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SLM制备Ti6Al4V合金表层组织的均质化及腐蚀行为研究
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作者 郑志军 张文韬 《中南大学学报(自然科学版)》 EI CAS CSCD 北大核心 2024年第8期2991-3001,共11页
采用激光选区熔化(SLM)增材制造工艺制备致密度为97.5%的Ti6Al4V合金,并利用高能喷丸与退火处理复合工艺对垂直建造方向的XOY面及平行建造方向的XOZ面进行均质化处理,然后对原始打印件、喷丸处理以及喷丸+退火处理的3种状态的试样进行... 采用激光选区熔化(SLM)增材制造工艺制备致密度为97.5%的Ti6Al4V合金,并利用高能喷丸与退火处理复合工艺对垂直建造方向的XOY面及平行建造方向的XOZ面进行均质化处理,然后对原始打印件、喷丸处理以及喷丸+退火处理的3种状态的试样进行电化学性能测试。研究结果表明:经喷丸处理后,原始打印件XOY面和XOZ面的组织趋于均质化,同时组织明显细化;喷丸既不改变衍射峰的位置,也不产生新的衍射峰,但可使衍射峰宽化;对于喷丸后经不同温度退火处理的样品,随退火温度的升高,XOY面和XOZ面的晶粒逐渐长大,在780℃退火后,二者均可获得α+β双相组织。对于原始打印件,XOY面和XOZ面的电化学腐蚀行为存在明显的差异,其中,XOY面的腐蚀倾向更小,耐蚀性能更优。经喷丸+退火处理后,这种差异明显减小,同时耐蚀性能进一步提高,经综合考虑可得喷丸+780℃退火为最佳工艺。 展开更多
关键词 激光选区熔化 TI6AL4V合金 喷丸 组织各向异性
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深冲用TC4板材组织织构 被引量:2
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作者 王红武 王俭 +3 位作者 任连宝 陈东 王小翔 王希哲 《金属学报》 SCIE EI CAS CSCD 北大核心 2002年第z1期191-193,共3页
分析了几种典型的TC4板材组织织构,阐述了织构与力学性能的关系,得出控制合理的织构可以获得优异的综合力学性能,消除各向异性.
关键词 TC4板材 组织织构 各向异性
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各向异性生物组织中偏振光传输的模拟与实验 被引量:4
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作者 云天梁 曾楠 +1 位作者 李伟 马辉 《光学学报》 EI CAS CSCD 北大核心 2009年第7期1926-1929,共4页
针对具有纤维状结构特征的生物组织(诸如肌肉、皮肤等),建立了包含球状散射体和具有取向分布的圆柱状散射体的仿体模型,并对偏振光在这类具有各向异性分布的复杂体系中的传输过程进行了蒙特卡罗模拟。给出了蒙特卡罗模拟程序的实现方法... 针对具有纤维状结构特征的生物组织(诸如肌肉、皮肤等),建立了包含球状散射体和具有取向分布的圆柱状散射体的仿体模型,并对偏振光在这类具有各向异性分布的复杂体系中的传输过程进行了蒙特卡罗模拟。给出了蒙特卡罗模拟程序的实现方法并验证了程序的可靠性,随后将程序用于模拟和分析一些肌肉组织的偏振成像实验。实验和模拟结果的一致性验证了用柱-球散射体混合的仿体模型来模拟各向异性生物组织的合理性。同时,通过模拟验证,得到了两个新的参量,分别可以用来表征组织样品中纤维的空间取向和组织样品的各向异性度。 展开更多
关键词 散射 偏振成像 蒙特卡罗模拟 各向异性组织 仿体
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热处理对增材制造316L不锈钢组织各向异性的影响 被引量:5
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作者 董智豪 郑志军 彭乐 《金属热处理》 CAS CSCD 北大核心 2021年第10期45-52,共8页
以选区激光熔化(SLM)制备的316L不锈钢为研究对象。首先对打印件的孔隙率、微观组织进行了表征,然后探究了热处理对组织各向异性及硬度的影响规律。结果表明,打印件的体积孔隙率和面孔隙率均较低,均在1%以下,二者之间没有明显差别;对于... 以选区激光熔化(SLM)制备的316L不锈钢为研究对象。首先对打印件的孔隙率、微观组织进行了表征,然后探究了热处理对组织各向异性及硬度的影响规律。结果表明,打印件的体积孔隙率和面孔隙率均较低,均在1%以下,二者之间没有明显差别;对于垂直打印方向的XY面,主要由互成67°交叉的条状微熔池组成,条状微熔池中包含柱状和胞状两种组织,前者主要位于熔池边界,长约几十微米、宽约400 nm,后者主要位于熔池中心位置,尺寸约400 nm;对于平行于打印方向的YZ面,熔池主要呈扇状,扇状熔池内部也包含柱状和胞状两种组织,但分布更加复杂,其中柱状组织贯穿多层熔池生长,XY面与YZ面在微观组织上存在着明显的各向异性。适当的热处理工艺可有效改善组织的各向异性,XY面在800℃×2 h热处理后基本可以实现均匀化,而YZ面在900℃×2 h处理后才达到均匀化。拥有微纳尺寸结构的增材制造件拥有比传统零件更高的硬度。此外,热处理可使不同方向上的硬度下降,但垂直打印方向上的硬度下降幅度更大。 展开更多
关键词 增材制造 316L不锈钢 微观组织各向异性 热处理
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针状焦制备过程中的中间相研究进展 被引量:7
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作者 张德保 申海平 范启明 《化工进展》 EI CAS CSCD 北大核心 2012年第S2期175-181,共7页
中间相的结构形态直接决定了针状焦的质量性能。本文对针状焦制备过程中的中间相结构以及影响中间相形成的各种因素进行了概述,并展望了针状焦制备过程中关于中间相研究的发展前景。
关键词 中间相 针状焦 各向异性组织
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Anisotropy of localized corrosion in 7050-T7451 Al alloy thick plate 被引量:4
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作者 宋丰轩 张新明 +2 位作者 刘胜胆 韩念梅 李东锋 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2013年第9期2483-2490,共8页
