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微波消解-原子吸收分光光度法测定蒲公英中重金属元素含量 被引量:9
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作者 李喜凤 邱天宝 +1 位作者 郝哲 余云辉 《时珍国医国药》 CAS CSCD 北大核心 2011年第6期1378-1379,共2页
目的测定蒲公英中重金属元素铅、镉、铜、砷、汞的含量。方法采用微波消解,以原子吸收分光光度法进行测定。结果河南不同产地蒲公英药材中铅、镉、铜、砷、汞的含量符合有关规定。结论该方法准确可靠,重复性好,可用于蒲公英中重金属元... 目的测定蒲公英中重金属元素铅、镉、铜、砷、汞的含量。方法采用微波消解,以原子吸收分光光度法进行测定。结果河南不同产地蒲公英药材中铅、镉、铜、砷、汞的含量符合有关规定。结论该方法准确可靠,重复性好,可用于蒲公英中重金属元素的含量测定,为蒲公英药材质量标准的进一步完善提供一定的科学依据。 展开更多
关键词 蒲公英 重金属 微波消解 原子吸光分光光度法
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富马酸亚铁叶酸片中铁的人体生物等效性研究 被引量:1
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作者 严晓星 姜莉苑 +5 位作者 丁黎 周娜 程露 贺彦娜 张全英 华雯妍 《药学与临床研究》 2013年第2期143-145,共3页
目的:研究富马酸亚铁叶酸片中铁在健康志愿者体内的生物利用度及生物等效性。方法:24例健康志愿者分别随机交叉口服受试制剂(富马酸亚铁叶酸片:一次2片,含富马酸亚铁304 mg×2,叶酸0.35 mg×2),参比制剂1(富马酸亚铁片:一次3片,... 目的:研究富马酸亚铁叶酸片中铁在健康志愿者体内的生物利用度及生物等效性。方法:24例健康志愿者分别随机交叉口服受试制剂(富马酸亚铁叶酸片:一次2片,含富马酸亚铁304 mg×2,叶酸0.35 mg×2),参比制剂1(富马酸亚铁片:一次3片,200 mg×3)和参比制剂2(叶酸片:一次2片,0.4 mg×2),采用原子吸光分光光度法测定血中铁的浓度。结果:健康志愿者口服受试制剂和参比制剂后,铁的Cmax分别为(1.70±0.53)μg·mL-1和(1.61±0.62)μg·mL-1;Tmax分别为(4.0±1.0)h和(4.3±1.5)h;AUC0-24 h分别为(14.4±8.5)μg·h·mL-1和(14.3±8.1)μg·h·mL-1;t1/2分别为(3.3±2.9)h和(3.2±2.3)h。Cmax、AUC0-24 h和AUC0-∞剂量校正后经双向单侧t检验和(1-2α)置信区间生物等效性评价,Tmax经非参数检验(Wilcoxon符号秩法)均无显著性差异(P>0.05)。结论:根据铁的结果判定,富马酸亚铁叶酸片和富马酸亚铁片生物等效。 展开更多
关键词 富马酸亚铁 原子吸光分光光度法 药代动力学 生物等效性
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Determination of Iron(Ⅱ), Iron(Ⅲ) and Total Iron in Some β -Thalassemia Patients Using Different Analytical Techniques
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作者 Nabil Fakhre Dashty Ali 《Journal of Environmental Science and Engineering(B)》 2013年第5期304-307,共4页
There are many well-known analytical methods for determination of iron(Ⅱ) and iron(Ⅲ). Among these methods: Gravimetric, titrimetric, potentiometric, conductometric and batch and flow-injection spectrophotometr... There are many well-known analytical methods for determination of iron(Ⅱ) and iron(Ⅲ). Among these methods: Gravimetric, titrimetric, potentiometric, conductometric and batch and flow-injection spectrophotometric methods. In present study, two batch spectrophotometric, atomic absorption spectrometric and biolabo kit methods have been used for determination of iron(Ⅱ), iron(Ⅲ) and total iron. The present methods have the advantages of high sensitivity, low cost reagent, low operation cost, simplicity, speed and their applications for determination of iron(Ⅱ) and iron(Ⅲ) in some serum samples of normal human and fl-thalasemia patients in Erbil city. For the first time especially in Erbil city attempts were made to use zero, first and second derivative spectra to identify the serum samples of some β-thallasemia patients from the normal human serum samples due to the appearance and resolution of peaks in both cases. 展开更多
关键词 Determination IRON β-thalassemia patients different analytical techniques.
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The Study on the determination method of Aluminum and its salts
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《International English Education Research》 2015年第4期52-54,共3页
This paper reviews the standard methods for the determination of the Aluminum and its salts, and makes comparative analyses from the operation conditions and its characteristics. The current national standard and the ... This paper reviews the standard methods for the determination of the Aluminum and its salts, and makes comparative analyses from the operation conditions and its characteristics. The current national standard and the industry standard methods include: the inductively coupled plasma atomic emission spectrometry, the inductively coupled plasma mass spectrometry, the atomic absorption spectrometry, the spectrophotometric method, the potential analysis and the titration analysis. 展开更多
关键词 ALUMINUM Aluminum salts determination method
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Contributions of anthropogenic and external natural forcings to climate changes over China based on CMIP5 model simulations 被引量:5
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作者 ZHAO Tian Bao LI Chun Xiang ZUO Zhi Yan 《Science China Earth Sciences》 SCIE EI CAS CSCD 2016年第3期503-517,共15页
Based on observations and historical simulations from the fifth phase of the Coupled Model Intercomparison Project(CMIP5) archive, the contributions of human activities(including greenhouse gases(GHGs), anthropogenic ... Based on observations and historical simulations from the fifth phase of the Coupled Model Intercomparison Project(CMIP5) archive, the contributions of human activities(including greenhouse gases(GHGs), anthropogenic aerosols(AAs), and land use(LU)) and external natural forcings(Nat) to climate changes in China over the past 50 years were quantified. Both anthropogenic and external natural forcings account for 95%–99% of the observed temperature change from 1951–1975 to 1981–2005. In particular, the temperature changes induced by GHGs are approximately 2–3 times stronger than the observed changes, and AAs impose a significant cooling effect. The total external forcings can explain 65%–78% of the observed precipitation changes over the past 50 years, in which AAs and GHGs are the primary external forcings leading to the precipitation changes; in particular, AAs dominate the main spatial features of precipitation changes in eastern China. Human activities also dominate the long-term non-linear trends in observed temperature during the past several decades, and, in particular, GHGs, the primary warming contributor, have produced significant warming since the 1960 s. Compared to the long-term non-linear trends in observed precipitation, GHGs have largely caused the wetting changes in the arid-semiarid region since the 1970 s, whereas AAs have led to the drying changes in the humid-semihumid region; both LU and Nat can impose certain impacts on the long-term non-linear trends in precipitation. Using the optimal fingerprinting detection approach, the effects of human activities on the temperature changes can be detected and attributed in China, and the effect of GHGs can be clearly detected from the observations in humid-semihumid areas. However, the anthropogenic effects cannot be detected in the observed precipitation changes, which may be due to the uncertainties in the model simulations and to other issues. Although some results in this paper still need improvement due to uncertainties in the coupled models, this study is expected to provide the background and scientific basis for climate changes to conduct vulnerability and risk assessments of the ecological systems and water resources in the arid-semiarid region of China. 展开更多
关键词 Human activity External natural forcings CMIP5 models Contributions Climate changes China
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