Size distribution of nano-carbides produced by duplex treatments of surface nanocrystallization(by surface severe plastic deformation) and plasma electrolytic carburizing on CP-Ti was investigated.Skewness and kurtosi...Size distribution of nano-carbides produced by duplex treatments of surface nanocrystallization(by surface severe plastic deformation) and plasma electrolytic carburizing on CP-Ti was investigated.Skewness and kurtosis of Gussian shape distribution curves were studied and the effect of time was determined.The usage of longer time is more suitable for achieving less size of complex nano-carbides.Surface roughness of treated samples was measured.It is observed that there is an optimum level for time on surface roughness increasing(difference between two measured data).展开更多
Hardness of materials depends significantly on the indentation size and grain/sub-grain size via microindentation and nanoindentation tests of high-purity tungsten with different structures.The grain boundary effect a...Hardness of materials depends significantly on the indentation size and grain/sub-grain size via microindentation and nanoindentation tests of high-purity tungsten with different structures.The grain boundary effect and indentation size effect were explored.The indentation hardness was fitted using the Nix-Gao model by considering the scaling factor.The results show that the scaling factor is barely correlated with the grain/sub-grain size.The interaction between the plastically deformed zone(PDZ) boundary and the grain/sub-grain boundary is believed to be the reason that leads to an increase of the measured hardness at the specific depths.Results also indicate that the area of the PDZ is barely correlated with the grain/sub-grain size,and the indentation hardness starts to stabilize once the PDZ expands to the dimension of an individual grain/sub-grain.展开更多
The warm-hot deformation behavior of 20CrMnTi steel was studied with hot compression tests at temperature range of 1123-1273 K and strain rate of 0.1-20 s^-1. The activation energy for warm-hot deformation is 426.064 ...The warm-hot deformation behavior of 20CrMnTi steel was studied with hot compression tests at temperature range of 1123-1273 K and strain rate of 0.1-20 s^-1. The activation energy for warm-hot deformation is 426.064 KJ/mol. The influences of Zener-Hollomon parameter, strain and grain size imposing on the flow stress were analyzed in the temperature range of warm-hot forging. Creep theory and mathematical theory of statistics were used to obtain mathematical models of flow stress. The research and results provide scientific basis for controlling microstructure of forging process through Zener-Hollomon parameter.展开更多
To describe the relationship between the whole material deformation behavior and each grain deformation behavior inmicro-forming,experimental and numerical modelling methods were employed.Tensile test results reveal t...To describe the relationship between the whole material deformation behavior and each grain deformation behavior inmicro-forming,experimental and numerical modelling methods were employed.Tensile test results reveal that contrary to the valueof flow stress,the scatter of flow stress decreases with the increase of thickness-to-grain diameter(T/d)ratio.Microhardnessevaluation results show that each grain owns unique deformation behavior and randomly distributes in each specimen.The specimenwith less number of grains would be more likely to form an easy deformation zone and produce the concentration of plasticdeformation.Based on the experiment results,a size-dependent model considering the effects of grain size,geometry size,and thedeformation behavior of each grain was developed.And the effectiveness and practicability of the size-dependent model wereverified by experimental results.展开更多
In order to provide parameters for numerical analyses of the huge Three-Gorge concrete dam (2309 m long by 175 m height), complete tensile stress-deformation curves for large-size plain concrete specimens were measure...In order to provide parameters for numerical analyses of the huge Three-Gorge concrete dam (2309 m long by 175 m height), complete tensile stress-deformation curves for large-size plain concrete specimens were measured and studied by per-forming uniaxial tensile tests on large-size unnotched specimens (250 mm×250 mm×1400 mm). The specimens were prepared with the three-graded-aggregate materials provided by the client of the Three-Gorge project. To prevent a failure occurring near the ends of the unnotched specimens, both the ends of each specimen (450 mm in length) were cast using a higher-strength concrete than the middle part (i.e., active part). Tensile tests were completed on a specially-designed tensile testing machine, which can be easily re-assembled to accommodate different-size specimens. To make the specimens fail stably, a cyclic loading scheme was adopted after the peak strength was reached. Four of five tests in this study were successful, and four complete tensile stress-deformation curves were obtained. It was found that the post-peak curve of the large-size specimens used in this study is more gradual than those for the small-size specimens reported in the literature.展开更多
