A simple method used for simultaneous measurement of phase retardation and optic axis of wave plate by employing 1/4 wave plate is demonstrated. The theoretical analysis of the measuring principle is presented in deta...A simple method used for simultaneous measurement of phase retardation and optic axis of wave plate by employing 1/4 wave plate is demonstrated. The theoretical analysis of the measuring principle is presented in detail. In the measurement, after adjusting a standard 1/4 wave plate and the fast (slow) axis of the plate to be measured parallel to the pass axis of the polarizer, the plate to be measured is rotated by 450 counterclockwisly. A stepping motor is used to rotate the analyzer. The experimental data are collected by a photodetector and then sent to a computer. According to the output data curve, the phase retardation and optic axis of the plate to be measured can be obtained simultaneously. To test the feasibility of the method, a λ /2 and a λ /8 wave plates are used as examples to demonstrate the measurement procedures. The phase retardation measurement accuracy is better than 0.5×10-2. This method can be used to measure the arbitrary phase retardation conveniently.展开更多
Reagents are optimized for the simultaneous determination of trace amounts of Cu^(2+), Cd^(2+) and Co^(2+) in zinc sulfate solution, which contains an extremely large excess of Zn^(2+). First, the reagents and their d...Reagents are optimized for the simultaneous determination of trace amounts of Cu^(2+), Cd^(2+) and Co^(2+) in zinc sulfate solution, which contains an extremely large excess of Zn^(2+). First, the reagents and their doses for the experiment are selected according to the characteristics of the zinc sulfate solution. Then, the reagent doses are optimized by analyzing the influence of reagent dose on the polarographic parameters(i.e. half-wave potential E_(1/2) and limiting diffusion current I_p). Finally, the optimization results are verified by simultaneously determining trace amounts of Cu^(2+), Cd^(2+) and Co^(2+) in the presence of an extremely large excess of Zn^(2+). The determination results indicate that the optimized reagents exhibit wide linearity, low detection limits, high accuracy and good precision for the simultaneous determination of trace amounts of Cu^(2+), Cd^(2+) and Co^(2+) in the presence of an extremely large excess of Zn^(2+).展开更多
文摘A simple method used for simultaneous measurement of phase retardation and optic axis of wave plate by employing 1/4 wave plate is demonstrated. The theoretical analysis of the measuring principle is presented in detail. In the measurement, after adjusting a standard 1/4 wave plate and the fast (slow) axis of the plate to be measured parallel to the pass axis of the polarizer, the plate to be measured is rotated by 450 counterclockwisly. A stepping motor is used to rotate the analyzer. The experimental data are collected by a photodetector and then sent to a computer. According to the output data curve, the phase retardation and optic axis of the plate to be measured can be obtained simultaneously. To test the feasibility of the method, a λ /2 and a λ /8 wave plates are used as examples to demonstrate the measurement procedures. The phase retardation measurement accuracy is better than 0.5×10-2. This method can be used to measure the arbitrary phase retardation conveniently.
基金Projects(61533021,61321003,61273185)supported by the National Natural Science Foundation of ChinaProject(2015CX007)supported by the Innovation-driven Plan in Central South University,ChinaProject(13JJ8003)supported by the Joint Fund of Hunan Provincial Natural Science Foundation of China
文摘Reagents are optimized for the simultaneous determination of trace amounts of Cu^(2+), Cd^(2+) and Co^(2+) in zinc sulfate solution, which contains an extremely large excess of Zn^(2+). First, the reagents and their doses for the experiment are selected according to the characteristics of the zinc sulfate solution. Then, the reagent doses are optimized by analyzing the influence of reagent dose on the polarographic parameters(i.e. half-wave potential E_(1/2) and limiting diffusion current I_p). Finally, the optimization results are verified by simultaneously determining trace amounts of Cu^(2+), Cd^(2+) and Co^(2+) in the presence of an extremely large excess of Zn^(2+). The determination results indicate that the optimized reagents exhibit wide linearity, low detection limits, high accuracy and good precision for the simultaneous determination of trace amounts of Cu^(2+), Cd^(2+) and Co^(2+) in the presence of an extremely large excess of Zn^(2+).