The corrosion anisotropy of 7050-T7451 A1 alloy thick plate in NaCI solution was investigated by immersion tests, slow strain rate testing (SSRT) technique, potentiodynamic and anode polarization measurements, optic... The corrosion anisotropy of 7050-T7451 A1 alloy thick plate in NaCI solution was investigated by immersion tests, slow strain rate testing (SSRT) technique, potentiodynamic and anode polarization measurements, optical microscropy (OM) and scanning electron microscopy (SEM) observations. The results show that the thick plate exhibits severe corrosion anisotropy due to the microstructure anisotropy. The observations of immersion surfaces together with the analysis of polarization curves reveal that the differences of the corrosion morphologies on various sections in this material are mainly related to the area fraction of the remnant second phase, and higher area fraction displays worst corrosion resistance. The stress corrosion cracking (SCC) susceptibility of different directions relative to the rolling direction is assessed by SSRT technique, ranked in the order: S direction 〉 L direction 〉 T direction. The result show that the smaller the grain aspect ratio, the better the corrosion resistance to SCC. 展开更多
关键词 7050-T7451 A1 alloy thick plate microstructure corrosion anisotropy
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Mixed grain structure and mechanical property anisotropy of AZ40 magnesium alloy bar with diameter of 160 mm 被引量:1
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作者 石国梁 张奎 +4 位作者 李兴刚 李永军 马鸣龙 袁家伟 卢春芳 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2015年第12期3944-3952,共9页
The mixed grain structure and mechanical property anisotropy of AZ40 magnesium alloy bar with a diameter of 160 mm manufactured by "multi-direction forging(MDF) + extrusion + online cooling" technique were inves... The mixed grain structure and mechanical property anisotropy of AZ40 magnesium alloy bar with a diameter of 160 mm manufactured by "multi-direction forging(MDF) + extrusion + online cooling" technique were investigated by optical microscopy(OM), scanning electron microscopy(SEM), X-ray diffraction macro-texture measurement and room temperature(RT) tensile test. The results show that mixed grain structure is caused by the micro-segregation of Al in semi-continuous casting ingot. Homogenization of(380 °C, 8 h) +(410 °C, 12 h) cannot totally eliminate such micro-segregation. During MDF and extrusion, the dendrite interiors with 3%-4% Al(mass fraction) transform to fine grain zones, yet the dendrite edges with about 6% Al transform to coarse grain zones. XRD macro-textures of the outer, R/2 and center show typical fiber texture characteristics and the intensity of [0001]//Ra D orientation in the outer(11.245) is about twice as big as those in the R/2(6.026) and center(6.979). The as-extruded AZ40 magnesium alloy bar has high elongation(A) and moderate ultimate tensile strength(Rm) in both extrusion direction(ED) and radius direction(Ra D), i.e., A of 19%-25% and Rm of 256-264 MPa; however, yield strength(Rp0.2) shows anisotropy and heterogeneity, i.e., 103 MPa in Ra D, 137 MPa in ED-C(the center) and 161 MPa in ED-O(the outer), which are mainly caused by the texture.(155 °C, 7 h) +(170 °C, 24 h) aging has no influence on strength and elongation of AZ40 magnesium bar. 展开更多
关键词 AZ40 magnesium alloy mixed grain structure mechanical properties ANISOTROPY MICRO-SEGREGATION texture
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Microstructure and mechanical properties of Ti6Al4V alloy prepared by selective laser melting combined with precision forging 被引量:12
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作者 Qi ZHANG Zheng-long LIANG +3 位作者 Miao CAO Zi-fan LIU An-feng ZHANG Bing-heng LU 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2017年第5期1036-1042,共7页
