The vibration pretreatment-microwave curing process is an efficient,low energy consumption,and high-quality out-of-autoclave curing process for carbon fiber resin matrix composites.This study aims to investigate the i...The vibration pretreatment-microwave curing process is an efficient,low energy consumption,and high-quality out-of-autoclave curing process for carbon fiber resin matrix composites.This study aims to investigate the impact of vibration pretreatment temperature on the fiber weight content,microscopic morphology and mechanical properties of the composite laminates by using optical digital microscopy,universal tensile testing machine and thermo-gravimetric analyzer.Additionally,the combined mode of Bragg fiber grating sensor and temperature measurement fiber was employed to explore the effect of vibration pretreatment on the strain process during microwave curing.The study results revealed that the change in vibration pretreatment temperature had a slight impact on the fiber weight content when the vibration acceleration remained constant.The metallographic and interlaminar strength of the specimen formed at a vibration pretreatment temperature of 80℃ demonstrated a porosity of 0.414% and a 10.69% decrease in interlaminar shear strength compared to autoclave curing.Moreover,the introduction of the vibration energy field during the microwave curing process led to a significant reduction in residual strain in both the 0°and 90°fiber directions,when the laminate was cooled to 60℃.展开更多
The diversity of interface morphologies is observed for directionally solidified Sn-0.65%Cd alloy under a travelling magnetic field (TMF) in the 4 mm-diameter sample. Under an upward TMF, planar and cellular interfa...The diversity of interface morphologies is observed for directionally solidified Sn-0.65%Cd alloy under a travelling magnetic field (TMF) in the 4 mm-diameter sample. Under an upward TMF, planar and cellular interface morphologies transform alternately with increasing magnetic flux density (B≤10.3 mT). The interface morphology transforms from shallow cellular to deep cellular morphology under a weak downward TMF (B=3.2 mT). When the magnetic flux density increases further, both sides of the interface morphology appear to be slightly inconsistent, but they roughly tend to be planar under a strong downward TMF (BS10.3 mT). The interface instability may be attributed to the flow driven by the TMF. Moreover, the shape of interface appears to be almost flat under an upward TMF, but deflective under a downward TMF.展开更多
MEMS gyroscope is a new inertial navigation sensor,which can measure the input angular rate of sensitive axis using Coriolis effect.Compared to the conventional gyroscope,it owns many unique advantages.A novel structu...MEMS gyroscope is a new inertial navigation sensor,which can measure the input angular rate of sensitive axis using Coriolis effect.Compared to the conventional gyroscope,it owns many unique advantages.A novel structure of vibrating ring gyroscope is proposed and the finite element model of the oscillator is established based on MEMS technology.Through the modal analysis,the natural frequency and mode shapes of the oscillator are obtained.By analyzing the effects of the structural parameters on the mode shapes and frequency of the harmonic oscillator,the optimal design parameters are got.The frequency difference between the operating mode and the other modes is greater than 1kHz after optimization,which can avoid the frequency coupling of the operating mode and other vibrating modes of the oscillator.The simulation results show that the performance parameters of the ring structure meet the design requirements and have obvious advantages.展开更多
In order to reduce the oxidation and volatilization caused by Mg element in the traditional methods for synthesizing Mg2Si compounds,Mg2Si thermoelectric materials were prepared by solid state reaction and microwave r...In order to reduce the oxidation and volatilization caused by Mg element in the traditional methods for synthesizing Mg2Si compounds,Mg2Si thermoelectric materials were prepared by solid state reaction and microwave radiation techniques.Structure and phase composition of the materials were investigated by X-ray diffraction.The electrical conductivity,Seebeck coefficient and thermal conductivity were measured as a function of temperature from 300 to 700 K.It is found that high purity Mg2Si powders can be obtained with excessive content of 8% Mg from the stoichiometric Mg2Si at 853 K and 2.5 kW for 30 min.A maximum dimensionless figure of merit,ZT,of about 0.13 was obtained for Mg2Si at 600 K.展开更多
Aim To investigate the effects of the incident orientation on the microwave attenuation. Methods Attenuation allowing microwave signal transmitting in an oblique or vertical direction through the solid propellant ex...Aim To investigate the effects of the incident orientation on the microwave attenuation. Methods Attenuation allowing microwave signal transmitting in an oblique or vertical direction through the solid propellant exhaust plume was computed, and the experiments were performed utilizing a lab scale solid rocket motor with a fully expanded nozzle. Results The predicted results accord well with the experimental results. Conclusion The microwave attenuation in the oblique path is greater than that in the vertical path.展开更多
