Poly(p-phenylene terephthalamide)(PPTA)pulp was prepared by polycondensation of the p-phenylene diamine(PPDA)with terephthaloyl chloride(TPC)in the completely anhydrous solvent system of N-methyl pyrrolidone(NMP)havin...Poly(p-phenylene terephthalamide)(PPTA)pulp was prepared by polycondensation of the p-phenylene diamine(PPDA)with terephthaloyl chloride(TPC)in the completely anhydrous solvent system of N-methyl pyrrolidone(NMP)having calcium chloride,in the presence of poly(vinyl pyrrolidone)(PVP)having a viscosity average molecular weight lower than 40 000.It was confirmed that the polycondensation could be accelerated,the inherent viscosity of the polymer could be increased,and the polymers could be fibrillated more easily by the addition of the PVP.FTIR and X-ray spectra proved that PVP had not combined into molecular chains of the resultant PPTA pulps.The morphology of the resultant pulps,the effect of viscosity average molecular weight,amount and adding mode of PVP on inherent viscosity,specific surface area,and mean length of the resultant pulps were discussed in detail.And the friction and wear properties of the compound reinforced by the resultant pulps were simply investigated.展开更多
This paper presents the study of vibration in each element of hard disk drive, especially the resonance of the actuator arm. The resonance occurs in hard disk drive is considered as one of the quality controlled param...This paper presents the study of vibration in each element of hard disk drive, especially the resonance of the actuator arm. The resonance occurs in hard disk drive is considered as one of the quality controlled parameter. The main purpose of the research is to investigate the relationship between the pivot bearing assembly process and the natural frequency of the actuator arm. The experiment is designed using the information from the hard disk drive manufacturer. The selected pivot bearing assembly process parameters have been controlled. The modal analysis of the assembled actuator arms has been done. The experiment results show the relationship of the specific process parameters and some of the actuator arm＇s modal frequency. The results also show that the affected vibration mode is the torsion mode only.展开更多
文摘Poly(p-phenylene terephthalamide)(PPTA)pulp was prepared by polycondensation of the p-phenylene diamine(PPDA)with terephthaloyl chloride(TPC)in the completely anhydrous solvent system of N-methyl pyrrolidone(NMP)having calcium chloride,in the presence of poly(vinyl pyrrolidone)(PVP)having a viscosity average molecular weight lower than 40 000.It was confirmed that the polycondensation could be accelerated,the inherent viscosity of the polymer could be increased,and the polymers could be fibrillated more easily by the addition of the PVP.FTIR and X-ray spectra proved that PVP had not combined into molecular chains of the resultant PPTA pulps.The morphology of the resultant pulps,the effect of viscosity average molecular weight,amount and adding mode of PVP on inherent viscosity,specific surface area,and mean length of the resultant pulps were discussed in detail.And the friction and wear properties of the compound reinforced by the resultant pulps were simply investigated.
文摘This paper presents the study of vibration in each element of hard disk drive, especially the resonance of the actuator arm. The resonance occurs in hard disk drive is considered as one of the quality controlled parameter. The main purpose of the research is to investigate the relationship between the pivot bearing assembly process and the natural frequency of the actuator arm. The experiment is designed using the information from the hard disk drive manufacturer. The selected pivot bearing assembly process parameters have been controlled. The modal analysis of the assembled actuator arms has been done. The experiment results show the relationship of the specific process parameters and some of the actuator arm＇s modal frequency. The results also show that the affected vibration mode is the torsion mode only.
