The extraction fraction E and overall volumetric mass transfer coefficient kka of TBP extracting butyric acid pro- cess in confined impinging jet reactors （CIJR） with two jets were investigated. The main variables t...The extraction fraction E and overall volumetric mass transfer coefficient kka of TBP extracting butyric acid pro- cess in confined impinging jet reactors （CIJR） with two jets were investigated. The main variables tested were the concentration of tri-butyl-phosphate （TBP） and butyric acid, the impinging velocity V, the impinging velocityratio of two phases Vorg/Vaq, the nozzle inner diameter di and the distance L between the jet axes and the top wall of the impinging chamber. The results showed that E and kLa increase with an increase of the impinging velocity V, the concentration ofTBP Corg, and the impinging velocity ratio Vor/Vaq. However, E and kta decrease with an increase of the inner diameter d1 from 1 to 2 mm, the concentration of butyric acid Caq from 0.5% （v/v） to 2% （v/v）. The factor L ranging from 3 to 11 mm has a negligible effect on E and kLa. A correlation on these variables and kLa was proposed based on the experimental data. These results indicated good mass transfer oerformance of CIJR in the extraction operation.展开更多
The paper presents an energy iterative method to determine the second critical velocity by comparing the time histories of the kinetic energy and the buckling deformation based on the finite element model of the impac...The paper presents an energy iterative method to determine the second critical velocity by comparing the time histories of the kinetic energy and the buckling deformation based on the finite element model of the impact system. To design anti-impact structures of the thin-wall cylindrical tubes with this new method, the cost of the experiment can be considerably reduced. The feasibility and validity of this method are demonstrated by a dropping hammer experiment. In addition, this paper deals with the influence of constrained damping layers on the anti-impact capability and energy-absorption of thin-wall cylindrical tubes. Results show that the constrained damping layers make the energy-absorption and the anti-impact capability increased comparing with the naked tubes; the thickness of the damping layer should be restricted in a range, or else the anti-impact capability will decrease with the increase of the damping layer thickness; for the constrained layer, the anti-impact capability will increase with the augment of its thickness.展开更多
基金Supported by the National Natural Science Foundation of China(21206002,21376016)the State Key Laboratory of Chemical Engineering(SKL-Ch E-13A03)
文摘The extraction fraction E and overall volumetric mass transfer coefficient kka of TBP extracting butyric acid pro- cess in confined impinging jet reactors （CIJR） with two jets were investigated. The main variables tested were the concentration of tri-butyl-phosphate （TBP） and butyric acid, the impinging velocity V, the impinging velocityratio of two phases Vorg/Vaq, the nozzle inner diameter di and the distance L between the jet axes and the top wall of the impinging chamber. The results showed that E and kLa increase with an increase of the impinging velocity V, the concentration ofTBP Corg, and the impinging velocity ratio Vor/Vaq. However, E and kta decrease with an increase of the inner diameter d1 from 1 to 2 mm, the concentration of butyric acid Caq from 0.5% （v/v） to 2% （v/v）. The factor L ranging from 3 to 11 mm has a negligible effect on E and kLa. A correlation on these variables and kLa was proposed based on the experimental data. These results indicated good mass transfer oerformance of CIJR in the extraction operation.
文摘The paper presents an energy iterative method to determine the second critical velocity by comparing the time histories of the kinetic energy and the buckling deformation based on the finite element model of the impact system. To design anti-impact structures of the thin-wall cylindrical tubes with this new method, the cost of the experiment can be considerably reduced. The feasibility and validity of this method are demonstrated by a dropping hammer experiment. In addition, this paper deals with the influence of constrained damping layers on the anti-impact capability and energy-absorption of thin-wall cylindrical tubes. Results show that the constrained damping layers make the energy-absorption and the anti-impact capability increased comparing with the naked tubes; the thickness of the damping layer should be restricted in a range, or else the anti-impact capability will decrease with the increase of the damping layer thickness; for the constrained layer, the anti-impact capability will increase with the augment of its thickness.