Array acoustic logging plays an important role in formation evaluation. Its data is a non-linear and non-stationary signal and array acoustic logging signals have time-varying spectrum characteristics. Traditional fil...Array acoustic logging plays an important role in formation evaluation. Its data is a non-linear and non-stationary signal and array acoustic logging signals have time-varying spectrum characteristics. Traditional filtering methods are inadequate. We introduce a Hilbert- Huang transform (HHT) which makes full preservation of the non-linear and non-stationary characteristics and has great advantages in the acoustic signal filtering. Using the empirical mode decomposition (EMD) method, the acoustic log waveforms can be decomposed into a finite and often small number of intrinsic mode functions (IMF). The results of applying HHT to real array acoustic logging signal filtering and de-noising are presented to illustrate the efficiency and power of this new method.展开更多
The influence of melt convection on dendrite growth during the upward-directional solidification of Pb-33%Sn binary alloys was investigated.The melt convection was modulated by traveling magnetic field.When the direct...The influence of melt convection on dendrite growth during the upward-directional solidification of Pb-33%Sn binary alloys was investigated.The melt convection was modulated by traveling magnetic field.When the direction of traveling magnetic field was changed from upward to downward,the primary dendrite spacing gradually increased,and the distribution peak of the primary dendrite spacing shifted to the field of narrower spacing.These result from the different intensities of melt convection,which are controlled by the traveling magnetic field.The effects of the traveling magnetic field on melt convection are similar to those of adjustment in the gravity level,thus,the primary dendrite spacing varies.When the intensity of the traveling magnetic field was 1 mT,and the drawing speed was 50 μm/s,the gravity acceleration reached 0.22g for the downward-traveling magnetic field and 3.07g for the upward-traveling magnetic field.展开更多
Aim To prepare triamcinolone-acetonide-acetate (TAA)-loaded solid lipidnanoparticles (SLN) carbomer gel with tripalmitin glyceride (TPG), and investigate theircharacteristics and transdermal drug delivery. Methods SLN...Aim To prepare triamcinolone-acetonide-acetate (TAA)-loaded solid lipidnanoparticles (SLN) carbomer gel with tripalmitin glyceride (TPG), and investigate theircharacteristics and transdermal drug delivery. Methods SLN suspension was prepared by high-pressurehomogenization technique, and then mixed with carbomer gel matrix to get SLN gel. The morphology,particle size with polydispersi-ty index (PI) and zeta potential were examined by atomic forcemicroscopy (AFM) and photon correlation spectroscopy (PCS). The entrapment efficiency, stability andin vitro drug release were also studied. The transdermal drug delivery through porcine ear skin wasevaluated using modified Franz diffusion cells. Results The SLN had a spherical shape with theaverage size of (95.5 - 186.2) nm, the zeta potential of (-26.3- -15.7) mV and the entrapmentefficiency of 67.4%-90.3% for different TAA encapsulated compounds. TAA-SLN carbomer gel had goodstability, the release profile in vitro fitted Higuchi equation. In comparison with conventionalhydrogels, TAA-SLN carbomer gel resulted in higher drug permeation amount and drug deposition withinporcine ear skin after 24 h penetration experiment. Conclusion TAA-SLN carbomer gel is preparedwith stable physicochemical properties. The release profile and improved drug permeation into skinmake it be a promising vehicle for transdermal drug delivery.展开更多
Carbon fiber reinforced plastics provide many excellent properties and are widely used in the aerospace industry.However,the existing composites autoclave process still faces difficulties such as high-energy consumpti...Carbon fiber reinforced plastics provide many excellent properties and are widely used in the aerospace industry.However,the existing composites autoclave process still faces difficulties such as high-energy consumption,uneven distribution of temperature field,complications of pressure transmission,and high cost,which limit their application in manufacturing of large complex composites components.In this study,the vibration treatment was introduced into the composites microwave curing process innovatively.On the basis of giving full play to the uniform heating characteristics of the microwave,the problems of a large number of internal defects and poor molding quality caused by the insufficient curing pressure have been solved.The results showed that the samples cured by the improved microwave process without external pressure had a few internal voids,excellent interface bonding conditions,and lower residual stress.Their properties were almost consistent with the samples prepared by the standard autoclave process,which provided a new method for the high-performance,efficient,safe,and low-cost manufacturing of large complex composites components.展开更多
Through the simulation of explicit dynamic analysis software LS-DYNA,made an analysis to the particle velocity and the stress distribution of surrounding rock when the explosives blasting.Explicated the mechanical cha...Through the simulation of explicit dynamic analysis software LS-DYNA,made an analysis to the particle velocity and the stress distribution of surrounding rock when the explosives blasting.Explicated the mechanical character of surrounding rock in the foun- dation pit blasting,provided a basis to set of blasting parameters and optimized the blast- ing construction.展开更多