To improve the mechanical properties of Ti6Al4V alloy prepared by selective laser melting(SLM)process,the precision forging was conducted at950°C and different strains and strain rates.The microstructure evolutio... To improve the mechanical properties of Ti6Al4V alloy prepared by selective laser melting(SLM)process,the precision forging was conducted at950°C and different strains and strain rates.The microstructure evolution of as-built samples and forged samples in both horizontal and vertical sections was visualized and analyzed by optical microscope and X-ray diffraction.The microstructure was improved by the precision forging and subsequent water quenching.The porosity in each section was accounted.It can be seen that high strain rate and large deformation result in low porosity,consequently contributing to a better fatigue performance.The micro-hardness was lowered after precision forging and water quenching,while the difference of microhardness between the horizontal and vertical sections became smaller,which illustrated that this process can improve the anisotropy of structural components fabricated by SLM. 展开更多
关键词 selective laser melting Ti6Al4V alloy precision forging MICROSTRUCTURE ANISOTROPY
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基于布洛克磁共振流动方程和贝塞尔函数的磁共振成像序列数学设计(英文) 被引量:2
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作者 O.B.Awojoyogbe O.M.Dada 《磁共振成像》 CAS CSCD 2013年第5期373-381,共9页
Bloch方程是NMR/MRI计算、模拟和实验的基础,但通常在不加特定的绝热和非绝热条件的前提下获得Bloch流动方程的解析解是非常困难的。流动方程的一般解析解可以为理解NMR/MRI的基本概念提供额外的信息,而又不需要通常的指数方程。作者的... Bloch方程是NMR/MRI计算、模拟和实验的基础,但通常在不加特定的绝热和非绝热条件的前提下获得Bloch流动方程的解析解是非常困难的。流动方程的一般解析解可以为理解NMR/MRI的基本概念提供额外的信息,而又不需要通常的指数方程。作者的目的是通过贝塞尔函数及其特性得到与时间无关的NMR流动方程的解析解。在不需要主观添加弥散项的前提下利用贝塞尔函数及其特性从NMR流动方程中获得了Stejskal-Tanner公式。这证实了弥散是Bloch流动方程的内在属性并可以通过如贝塞尔函数的适当数学函数提取出来。从解析解得到的非高斯行为的弥散信号在如脑白质的各项异性组织环境中是非常有意义的。发现弥散系数是与T1和T2弛豫参数直接相关的,因此通过对大量已有的贝塞尔函数进行合适利用可以在四个分离的缓存内采集MRI信号(实部和虚部,相位和绝对值)。能够利用MRI监测药物对于不同组织尤其是脑部功能活动的效果。 展开更多
关键词 弥散磁共振成像 Bloch磁共振方程 贝塞尔函数 曲折度和各向异性组织环境
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Effect of large strain cross rolling on microstructure and properties of Al-Li alloy plates with high magnesium content 被引量:4
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作者 Cai-he FAN Dong-sheng ZHENG +3 位作者 Xi-hong CHEN Jian-jun YANG Yong LIU Hui-zhong LI 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2019年第2期263-269,共7页
Transmission electron microscopy(TEM),electron backscattered diffraction imaging(EBSD)and X-ray diffractometry were used to analyze the microstructure and texture characteristics of Al-9.8Mg-1.5Li-0.4Mn alloy cross-ro... Transmission electron microscopy(TEM),electron backscattered diffraction imaging(EBSD)and X-ray diffractometry were used to analyze the microstructure and texture characteristics of Al-9.8Mg-1.5Li-0.4Mn alloy cross-rolled and extruded plates,and the tensile properties and deep drawing performance were measured.The results show that the occurrence of dynamic recrystallization was promoted,the grains were refined and the preferred orientation of the recrystallized grains was improved by large strain cross rolling.Compared with CBA and CCB rolling methods,CBB rolling method significantly reduced the orientation density of the typical Brass texture{110}?112?in the extruded plates.The orientation densities of Copper texture{112}?111?and Brass texture{110}?112?on theβorientation line in the CBB rolled plates were the lowest,and there were no typical texture features in the plates.Meanwhile,better deep drawing could be gained in the CBB rolled plates,and the mechanical properties of the 0°,45°and 90°directions were basically the same.The tensile strength,yield strength and elongation at room temperature for the CBB rolled plates were 617 MPa,523 MPa and over 20.1%,respectively.The deviation of the mechanical properties at different directions was less than 3%. 展开更多
