含水物质红外光谱测试的样品制备

介绍了含水物质红外光谱测试中常用的样品制备技术 ,包括结晶压片法、吸附压片法、蒸发涂片法、蒸发成膜法。

生物质能发电厂烟气余热回收技术应用与效益

文章根据湖南省内生物质能发电厂的实际情况,阐述了生物质燃料含水量对发电效益的影响,降低生物质燃料的含水率是提高发电效益的重要途径之一。通过回收发电厂排放的烟气余热,利用低品位的能源,将生物质燃料的含水量干燥至25%左右,大大提高了发电厂的经济效益。

DGJ-10A型冷冻真空干燥机

冷冻真空干燥机是将含水物质或溶液预先冻结,然后在高真空下升华而得到干燥制品。经冷冻干燥的物质,原有的化学、生理性能不变,容易保存,加水后可以还原,故广泛用于化学工业、制药工业、食品工业,特别适用于对热敏感的生物制品,如抗菌素、疫苗、血液制品、酶类、激素等其他生物化学制品。

确定水驱油藏水侵量的简易新方法

目前已有的计算水驱油藏水侵量的方法大多比较复杂，为了准确、简便地预测水驱油田水侵量，通过对水驱油藏水驱规律特征和水侵量计算方法的研究，结合目前的生产动态资料，基于甲型、乙型、丙型和丁型4种常用水驱特征曲线，利用Welge方程推导出油田油水渗流特征关系，再结合水侵量的物质平衡原理，建立了计算水驱油田水侵量的新模型。新方法不需要对水体的形态及大小作出任何假设，且计算所需参数容易获取。通过实例计算表明，新方法计算过程简便，计算结果准确，实用性强。

Chemical and Organic Contamination of Phreatic Aquifer of Sidi Bouzid （Center West of Tunisia）

An understanding of the long-term changes in the nitrate and microbial contamination pattern of the groundwater of Sidi Bouzid （Centre West of Tunisia） is critical to conservation of drinking water in rural areas supporting mixed land-use activities such as cropping, livestock farming, and residence. The phreatic aquifer was revealed polluted by domestic disposals of the wastewaters in the urban zone. The average nitrate concentration in the groundwater of the east of the mioplioquaternary aquifer of Saddaguia （Sidi Bouzid） rose from 50 mg NO3- during 1996 to over 100 mg in 2003, which represents an increase of some 10 mg per year. Nitrate groundwater pollution during the period 1996-2003 was the result of the abusive use of fertilizers.In the cultivated zone, we must reduce the effects of the excessive use of the nitrogen fertilizers on the basis of monitoring soil once a year, managing water resources, rationalizing the use of the chemical substances. In urban zones, most of lost wells located in the perimeter reveal the gravity of the state of the aquifer. This last is organically polluted and requires an immediate action for the generalization of the purification network. We need to take into account the reality of under soil in all future planning＇s and arrangements. A scheme of sanitation seems necessary before all plans of arrangement. The extension of the sewer network must give the priority to the most vulnerable zones.

Reflux-synthesized bulk and diluted W-Nb-O mixed oxide bronzes for the valorization of short-chain oxygenates aqueous mixtures

This work reports the preparation of bulk and KIT-6-diluted W-Nb-O mixed oxide bronzes by a reflux method. The influence of the incorporation of Nb and a mesoporous silica on the physicochemical features of the catalysts is studied. The addition of Nb favors the formation of single-phase oxide bronze structure, with improved Lewis acidity;while the incorporation of KIT-6 gives rise to well-dispersed mixed metal oxide particles on the diluter. These diluted W-Nb-O catalysts present enhanced surface areas and mesopore volumes. The materials have been tested in the valorization of an aqueous model mixture (acetol/propanal/ethanol/acetic acid/water weight ratio of 5/25/10/30/30), through C-C bond formation reactions. The increase in the Lewis nature of surface acid sites stands as the key point to maximize the total organic yield during the reaction (C5-C10 products). The best catalysts maintain their catalytic behavior after five consecutive uses.

差频式水份测定仪的探讨

本文探讨了差频式物质含水量测定仪的基本原理，期望能快速准确测定各种物质如：粮食、酒类、食品、烟草及各种中医药材等的含水量。

Analysis of Tuber Yield- and Maturity- Related Traits in Water Yam （Dioscorea alata L.）

Inadequate yield potential of available varieties and their long growth periods are two of the factors limiting yam （Dioscorea spp.） production. Identifying yield- and maturity-related traits and breeding for them will enhance production. Ten morphological/physiological traits： time of shoot emergence, time of tuber initiation, plant height, shoot dry weight, time of shoot senescence, tuber fresh weight （tuber yield）, tuber number/plant, tuber parenchyma colour, tuber dry matter content and tuber dormancy period were assessed in eight accessions of D. alata L. （water yam） on the field in 2008 and 2009. Tuber yield-related traits were identified as shoot dry weight and time of shoot emergence. Shoot dry weight had the strongest positive effect; time of shoot emergence had a negative effect. High yielding accessions had a high shoot dry weight, but were low in tuber dry matter content. Uniform tuber parenchyma colour was the sole trait related to tuber maturity, but early and late senescing accessions did not consistently differ in the trait. TDa 00/00103 is high yielding and early maturing and may be used as a parent for breeding for high yield and early maturity in D. alata.

