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气相顶空色谱法测定原料样6-APA中的残留溶媒 被引量:2
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作者 王英 王晓丹 《黑龙江医药》 CAS 2005年第1期27-28,共2页
目的:建立测定原料药6-APA 中残留溶媒的气相顶空色谱法。方法:选4-甲基-2-戊酮作内标物,以内标法在极性弹性石英毛细柱上进行各组分分离,效果好。柱温:120℃,进样口温度:200℃,检测器温度:250℃,结果:平均回收率:乙酸丁酯99.3%,结论:... 目的:建立测定原料药6-APA 中残留溶媒的气相顶空色谱法。方法:选4-甲基-2-戊酮作内标物,以内标法在极性弹性石英毛细柱上进行各组分分离,效果好。柱温:120℃,进样口温度:200℃,检测器温度:250℃,结果:平均回收率:乙酸丁酯99.3%,结论:该方法克服了人工控温,进样不准的缺点,重现性好,精度高。 展开更多
关键词 气相顶空色谱法 测定 原料样6-APA 残留溶媒
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海洋沉积物基质多环芳烃标准参考物质的原料样品制备研究
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作者 付丹 李娟 +3 位作者 彭模 蔡瑞 周超凡 郑江鹏 《环境监控与预警》 2022年第6期38-42,共5页
海洋沉积物基质多环芳烃(PAHs)标准参考物质是海洋环境沉积物监测分析中质量控制和质量保证的重要保障。由于缺少对相关原料样筛选研究,目前我国尚未有自主制备的海洋沉积物基质PAHs标准参考物质。通过海洋沉积物原始数据调研、定点筛... 海洋沉积物基质多环芳烃(PAHs)标准参考物质是海洋环境沉积物监测分析中质量控制和质量保证的重要保障。由于缺少对相关原料样筛选研究,目前我国尚未有自主制备的海洋沉积物基质PAHs标准参考物质。通过海洋沉积物原始数据调研、定点筛查、实验室间验证等手段,对江苏近岸海域海洋沉积物原料样进行筛选研究。结果表明,连云港赣榆某入海口点位的海洋沉积物样品∑PAHs的质量分数为413μg/kg,该样品各粒径中的PAHs质量分数分布均匀,精密度能够满足我国海洋沉积物环境监测质量控制需求,可以为进一步制备海洋沉积物PAHs标准参考物质提供技术支持。 展开更多
关键词 海洋沉积物 多环芳烃 标准参考物质 原料样
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Identification of Pathogenic Germs and Antibiotics Residues in the Raw Milk and Their Effects on Human Health
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作者 Tadjine Nacera Tassist Amina +2 位作者 Bradea Maria-Stela Tarzali Dalila Guetarni Djamel 《Journal of Life Sciences》 2011年第2期129-131,共3页
Milk is a food of great value, it provides more essential nutrient than any other natural food. The presence of pathogenic bacteria and antibiotic residues in milk can cause a real danger to consumers. Effectively, th... Milk is a food of great value, it provides more essential nutrient than any other natural food. The presence of pathogenic bacteria and antibiotic residues in milk can cause a real danger to consumers. Effectively, the milk consumption contaminated by bacteria can have an immediate impact which means a toxi-infection. Therefore, the presence of antibiotics residues in milk can constitute an important risk at the allergic and antibiotic resistance cases on the consumer. The present study concerning the pathogens germs identification and Antibiotic residues seeking in milk and their impact on the human health, has been realized on a total number of 80 samples of raw milk resulted from direct sale channel (dairies) throughout Blida different regions localities. The Microbiological analysis has shown only three conform samples to JORA Standards. Really, milk non-conformity results to the microbiological standards consisting on total aerobic mesophilic flora total count, total coliforms, Thermotolerant coliforms E. coli, Faecal streptococcus, Staphylococcus aureus have shown the following contamination rate: 61.25%, 93.75%, 86.25%, 55%, 93.75% and 50%. Salmonella is characterized by a total absence in all analyzed milk samples. Moreover, the antibiotics residues research by Delvotest SP make plainly visible 33 positive samples. Further, two samples of the three which were judged conform to the bacteriology standards has been found contaminated by the antibiotic residues. The analyzed milk quality can be considered as a real danger to the consumption. 展开更多
关键词 Raw milk DAIRIES pathogenic bacteria antibiotics residues Delvotest SP.
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Incidence of Coagulase Positive Staphylococcus aureus in Raw Cow Milk Produced by Cattle Farms in Fieri Region in Albania
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作者 Kapllan Sulaj Jorida Terpollari +5 位作者 Renata Kongoli Kastriot Korro Sokol Duro Fejzo Selami Ilirian Kumbe Bejo Bizhga 《Journal of Life Sciences》 2013年第4期390-394,共5页
One hundred and five raw cow milk samples were collected from cattle farms located in Fieri from 2007 to 2009 and have been analyzed for presence of coagulase positive Staphylococcus aureus. Nineteen samples were conf... One hundred and five raw cow milk samples were collected from cattle farms located in Fieri from 2007 to 2009 and have been analyzed for presence of coagulase positive Staphylococcus aureus. Nineteen samples were confirmed positive for the presence of this pathogen. Stapylococcus aureus isolates identified appeared typically and atypically characteristics of growth colonies in Baird Parker agar plates at 37°C for 24-48 h. 6 out of 19 strains showed typical characteristics and 13 out 19 (68%) isolates had atypical characteristics. Coagulase positive Staphylococcus aureus was found in 18% (1911 05) of fresh milk samples. Milk produced by cows with subclinical mastitis largely influences Staphylococcus aureus count of bulk tank milk than contamination of milking and milk handling equipment by this pathogen. All S. aureus isolates were coagulase positive. 5 (or about 25%) of isolates of S. aureus identified were resistant to penicillin, 7 out 19 isolates or 36% resistant to methicilin and 9 out 19 strains or 47% resistant to vancomycin. Another objective of this study was the evaluation of the number of S. aureus per mL raw milk. The results confirmed that II (57.8%) out of 19 positive cases had more than 100 cfu/mL, indicating a possible risk for intoxication caused by production of entertoxines of coagulase positive S. aureus. 展开更多
关键词 Staphylococcus aureus INCIDENCE caw milk Fieri Albania.
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