关键词 cross rolling Al-Li alloy plate MICROSTRUCTURE ANISOTROPY texture feature
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Influence of rolling ways on microstructure and anisotropy of AZ31 alloy sheet
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作者 陈兴品 尚都 +2 位作者 肖睿 黄光杰 刘庆 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2010年第B07期589-593,共5页
Two rolling ways,unidirectional rolling and cross rolling,were carried out on twin roll cast AZ31 alloy sheet to study the influence of strain path change on the evolution of the rolling microstructure and texture as ... Two rolling ways,unidirectional rolling and cross rolling,were carried out on twin roll cast AZ31 alloy sheet to study the influence of strain path change on the evolution of the rolling microstructure and texture as well as the anisotropic properties of AZ31 alloy sheet with microscopy,X-ray diffraction technique and tensile tests.It is found that cross rolling gives rise to more uniform microstructure and stronger texture intensities compared with unidirectional rolling.The differences in the microstructure and texture intensities are reflected in the anisotropy characterized by the difference in the yield stress and the fracture elongation that were measured along directions in the rolling plane at angles of 0■,45■and 90■from the rolling direction. 展开更多
关键词 AZ31 alloy sheet cross rolling MICROSTRUCTURE TEXTURE ANISOTROPY
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Self-Organized Criticality in an Anisotropic Earthquake Model
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作者 Bin-Quan Li Sheng-Jun Wang 《Communications in Theoretical Physics》 SCIE CAS CSCD 2018年第3期280-284,共5页
We have made an extensive numerical study of a modified model proposed by Olami,Feder,and Christensen to describe earthquake behavior.Two situations were considered in this paper.One situation is that the energy of th... We have made an extensive numerical study of a modified model proposed by Olami,Feder,and Christensen to describe earthquake behavior.Two situations were considered in this paper.One situation is that the energy of the unstable site is redistributed to its nearest neighbors randomly not averagely and keeps itself to zero.The other situation is that the energy of the unstable site is redistributed to its nearest neighbors randomly and keeps some energy for itself instead of reset to zero.Different boundary conditions were considered as well.By analyzing the distribution of earthquake sizes,we found that self-organized criticality can be excited only in the conservative case or the approximate conservative case in the above situations.Some evidence indicated that the critical exponent of both above situations and the original OFC model tend to the same result in the conservative case.The only difference is that the avalanche size in the original model is bigger.This result may be closer to the real world,after all,every crust plate size is different. 展开更多
关键词 self-organized criticality earthquake model power-law
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