STUDY ON SIDE REACTION IN THE SYNTHESIS OF HYPERCROSSLINKED POLYMERS

The systematical study about side reactions have revealed the formation mechanism of oxygen-containing groups of hypercrosslinked polymers. Surface chemistry and functionality of the polymers are characterized by Fourier-transform infrared spectroscopy (FT-IR), solid state nuclear magnetic resonance (NMR) and contact angle. The results showed that the ether groups were from chloromethylated reaction, and the alcohol groups arose from partial hydrolysis of chloromethyl groups during the post-crosslinking reaction, and the carbonyl functionality was formed by further oxidation of the alcohol groups. Catalyst and solvent used in the postcrosslinking reaction would greatly influence the surface chemistry of the polymer.

Valorization of the Use of Calcareous Tuff and Dune Sand in Saharan Road Design

This research objective is to propose a co-valorization of powdered tuff, containing a slight amount of clay and dune sand, by mixing the two substances at different rates such as 0%, 5%, 15%, 25% and 35% of sand. The adapted criteria formulas are those recommended by the technical Saharan road. The results of the proposed study showed that ＂tuff-sand＂ mixtures are denser with a lower optimum water content modified proctor, the fine rate decreases together with the plasticity index, whereas the bearing index （CBR： California bearing ratio test） increases. The intrinsic characteristics, cohesion and sensitivity of mixtures with respect to compactness are almost identical to those oftuffwithout addition. The optimal adapted sand incorporation rate is estimated at 25% at 96% of compactness. Under these conditions, the amount of fines decreases from 40% to an acceptable level of 25% and the plasticity index from 16.2 to 12. The compaction water content decreases by 36% and the CBR （bearing index） increases by 30% and the compressive strength and sensitivity, according to compactness, of the elaborated material are almost identical to those oftuffwithout addition.

Nutritional Analysis of Fast Food in Streets of Patna Town, Bihar

Mushroom growth of street fast food is a boon for changing lifestyle of urban people. However, its nutritional aspect is also a matter of concern. The objective of the present study was hence to assess the nutrient components of fast food sold in streets of Patna town. A total of 30 fast food samples from streets were collected from different locations of Patna town in aseptic containers and immediately transferred to the laboratory for proximate analysis. Descriptive statistics was used to analyze the collected data. In terms of nutrient contribution, the highest energy content was found in Hot potato chips （536 ~ 85.2 kcal /I00 g） followed by Chicken chawmin （527 ~ 253.08 kcal/plat）, Chilli chicken （464 ~ 91.8 kcal/plat） and Pav bhaji （425 -4- 164 kcal/plat）. Highest level of protein was detected in Chilli chicken at 27.3 ~ 5.01 g per serving. Protein of Chilli chicken supplied approximately 29% of the total energy content per serving. Maximum amount of fat was also found in Chilli ckicken （35.5 ~ 31.89 g/plat）. Total fat contribution of Chilli ckicken to the total energy per serving found to be approximately 67%. Highest level of carbohydrate was detected in Idli at 15.0 ~ 9.18 g per serving of sample which contributed approximately 91% of the total energy content per serving. From this study it was concluded that street fast foods provide an appreciable amount of recommended nutrient composition. It could be observed in this study that street fast foods supply appreciable amount of nutrients and calories to the people of Patna.

Macronutrient Composition and Digestibility of Extruded and Fermented Soya Protein Products

The macronutrient composition and in vitro protein digestibility of extruded fermented and unfermented extruded soya protein products （low, medium and high moisture）, raw and fermented soya meal and soya kernel were studied. The protein content （g/100g soya dry weight） ranged from 38.20 to 62.98 with the highest content in the high moisture extruded protein product fermented with 5 mL inoculum of Bacillus natto. Contents of carbohydrates ranged from 14.77 to 29.08 while those of crude fibre, fat and ash were generally low. Fermentation better improved protein digestibility in the raw soya meal and kernel than in the unfermented extruded and extruded fermented products. SDS-PAGE electrophoresis revealed some degradation of the protein sub units of fermented samples.

The Influence of the ＂Terroir＂ Concerning the Quantity and Quality of Grapes Yield at White Grapevine Varieties Growing in the lasi Vineyard

Abstract： Romania is famous of the potential of his vineyard, winemaking is a traditional occupation, in fact it can be said that there are many areas that can provide a vineyard product. Moreover, typicity and authenticity of a wine are defining conditions under conditions of fierce intemational competition to guarantee success of wine. There were concerns for determining areas with designation of origin from a vineyard that will produce quality wines, but the purpose of this study is to delimit the level of a vineyard small area that can ensure the achievement of a certain type of wine, a quality required by consumers. The research was made during 2006-2008 and revealed that the production of quality grapes and are influenced by different factors such as genetic, environmental and technological acting in complex. This is a first attempt to study characterize the concept of ＂terroir＂, as applied in the Copou vineyard from lasi county and provides information on the behavior of two varieties of grapes for wine： Feteasca Regala and Muscat Ottonel. Depending on the purpose, observations and calculations have found the influence of soil characteristics on several biochemical parameters and productive at varieties of Feteasca Regala and Muscat Ottonel （soluble carbohydrate content, total acidity, the average yield of grapes） for the purpose of knowledge than a more detailed wine center in northeast of Romania. The results of this study can be used to determine with precision small areas crop at the parcel that will produce quality wines.