A constitutive equation was proposed to describe the effect of grain size on the deformation behavior.And a coupling simulation of deformation with heat transfer and microstructure was carried out in isothermal upsett...A constitutive equation was proposed to describe the effect of grain size on the deformation behavior.And a coupling simulation of deformation with heat transfer and microstructure was carried out in isothermal upsetting process of Ti60 alloy.The effects of processing parameters on the equivalent strain,the equivalent stress,the temperature rise and the grain size distribution in isothermal upsetting process of Ti60 alloy were analyzed.It is concluded that the uniformity of equivalent strain and equivalent stress increases with the increase of deformation temperature.However,the temperature rise and the grain size decreases with the increase of deformation temperature.The non-uniformity of equivalent strain,equivalent stress,temperature field and grain size increases with the increase of height reduction.And the calculated grain size using simulation is in good agreement with the experimental one.展开更多
Patterns of shear band, precursors to shear failure occurring in strain-softening stage, axial, lateral and volumetric strains as well as Poisson's ratio of plane strain rock specimens in compression for different he...Patterns of shear band, precursors to shear failure occurring in strain-softening stage, axial, lateral and volumetric strains as well as Poisson's ratio of plane strain rock specimens in compression for different heights were investigated by use of Fast Lagrangian Analysis of Continua(FLAC). A material imperfection closer to the lower-left corner of the specimen was prescribed. For finer mesh, the imperfection was modeled by four null elements, while it was modeled by a null element for coarser mesh. FISH functions were written to calculate the entire deformational characteristics of the specimen. In elastic stage, the adopted constitutive relation was linear elastic; in strain-softening stage, a composite Mohr-Coulomb criterion with tension cut-off and a post-peak linear constitutive relation were adopted. Height of rock specimen does not influence shear band's pattern (including the thickness and inclination angle of shear band). The slopes of the post-peak stress-axial strain curve, stress-lateral strain curve, lateral strain-axial strain curve, Poisson's ratio-axial strain curve and volumetric strain-axial strain curve depend on the height. Hence, the slopes of these curves cannot be considered as material properties. Nonlinear deformation prior to the peak stress is a kind of precursors to shear failure, which is less apparent for shorter specimen. For the same axial strain, lower lateral expansion is reached for shorter specimen, leading to lower Poisson's ratio and higher volumetric strain. The maximum volumetric strain of longer specimen is less than that of shorter specimen. The conclusions drawn from numerical results using finer mesh qualitatively agree with those using coarser mesh.展开更多
In order to clarify the influence of grain size on cyclic deformation response of superalloy sheets and springback behavior,cyclic loading-unloading and shearing tests were performed on the superalloy foils with 0.2 m...In order to clarify the influence of grain size on cyclic deformation response of superalloy sheets and springback behavior,cyclic loading-unloading and shearing tests were performed on the superalloy foils with 0.2 mm in thickness and diverse grain sizes.The results show that,the decline ratio of elastic modulus is weakened with increasing grain size,and the Bauschinger effect becomes evident with decreasing grain size.Meanwhile,U-bending test results determine that the springback is diminished with increasing grain size.The Chaboche,Anisotropic Nonlinear Kinematic(ANK)and Yoshida-Uemori(Y-U)models were utilized to fit the shear stress-strain curves of specimens.It is found that Y-U model is sufficient of predicting the springback.However,the prediction accuracy is degraded with increasing grain size.展开更多
A new phenomenological and empirically-based constitutive model was proposed to modify the term in the original Johnson−Cook constitutive model.The new model can be used to describe and predict the flow stress of AA10...A new phenomenological and empirically-based constitutive model was proposed to modify the term in the original Johnson−Cook constitutive model.The new model can be used to describe and predict the flow stress of AA1070 aluminum with different initial grain sizes in the hot working process.This developed model considers thermal softening,strain-rate hardening,strain hardening,initial grain size,and interactions with each other and can correctly model the behavior of AA1070 at elevated temperature with different strains,strain rates,and initial grain sizes.The hot flow behavior of AA1070 was investigated through compression tests over wide ranges of temperature from 623 to 773 K,strain rate from 0.005 to 0.5 s−1 and initial grain size from 50 to 450μm.Results show that the initial grain size has a significant effect on the flow behavior of AA1070.Then,correlation coefficient(R),average absolute relative error(AARE),and relative error were examined for comparative predictability of the model.Results show that flow stresses for different initial grain sizes calculated by the new proposed model perfectly correlate with experimental ones,with a mean relative error of 1.19%,which confirms that the new modified Johnson−Cook relation can give a precise estimation of the hot flow stress of AA1070 aluminum by considering the initial grain size.展开更多
