A new type of reactor,featured with impinging stream-rotating packed bed(IS-RPB)and coil pipes,was designed and used to prepare p-hydroxybenzaldehyde(PHB)by hydrolysis from diazonium salts.The influence of operati...A new type of reactor,featured with impinging stream-rotating packed bed(IS-RPB)and coil pipes,was designed and used to prepare p-hydroxybenzaldehyde(PHB)by hydrolysis from diazonium salts.The influence of operating parameters,such as reaction temperature,reaction time and high gravity factor,on the yield of PHB was investigated.Compared with the traditional kettle-type reactor,the yield of PHB with the new reactor is increased significantly and the reaction time is much shorter.Under the optimum conditions,the yield of PHB is increased from 51%to 84.1%.The reactor offers an opportunity for replacing the traditional batch mode operation with a continuous process.展开更多
The paper presents a technical solution which provides energy saving at full speed, as well as duplication of screw propeller and main propulsion system incase it's out of order. The description of the corresponding ...The paper presents a technical solution which provides energy saving at full speed, as well as duplication of screw propeller and main propulsion system incase it's out of order. The description of the corresponding device, designed for transport refrigerator ship, is shown as well as its location on board. Value of energy saving from the use of contra propeller is estimated. The results of the assessment required power to move the ship at low speed by the action of the contra propeller operating in the reactive mode are demonstrated. It is shown, that the ship equipped with the proposed device will get the additional class notation related to the redundancy or duplication of the propulsion system of Russian Maritime Register of Shipping.展开更多
基金Supported by the Science and Technology Key Projects of Shanxi Province(20090321113)
文摘A new type of reactor,featured with impinging stream-rotating packed bed(IS-RPB)and coil pipes,was designed and used to prepare p-hydroxybenzaldehyde(PHB)by hydrolysis from diazonium salts.The influence of operating parameters,such as reaction temperature,reaction time and high gravity factor,on the yield of PHB was investigated.Compared with the traditional kettle-type reactor,the yield of PHB with the new reactor is increased significantly and the reaction time is much shorter.Under the optimum conditions,the yield of PHB is increased from 51%to 84.1%.The reactor offers an opportunity for replacing the traditional batch mode operation with a continuous process.
文摘The paper presents a technical solution which provides energy saving at full speed, as well as duplication of screw propeller and main propulsion system incase it's out of order. The description of the corresponding device, designed for transport refrigerator ship, is shown as well as its location on board. Value of energy saving from the use of contra propeller is estimated. The results of the assessment required power to move the ship at low speed by the action of the contra propeller operating in the reactive mode are demonstrated. It is shown, that the ship equipped with the proposed device will get the additional class notation related to the redundancy or duplication of the propulsion system of Russian Maritime Register of Shipping.