Production and Quality Evaluation of Pringles from Composite Flour of Cocoyam and Wheat Flour

Work assessed ＂Pringles＂ as an imitate snack produced from composite flour of cocoyam and wheat. This was carried out in order to exploit the nutritional and aesthetic value of cocoyam （Colocasia escullenta Vat.） to improve the overall quality of the Pringles as against its production from potato and wheat composite flour. Composite flour （100%：0%, 90%：10%, 80%：20%, 70%：30%, 60%：40% and 50%：50%） of cocoyam and wheat respectively as the major raw materials were adopted and used for the production of the Pringles. Physicochemical analysis （pH, water absorption capacity （WAC）, bulk density （BD） and swelling capacity （SC））; proximate analysis （protein, fats, ash, moisture and carbohydrate content） and sensory evaluation （colour, texture, taste and overall acceptability） were carried out on the samples produced using standard methods. Physicochemical analysis showed the pH of 5.48 to 6.61, WAC （12.00 to 17.50）, BD （1.43 to 1.56） and SW （1.03 to 1.38）. However, sample with 10% cocoyam and 90% wheat composite flour gave the best physicochemical properties of pH （5.98）, WAC （14.00）, BD （1.56） and SC （1.38）. The proximate analysis showed that carbohydrate content ranging between 53.36 to 61.12, and protein content （8.17 to 12.29）, fat content （16.67 to 23.97）, ash content （3.49 to 45.53）, fiber content （1.71 to 2.83） and moisture content （8.76 to 14.54）. Sample B equally gave the nutrient proximate combination of appreciable percentage on the average. The result of the sensory evaluation showed that there is no significant difference between the samples produced in terms of aroma. There is a significant different between samples A, B and the remaining samples in terms of colour and taste. On the overall acceptability, samples A, C and D showed no significant difference but the highest mean score was found with sample B. Conclusively, acceptable snack （Pringles） can be produced from cocoyam and wheat in ratio 90%： 10%, respectively.

The Importance of Consuming Charales （Chirostomajordani） for Human Nutrition

The diversity of existing food may decrease malnutrition through the consumption of underutilized species. In Mexico, the ＂charal＂ fish Chirostoma spp. is grouped in five species： Chirostoma grandocule, Chirostoma patzcuaro, Chirostoma humboltianum, Chirostoma attenuatum and Chirostomajordani which live in lakes in the country, and they are not consumed or their demand is low The objective of this research was to analyze the macronutrients of Chirostomajordani charal and inform population their nutritional value to increase human nutrition. Sampling was provided at Xochimilco channels in Xochimilco, D.F., summer and winter seasons at 2009. Fish （200 g） were maintained in channels water for proximal analysis according AOAC methods （1995）. The results in dry bases were： protein 74.36%, lipids 1.24%, fiber 0.27%, minerals 4.9%, and soluble carbohydrates 19.23%. This fish grants protein, plastic material essential for human development： its lipid and carbohydrate contents, sources of energy, are low; however, the excess of disseminated proteins increase the energy sources. Fiber is found in a minimum amount. Dehydrated charales may be stored without refrigeration up to 3 months, maintaining their nutritional value. Consumption of the charal should be considered in the basic diet for its nutritional properties, to diminish malnutrition in the Mexico and other countries.

Effects of Nitrogen Sources on Nitrate Reductase Activity and Some Physiological Parameters in Psyllium （Plantago ovata F.） under Salinity Stress

The effects of three nitrogen sources （ammonium, nitrate and ammonium＋nitrate） and three salt treatments （0, 100 and 200 mM NaCl） on nitrate reductase activity, proline, soluble protein and carbohydrate contents in psylliom （Plantago ovata） plants were Studied. The nitrate reductase activity tended to increase when NO3- was included in the root-zone solution, but decrease as salinity increased. All N sources stimulated plant growth and nutrient uptake. Shoot and root dry matter tended to decrease as salinity increased, but less so when both NH4＋ and NO3- were present. Shoot biomass accumulated to significantly greater quantities under the mixed-N treatments than when produced using either NH4＋ or NO3- N-form alone. Although not statistically significant, the root biomasses showed a similar tendency. Generally, leaf proline and soluble shoot carbohydrate contents increased with increasing salinity in contrast to soluble protein which decreased regardless of the N source. Under salinity conditions, the concentration of Na＋ in shoot and root tissues was highest in ammonium-N treatment, while that of K＋ was highest in the mixed-N treatment.