To seek and describe the influence of bubble size on geometric and motion characteristics of the bubble,six nozzles with different outlet diameters were selected to inject air into water and to produce different bubbl...To seek and describe the influence of bubble size on geometric and motion characteristics of the bubble,six nozzles with different outlet diameters were selected to inject air into water and to produce different bubble sizes.High-speed photography in conjunction with an in-house bubble image processing code was used.During the evolution of the bubble,bubble shape,traveling trajectory and the variation of bubble velocity were obtained.Bubble sizes acquired varied from0.25to8.69mm.The results show that after the bubble is separated from the nozzle,bubble shape sequentially experiences ellipsoidal shape,hat shape,mushroom shape and eventually the stable ellipsoidal shape.As the bubble size increases,the oscillation of the bubble surface is intensified.At the stabilization stage of bubble motion,bubble trajectories conform approximately to the sinusoidal function.Meanwhile,with the increase in bubble size,the bubble trajectory tends to be straightened and the influence of the horizontal bubble velocity component on the bubble trajectory attenuates.The present results explain the phenomena related to relatively large bubble size,which extends the existing relationship between the bubble terminal velocity and the equivalent bubble diameter.展开更多
Carbon nanotubes are a promising candidate for the application of flexible electronics due to the ultrahigh intrinsic conductivity and excellent mechanical flexibility. In the present work, the morphology of the ultra...Carbon nanotubes are a promising candidate for the application of flexible electronics due to the ultrahigh intrinsic conductivity and excellent mechanical flexibility. In the present work, the morphology of the ultrathin (diameter<20 nm) multi-walled carbon nanotubes (MWCNTs) under an axial compression was investigated by using in-situ transmission electron microscopy. Moreover, the overall dynamic deformation processes and the force-displacement (F-D) curves of the MWCNTs were also examined. Interestingly, the MWCNTs almost restored their original morphology after 15 loading-unloading cycles. The deformation and recovery process indicate that the MWCNTs are flexible and exhibit excellent durability against compression. The Young’s modulus of the MWCNTs is estimated with the value of ∽0.655 TPa derived from the F-D curves fitting. Our results suggest that the ultrathin carbon nanotube structures may have great application potentials in flexible devices.展开更多
基金Partial work of this project funded by National Elite Foundation of Iran and Iranian Nanotechnology Initiative is appreciated.
文摘Size distribution of nano-carbides produced by duplex treatments of surface nanocrystallization(by surface severe plastic deformation) and plasma electrolytic carburizing on CP-Ti was investigated.Skewness and kurtosis of Gussian shape distribution curves were studied and the effect of time was determined.The usage of longer time is more suitable for achieving less size of complex nano-carbides.Surface roughness of treated samples was measured.It is observed that there is an optimum level for time on surface roughness increasing(difference between two measured data).
基金Project(51174235)supported by the National Natural Science Foundation of China
文摘Hardness of materials depends significantly on the indentation size and grain/sub-grain size via microindentation and nanoindentation tests of high-purity tungsten with different structures.The grain boundary effect and indentation size effect were explored.The indentation hardness was fitted using the Nix-Gao model by considering the scaling factor.The results show that the scaling factor is barely correlated with the grain/sub-grain size.The interaction between the plastically deformed zone(PDZ) boundary and the grain/sub-grain boundary is believed to be the reason that leads to an increase of the measured hardness at the specific depths.Results also indicate that the area of the PDZ is barely correlated with the grain/sub-grain size,and the indentation hardness starts to stabilize once the PDZ expands to the dimension of an individual grain/sub-grain.
基金Project supported by the Shanghai Automotive Industry Science andTechnology Development Fund, China
文摘The warm-hot deformation behavior of 20CrMnTi steel was studied with hot compression tests at temperature range of 1123-1273 K and strain rate of 0.1-20 s^-1. The activation energy for warm-hot deformation is 426.064 KJ/mol. The influences of Zener-Hollomon parameter, strain and grain size imposing on the flow stress were analyzed in the temperature range of warm-hot forging. Creep theory and mathematical theory of statistics were used to obtain mathematical models of flow stress. The research and results provide scientific basis for controlling microstructure of forging process through Zener-Hollomon parameter.
