A nickel-based superalloy with good corrosion resistance was fabricated by directional solidification, and its microstructure and tensile properties at elevated temperatures were investigated. Microstructure observati...A nickel-based superalloy with good corrosion resistance was fabricated by directional solidification, and its microstructure and tensile properties at elevated temperatures were investigated. Microstructure observations reveal that the γ＇ precipitates are arrayed in the y matrix regularly with some MC, Ni5Hf and M3B2 particles distributed along the grain boundary. The tensile tests exhibit that the tensile properties depend on temperature significantly and demonstrate obvious anomalous yield and intermediate-temperature brittleness （ITB） behavior. Below 650℃, the yield strength decreases slightly but the ultimate tensile strength almost has no change. When the temperature is between 650 ℃ and 750 ℃, the yield and ultimate tensile strengths rise rapidly, and after then they both decrease gradually with temperature increasing further. The elongation has its minimum value at about 700 ℃. The TEM examination exhibits that sharing of the γ＇ by dislocation is almost the main deformation mechanism at low temperatures, but the γ＇ by-pass dominates the deformation at high temperatures. The transition temperature from shearing to by-pass should be around 800 ℃. The anomalous yield and intermediate-temperature brittleness behaviors should be attributed to the high content of γ＇. In addition, the carbides and eutectic structure also contribute some to the ITB behaviors of the alloy.展开更多
Post-irradiation examination of encapsulated INCONEL 600 coiled flux detectors that had failed after several years of service in a CANDU reactor showed that many of the detector wires inside the carrier rod were broke...Post-irradiation examination of encapsulated INCONEL 600 coiled flux detectors that had failed after several years of service in a CANDU reactor showed that many of the detector wires inside the carrier rod were broken. It was concluded that failure occurred because the He cover gas was lost and replaced by air. Because He is a better thermal conductor than air, and because nuclear heating is significant, the temperature of the assembly increased. The examination showed that those parts of the INCONEL 600 detector wires that had operated at the highest temperature were the most severely embrittled. Parts of the same detector wires that were operating at lower temperatures remained ductile. The temperature dependence for the embrittlement of INCONEL 600 material can be explained in terms of the transition from recombination-dominated to sink-dominated reaction-rate kinetics for point defect accumulation at sinks. Cavity formation and accumulation at grain boundaries could weaken the material and result in the observed brittle intergranular failure.展开更多
基金Projects(2012BAI18B05,2012BAI18B01)supported by the Twelfth Five-Year National Science&Technology Support Program of ChinaProject(2009CB93004)supported by the National Basic Researh Program of China
文摘A nickel-based superalloy with good corrosion resistance was fabricated by directional solidification, and its microstructure and tensile properties at elevated temperatures were investigated. Microstructure observations reveal that the γ＇ precipitates are arrayed in the y matrix regularly with some MC, Ni5Hf and M3B2 particles distributed along the grain boundary. The tensile tests exhibit that the tensile properties depend on temperature significantly and demonstrate obvious anomalous yield and intermediate-temperature brittleness （ITB） behavior. Below 650℃, the yield strength decreases slightly but the ultimate tensile strength almost has no change. When the temperature is between 650 ℃ and 750 ℃, the yield and ultimate tensile strengths rise rapidly, and after then they both decrease gradually with temperature increasing further. The elongation has its minimum value at about 700 ℃. The TEM examination exhibits that sharing of the γ＇ by dislocation is almost the main deformation mechanism at low temperatures, but the γ＇ by-pass dominates the deformation at high temperatures. The transition temperature from shearing to by-pass should be around 800 ℃. The anomalous yield and intermediate-temperature brittleness behaviors should be attributed to the high content of γ＇. In addition, the carbides and eutectic structure also contribute some to the ITB behaviors of the alloy.
文摘Post-irradiation examination of encapsulated INCONEL 600 coiled flux detectors that had failed after several years of service in a CANDU reactor showed that many of the detector wires inside the carrier rod were broken. It was concluded that failure occurred because the He cover gas was lost and replaced by air. Because He is a better thermal conductor than air, and because nuclear heating is significant, the temperature of the assembly increased. The examination showed that those parts of the INCONEL 600 detector wires that had operated at the highest temperature were the most severely embrittled. Parts of the same detector wires that were operating at lower temperatures remained ductile. The temperature dependence for the embrittlement of INCONEL 600 material can be explained in terms of the transition from recombination-dominated to sink-dominated reaction-rate kinetics for point defect accumulation at sinks. Cavity formation and accumulation at grain boundaries could weaken the material and result in the observed brittle intergranular failure.
