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铀同位素标准物质在核燃料系统实验室间比对中的应用
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作者 陈岚 王妍妍 《同位素》 CAS 2021年第2期163-168,共6页
在核燃料系统分析检测实验室间比对活动中,首次开展铀同位素检测项目的设计、策划和实施,选取国家一级标准物质“八氧化三铀中铀同位素标准物质”作为分割样品对,分别采用Z比分数、标准物质测量结果的误差允许限(E)作为能力统计量,对实... 在核燃料系统分析检测实验室间比对活动中,首次开展铀同位素检测项目的设计、策划和实施,选取国家一级标准物质“八氧化三铀中铀同位素标准物质”作为分割样品对,分别采用Z比分数、标准物质测量结果的误差允许限(E)作为能力统计量,对实验室间铀同位素丰度的比对结果进行统计和分析,对测量结果有问题或不满意的情况进行分析和建议。通过首次开展铀同位素项目的比对,拓展了核工业系统实验室能力验证范畴,进一步提高实验室的检测水平,对核燃料循环生产中铀同位素的测量提供了技术基础保障和质量保证。 展开更多
关键词 核燃料系统 同位素标准物质 实验室间比对 Z比分数 误差允许限(E)
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放射性同位素标准目录
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《核标准计量与质量》 1998年第3期54-56,共3页
关键词 同位素标准
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与标准平均海水同位素成分相近的石英水三相点瓶的研制
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作者 赵明坚 G +1 位作者 F Strouse 《计量学报》 CSCD 北大核心 2007年第z1期47-50,共4页
介绍了与标准平均海水同位素(VSMOW)成分相近的石英水三相点瓶的研制过程和试验分析结果.利用新的制作工艺,所有水三相点瓶的同位素成分δD和δ18O可被分别控制在±10‰和±1.5‰之内,这样即使没有进行同位素修正,由同位素成分... 介绍了与标准平均海水同位素(VSMOW)成分相近的石英水三相点瓶的研制过程和试验分析结果.利用新的制作工艺,所有水三相点瓶的同位素成分δD和δ18O可被分别控制在±10‰和±1.5‰之内,这样即使没有进行同位素修正,由同位素成分与VSMOW的偏离对温度的影响仍可控制在±8μK之内.如果对某个水三相点容器的同位素成分单独分析,并用分析结果对水三相点温度值进行修正,则由上述因素对温度的影响可控制在±3μK之内.实验结果表明,硼硅玻璃水三相点瓶的年漂移约为-13μK,而石英水三相点瓶年漂移约为-2μK,因此,石英水三相点瓶比硼硅玻璃水三相点瓶的性能更加优越. 展开更多
关键词 计量学 水三相点 石英水三相点瓶 标准平均海水同位素
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全国核能标准化技术委员会放射性同位素分技术委员会三届一次会议在京召开
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作者 韩全胜 《核标准计量与质量》 1997年第1期52-52,共1页
关键词 放射性同位素 标准化技术 技术委员会 同位素标准 标准化工作 核能 开发和应用 工作总结 工作规划 全体委员
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Short-term effectiveness of radiochemoembolization for selected hepatic metastases with a combination protocol 被引量:2
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作者 Shahram Akhlaghpoor Alireza Aziz-Ahari +3 位作者 Mahasti Amoui Shahnaz Tolooee Hossein Poorbeigi Shahab Sheybani 《World Journal of Gastroenterology》 SCIE CAS CSCD 2012年第37期5249-5259,共11页
AIM: To introduce the combination method of radio- chemoembolization for the treatment of selected he- patic metastases. METHODS: Twenty patients with biopsy proven hepat- ic metastases were selected from those who ... AIM: To introduce the combination method of radio- chemoembolization for the treatment of selected he- patic metastases. METHODS: Twenty patients with biopsy proven hepat- ic metastases were selected from those who underwent transarterial radiochemoembolization, a novel combina- tion protocol, between .lanuary 2009 and July 2010. Patients had different sources of liver metastasis. The treatment included transarterial administration of three chemotherapeutic drugs (mitomycin, doxorubicin and cisplatin), followed by embolization with large (50-150 μm) radioisotope particles of chromic 32R Multiphasic computer tomography or computer tomography stud- ies, with and without contrast medium injections, were performed for all patients for a short-term period before and after the treatment sessions. The short-term effec- tiveness of this procedure was evaluated by modified response evaluation criteria in solid tumors (mRECIST), which also takes necrosis into account. The subjective percentage of necrosis was also assessed. The re- sponse evaluation methods were based on the changes in size, number, and the enhancement patterns of the lesions between the pre- and post-treatment imaging studies. RESULTS: Patients had liver metastasis from colorectal carcinomas, breast cancer, lung cancer and carcinoid tumors. The response rate based on the mRECIST criteria was 5% for complete response, 60% for par- tial response, 10% for stable disease, and 25% for progressive disease. Regarding the subjective necrosis percentage, 5% of patients had complete response, 50% had partial response, 25% had stable disease, and 20% had progressive disease. Based on traditional RECIST criteria, 3 patients (15%) had partial response, 13 patients (65%) had stable disease, and 4 patients (20%) had disease progression. In most patients, colorectal carcinoma was the source of