precipitates.The dynamic precipitation of large volume fraction of lamellar Mg_(17)Al_(12) in NPC samples leads to the basaláañslip as the dominant creep mechanism,and the NPC samples have obvious anisotropy.In the PC samples,dynamic precipitation of large volume fraction of spherical Mg_(17)Al_(12) has inhibitory effect on the basaláañslip.The pyramidalác+añslip and twinning improve the creep anisotropy resistance significantly.
基金Project(10020072) supported by Brain Pool Program of Korea Government and Core Technology R & D Program for the Development of High Performance Eco-friendly Structural Materials of the Korean Ministry of Commerce, Industry and Energy
文摘A Thermecmastor-Z hot deformation simulator,optical microscopy,XRD and TEM were employed to characterize the flow stress behavior and microstructure of twin roll cast ZK60 magnesium alloy during initial stage of hot compression at elevated temperature of 300 ℃ and 400 ℃ and a given strain rate of 10-2s-1.The results suggest that flow stress drop during initial stage of hot compression at 300℃,generally led by dynamic recrystallization,is attributed to twinning,correspondingly to dynamic recrystallization as deformation temperature is raised to 400 ℃.
基金the National Natural Science Foundation of China(No.51601154)Southwest University Undergraduate Innovation Project(No.zsm2021026).
文摘The influence of free-end torsion on compressive behavior of an extruded AZ31 rod at various temperatures was studied.Pre-torsion generates a high density of dislocations and a large number of{1012}twins in the matrix,which can largely enhance the compressive yield strength at RT and 100℃.However,with increasing temperature,hardening effect via pre-torsion gradually decreases.When the compressive temperature reaches 300℃,pre-torsion reduces the compressive yield strength.Moreover,initial dislocations and twins via torsion help to refine the sub-structure and accelerate the continuous dynamic recrystallization during compression at 200℃.Thus,twisted sample exhibits more rapid flow softening behavior than the as-extruded sample at 200℃.When compressed at 300℃,the twins and dislocations via torsion were largely eliminated during the holding time,and the discontinuous dynamic recrystallization was enhanced.It is found that the compression curves of twisted sample and as-extruded sample tended to be coincident at 300℃.Related mechanisms were discussed in detail.