文摘To describe the relationship between the whole material deformation behavior and each grain deformation behavior inmicro-forming,experimental and numerical modelling methods were employed.Tensile test results reveal that contrary to the valueof flow stress,the scatter of flow stress decreases with the increase of thickness-to-grain diameter(T/d)ratio.Microhardnessevaluation results show that each grain owns unique deformation behavior and randomly distributes in each specimen.The specimenwith less number of grains would be more likely to form an easy deformation zone and produce the concentration of plasticdeformation.Based on the experiment results,a size-dependent model considering the effects of grain size,geometry size,and thedeformation behavior of each grain was developed.And the effectiveness and practicability of the size-dependent model wereverified by experimental results.
文摘In order to provide parameters for numerical analyses of the huge Three-Gorge concrete dam (2309 m long by 175 m height), complete tensile stress-deformation curves for large-size plain concrete specimens were measured and studied by per-forming uniaxial tensile tests on large-size unnotched specimens (250 mm×250 mm×1400 mm). The specimens were prepared with the three-graded-aggregate materials provided by the client of the Three-Gorge project. To prevent a failure occurring near the ends of the unnotched specimens, both the ends of each specimen (450 mm in length) were cast using a higher-strength concrete than the middle part (i.e., active part). Tensile tests were completed on a specially-designed tensile testing machine, which can be easily re-assembled to accommodate different-size specimens. To make the specimens fail stably, a cyclic loading scheme was adopted after the peak strength was reached. Four of five tests in this study were successful, and four complete tensile stress-deformation curves were obtained. It was found that the post-peak curve of the large-size specimens used in this study is more gradual than those for the small-size specimens reported in the literature.
基金Project(KP200905) supports by the Fund of the State Key Laboratory of Solidification Processing in Northwestern Polytechnical University,China
文摘A constitutive equation was proposed to describe the effect of grain size on the deformation behavior.And a coupling simulation of deformation with heat transfer and microstructure was carried out in isothermal upsetting process of Ti60 alloy.The effects of processing parameters on the equivalent strain,the equivalent stress,the temperature rise and the grain size distribution in isothermal upsetting process of Ti60 alloy were analyzed.It is concluded that the uniformity of equivalent strain and equivalent stress increases with the increase of deformation temperature.However,the temperature rise and the grain size decreases with the increase of deformation temperature.The non-uniformity of equivalent strain,equivalent stress,temperature field and grain size increases with the increase of height reduction.And the calculated grain size using simulation is in good agreement with the experimental one.
基金Supported by the National Natural Science Foundation of China(50309004)
文摘Patterns of shear band, precursors to shear failure occurring in strain-softening stage, axial, lateral and volumetric strains as well as Poisson's ratio of plane strain rock specimens in compression for different heights were investigated by use of Fast Lagrangian Analysis of Continua(FLAC). A material imperfection closer to the lower-left corner of the specimen was prescribed. For finer mesh, the imperfection was modeled by four null elements, while it was modeled by a null element for coarser mesh. FISH functions were written to calculate the entire deformational characteristics of the specimen. In elastic stage, the adopted constitutive relation was linear elastic; in strain-softening stage, a composite Mohr-Coulomb criterion with tension cut-off and a post-peak linear constitutive relation were adopted. Height of rock specimen does not influence shear band's pattern (including the thickness and inclination angle of shear band). The slopes of the post-peak stress-axial strain curve, stress-lateral strain curve, lateral strain-axial strain curve, Poisson's ratio-axial strain curve and volumetric strain-axial strain curve depend on the height. Hence, the slopes of these curves cannot be considered as material properties. Nonlinear deformation prior to the peak stress is a kind of precursors to shear failure, which is less apparent for shorter specimen. For the same axial strain, lower lateral expansion is reached for shorter specimen, leading to lower Poisson's ratio and higher volumetric strain. The maximum volumetric strain of longer specimen is less than that of shorter specimen. The conclusions drawn from numerical results using finer mesh qualitatively agree with those using coarser mesh.