metastasis (13 patients). Based on the mRECIST criteria, 8 out of these 13 patients had partial responses, while one remained stable, and 5 showed progressive disease. We also had 5 cases of breast cancer metastasis which mostly remained stable (4 cases), with only one partial response after the procedure. Six patients had bilobar involvement; three of them received two courses of radiochemoembolization. The follow up imaging study of these patients was performed after the second ses- sion. In the studied patients there was no evidence of extrahepatic occurrence, including pulmonary radioac- tive deposition, which was proven by Bremsstrahlung scintigraphy performed after the treatment sessions. For the short-term follow-ups for the 2 mo after the therapy, no treatment related death was reported. The mostly common side effect was post-embolization syndrome, presented as vomiting, abdominal pain, and fever. Nineteen (95%) patients experienced this syndrome in different severities. Two patient had asci- tes (with pleural effusion in one patient) not related to hepatic failure. Moreover, no cases of acute liver failure, hepatic infarction, hepatic abscess, biliary necrosis, tu- mor rupture, surgical cholecystitis, or non-targeted gut embolization were reported. Systemic toxicities such as alopecia, marrow suppression, renal toxicity, or cardiac failure did not occur in our study group. CONCLUSION: Radiochemoembolization is safe and effective for selected hepatic metastases in a short- term follow-up. Further studies are required to show the long-term effects and possible complications of this approach. 展开更多
关键词 Hepatic metastasis Radiochemoemboliza-tion Phosphorus radioisotopes TREATMENT OUTCOME
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Standard-sample bracketing calibration method combined with Mg as an internal standard for silicon isotopic compositions using multi-collector inductively coupled plasma mass spectrometry 被引量:3
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作者 Honglin Yuan Cheng Cheng +1 位作者 Kaiyun Chen Zhian Bao 《Acta Geochimica》 EI CAS CSCD 2016年第4期421-427,共7页
Silicon isotope analysis traditionally uses a standard-sample bracketing (SSB) method that relies upon greater instrument stability than can be consistently expected. The following proposed method reduces the level ... Silicon isotope analysis traditionally uses a standard-sample bracketing (SSB) method that relies upon greater instrument stability than can be consistently expected. The following proposed method reduces the level of instrumental stability required for the analysis process and provides a valid solution for high-precision and accurate studies of Si isotopic compositions. Rock samples were dissolved by using alkali fusion and acidification. Silicon isotopes were purified with an ion exchange resin. Interfering peaks for isotopes were separated by using a Nu Plasma 1700 multi-collector inductively coupled plasma mass spectrometry (MS) system in high-resolution mode (M/AM 〉 8000 RP). Two magnesium isotopes (25Mg and 26Mg) and three silicon isotopes (28Si, 29Si, and 3;Si) were analyzed in the same data collection cycle. Mg isotopes were used as an internal standard to calibrate the mass discrimination effects in MS analysis of Si isotopes in combination with the SSB method in order to reduce the effects of MS interference and instrumental mass dis- crimination on the accuracy of measurements. The conventional SSB method without the Mg internal standard and the proposed SSB method with Mg calibration delivered consistent results within two standard deviations. When Mg was used as an internal standard for calibration, the analysis precision was better than 0.05 %0 amu. 展开更多
关键词 Si isotope Mg internal standard - MC-ICP- MS Rock samples High resolution
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CSBTS/TC58/SC4三届二次年会在广西召开
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《核标准计量与质量》 1998年第1期51-51,共1页
关键词 荧光分析 广西 技术委员会 同位素标准 分析方法 标准建议 标准化研究 行业标准 标准化技术 度量值
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