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ICP-AES法检验含金基体多元素混合标准溶液的均匀性 被引量:4
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作者 李桂华 张凤霞 +2 位作者 刘化峰 黄准 祝培明 《贵金属》 CAS CSCD 北大核心 2015年第3期55-59,66,共6页
为了消除黄金基体对部分被测(杂质)元素产生的干扰与抑制作用,采用基体匹配法,配制了含金基体混合多元素标准溶液。用ICP-AES法对该含金基体溶液中的Ag、Cu、Fe、Zn元素进行了均匀性检验。采用F和t检验法联用统计处理数据对该溶液进行... 为了消除黄金基体对部分被测(杂质)元素产生的干扰与抑制作用,采用基体匹配法,配制了含金基体混合多元素标准溶液。用ICP-AES法对该含金基体溶液中的Ag、Cu、Fe、Zn元素进行了均匀性检验。采用F和t检验法联用统计处理数据对该溶液进行了均匀性评价。检验结果表明瓶间和瓶内的均值和方差不存在显著性差异,证明该含金基体混合多元素标准溶液是均匀的。 展开更多
关键词 分析化学 含金基体 F检验法 t检验法 均匀性
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Comparing potentials for gas outburst in a Chinese anthracite and an Australian bituminous coal mine 被引量:8
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作者 Li Guoqing Saghafi Abouna 《International Journal of Mining Science and Technology》 SCIE EI 2014年第3期391-396,共6页
Gas outbursts in underground mining occur under conditions of high gas desorption rate and gas content,combined with high stress regime, low coal strength and high Young's modulus. This combination of gas and stre... Gas outbursts in underground mining occur under conditions of high gas desorption rate and gas content,combined with high stress regime, low coal strength and high Young's modulus. This combination of gas and stress factors occurs more often in deep mining. Hence, as the depth of mining increases, the potential for outburst increases. This study proposes a conceptual model to evaluate outburst potential in terms of an outburst indicator. The model was used to evaluate the potential for gas outburst in two mines, by comparing numerical simulations of gas flow behavior under typical stress regimes in an Australian gassy mine extracting a medium-volatile bituminous coal, and a Chinese gassy coal mine in Qinshui Basin(Shanxi province) extracting anthracite coal. We coupled the stress simulation program(FLAC3D) with the gas simulation program(SIMED II) to compute the stress and gas pressure and gas content distribution following development of a roadway into the targeted coal seams. The data from gas content and stress distribution were then used to quantify the intensity of energy release in the event of an outburst. 展开更多
关键词 Coal OUTBURST Gas content PERMEABILITY Stress Energy
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Determination of Selected Toxic Elements in Apples from Organic Farming 被引量:1
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作者 Michaela Zeiner Iva Juranovic Cindric +1 位作者 Ivona Krizman Gerhard Stingeder 《Journal of Chemistry and Chemical Engineering》 2011年第7期577-582,共6页
Due to the elevated ecological awareness nowadays the consumption of products of organic agriculture is increasing. Organic farming means excluding the use of synthetic inputs, such as synthetic fertilizers and pestic... Due to the elevated ecological awareness nowadays the consumption of products of organic agriculture is increasing. Organic farming means excluding the use of synthetic inputs, such as synthetic fertilizers and pesticides or genetically modified organisms, but there are only a few regulations regarding heavy metal concentrations in soils. Thus a not negligible uptake of metals from the soil where the apple trees are grown may occur. Furthermore inorganic copper compounds being traditional fertilizers for apple trees are not considered as synthetic fertilizers, thus they are still used in organic apple farming for soil or foliar application. Thus also apples produced by organic agriculture may contain toxic elements, such as cadmium, chromium, copper, and lead. The concentrations of these elements were determined in whole apples, as well as in the flesh and peel in order to estimate the possible risk for human health. Prior to analysis using ICP-AES samples underwent a microwave assisted digestion. The LODs obtained are below the recommended maximum levels in vegetables/fruits by WHO. In all samples no Cu, Cr, and Pb could be detected. Only Ca was found in the peel of about a third of samples investigated in concentrations between LOD and LOQ (1-3 μg/g). 展开更多
关键词 Apples CADMIUM CHROMIUM copper LEAD organic farming.
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