基金the National Natural Science Foundation of China(Nos.51975031,52075023,51635005)Defense Industrial Technology Development Program,China(No.JCKY2018601C207)。
文摘In order to clarify the influence of grain size on cyclic deformation response of superalloy sheets and springback behavior,cyclic loading-unloading and shearing tests were performed on the superalloy foils with 0.2 mm in thickness and diverse grain sizes.The results show that,the decline ratio of elastic modulus is weakened with increasing grain size,and the Bauschinger effect becomes evident with decreasing grain size.Meanwhile,U-bending test results determine that the springback is diminished with increasing grain size.The Chaboche,Anisotropic Nonlinear Kinematic(ANK)and Yoshida-Uemori(Y-U)models were utilized to fit the shear stress-strain curves of specimens.It is found that Y-U model is sufficient of predicting the springback.However,the prediction accuracy is degraded with increasing grain size.
文摘A new phenomenological and empirically-based constitutive model was proposed to modify the term in the original Johnson−Cook constitutive model.The new model can be used to describe and predict the flow stress of AA1070 aluminum with different initial grain sizes in the hot working process.This developed model considers thermal softening,strain-rate hardening,strain hardening,initial grain size,and interactions with each other and can correctly model the behavior of AA1070 at elevated temperature with different strains,strain rates,and initial grain sizes.The hot flow behavior of AA1070 was investigated through compression tests over wide ranges of temperature from 623 to 773 K,strain rate from 0.005 to 0.5 s−1 and initial grain size from 50 to 450μm.Results show that the initial grain size has a significant effect on the flow behavior of AA1070.Then,correlation coefficient(R),average absolute relative error(AARE),and relative error were examined for comparative predictability of the model.Results show that flow stresses for different initial grain sizes calculated by the new proposed model perfectly correlate with experimental ones,with a mean relative error of 1.19%,which confirms that the new modified Johnson−Cook relation can give a precise estimation of the hot flow stress of AA1070 aluminum by considering the initial grain size.
基金Project(51676087)supported by the National Natural Science Foundation of China
文摘To seek and describe the influence of bubble size on geometric and motion characteristics of the bubble,six nozzles with different outlet diameters were selected to inject air into water and to produce different bubble sizes.High-speed photography in conjunction with an in-house bubble image processing code was used.During the evolution of the bubble,bubble shape,traveling trajectory and the variation of bubble velocity were obtained.Bubble sizes acquired varied from0.25to8.69mm.The results show that after the bubble is separated from the nozzle,bubble shape sequentially experiences ellipsoidal shape,hat shape,mushroom shape and eventually the stable ellipsoidal shape.As the bubble size increases,the oscillation of the bubble surface is intensified.At the stabilization stage of bubble motion,bubble trajectories conform approximately to the sinusoidal function.Meanwhile,with the increase in bubble size,the bubble trajectory tends to be straightened and the influence of the horizontal bubble velocity component on the bubble trajectory attenuates.The present results explain the phenomena related to relatively large bubble size,which extends the existing relationship between the bubble terminal velocity and the equivalent bubble diameter.
基金supported by the National Natural Science Foundation of China (No.51573201, No.21773205, No.51501209, and No.201675165)NSFC-Zhejiang Joint Fund for the Integration of Industrialization and Informatization (U1709205)+6 种基金National Key R&D Program of China (2017YFB0406000)the Project of the Chinese Academy of Sciences (YZ201640 and KFZDSW-409)Public Welfare Project of Zhejiang Province (2016C31026)Science and Technology Major Project of Ningbo (2016B10038 and 2016S1002)International S&T Cooperation Program of Ningbo (2017D10016)the 3315 Program of Ningbothe Science and Technology Major Project of Ningbo (2015S1001)
文摘Carbon nanotubes are a promising candidate for the application of flexible electronics due to the ultrahigh intrinsic conductivity and excellent mechanical flexibility. In the present work, the morphology of the ultrathin (diameter<20 nm) multi-walled carbon nanotubes (MWCNTs) under an axial compression was investigated by using in-situ transmission electron microscopy. Moreover, the overall dynamic deformation processes and the force-displacement (F-D) curves of the MWCNTs were also examined. Interestingly, the MWCNTs almost restored their original morphology after 15 loading-unloading cycles. The deformation and recovery process indicate that the MWCNTs are flexible and exhibit excellent durability against compression. The Young’s modulus of the MWCNTs is estimated with the value of ∽0.655 TPa derived from the F-D curves fitting. Our results suggest that the ultrathin carbon nanotube structures may have great application potentials in flexible devices.