A high power dual-wavelength Ti:sapphire laser system with wide turning range and high efficiency is described, which consists of two prism-dispersed resonators pumped by an a11-solid-state frequency-doubled Nd:YAG ...A high power dual-wavelength Ti:sapphire laser system with wide turning range and high efficiency is described, which consists of two prism-dispersed resonators pumped by an a11-solid-state frequency-doubled Nd:YAG laser. Tunable dual-wavelength outputs, with one wavelength range from 750nm to 795nm and the other from 80Ohm to 850nm, have been demonstrated. With a pump power of 23 W at 532nm, a repetition rate of 6.5kHz and a pulse width of 67.6ns, the maximum dual-wavelength output power of 5.6 W at 785.3nm and 812.1 run, with a pulse width of 17.2ns and a line width of 2nm, has been achieved, leading to an optical-to-optical conversion efficiency of 24.4%.展开更多
It has been shown that much dynamic information is hidden in the pressure fluctuation signals of a gas-solid fluidized bed. Unfortunately, due to the random and capricious nature of this signal, it is hard to realize ...It has been shown that much dynamic information is hidden in the pressure fluctuation signals of a gas-solid fluidized bed. Unfortunately, due to the random and capricious nature of this signal, it is hard to realize reliable analysis using traditional signal processing methods such as statistical analysis or spectral analysis, which is done in Fourier domain. Information in different frequency band can be extracted by using wavelet analysis. On the evidence of the composition of the pressure fluctuation signals, energy of low frequency (ELF) is proposed to show the transition of fluidized regimes from bubbling fluidization to turbulent fluidization. Plots are presented to describe the fluidized bed's evolution to help identify the state of different flow regimes and provide a characteristic curve to identify the fluidized status effectively and reliably.展开更多
基金Projects(52175373,52005516)supported by the National Natural Science Foundation of ChinaProject(2018YFA0702800)supported by the National Key Basic Research Program,ChinaProject(ZZYJKT2021-03)supported by the State Key Laboratory of High Performance Complex Manufacturing,Central South University,China。
文摘The vibration pretreatment-microwave curing process is an efficient,low energy consumption,and high-quality out-of-autoclave curing process for carbon fiber resin matrix composites.This study aims to investigate the impact of vibration pretreatment temperature on the fiber weight content,microscopic morphology and mechanical properties of the composite laminates by using optical digital microscopy,universal tensile testing machine and thermo-gravimetric analyzer.Additionally,the combined mode of Bragg fiber grating sensor and temperature measurement fiber was employed to explore the effect of vibration pretreatment on the strain process during microwave curing.The study results revealed that the change in vibration pretreatment temperature had a slight impact on the fiber weight content when the vibration acceleration remained constant.The metallographic and interlaminar strength of the specimen formed at a vibration pretreatment temperature of 80℃ demonstrated a porosity of 0.414% and a 10.69% decrease in interlaminar shear strength compared to autoclave curing.Moreover,the introduction of the vibration energy field during the microwave curing process led to a significant reduction in residual strain in both the 0°and 90°fiber directions,when the laminate was cooled to 60℃.
基金Project(50774061) supported by the National Natural Science Foundation of ChinaProject(28-TP-2009) supported by the Research Fund of State Key Laboratory of Solidification Processing(NWPU),China
文摘The diversity of interface morphologies is observed for directionally solidified Sn-0.65%Cd alloy under a travelling magnetic field (TMF) in the 4 mm-diameter sample. Under an upward TMF, planar and cellular interface morphologies transform alternately with increasing magnetic flux density (B≤10.3 mT). The interface morphology transforms from shallow cellular to deep cellular morphology under a weak downward TMF (B=3.2 mT). When the magnetic flux density increases further, both sides of the interface morphology appear to be slightly inconsistent, but they roughly tend to be planar under a strong downward TMF (BS10.3 mT). The interface instability may be attributed to the flow driven by the TMF. Moreover, the shape of interface appears to be almost flat under an upward TMF, but deflective under a downward TMF.
文摘MEMS gyroscope is a new inertial navigation sensor,which can measure the input angular rate of sensitive axis using Coriolis effect.Compared to the conventional gyroscope,it owns many unique advantages.A novel structure of vibrating ring gyroscope is proposed and the finite element model of the oscillator is established based on MEMS technology.Through the modal analysis,the natural frequency and mode shapes of the oscillator are obtained.By analyzing the effects of the structural parameters on the mode shapes and frequency of the harmonic oscillator,the optimal design parameters are got.The frequency difference between the operating mode and the other modes is greater than 1kHz after optimization,which can avoid the frequency coupling of the operating mode and other vibrating modes of the oscillator.The simulation results show that the performance parameters of the ring structure meet the design requirements and have obvious advantages.
基金Project (2009BB4228) supported by the Natural Science Foundation Project of Chongqing Science and Technology Commission,ChinaProject (CK2010Z09) supported by the Research Foundation of Chongqing University of Science and Technology,China
文摘In order to reduce the oxidation and volatilization caused by Mg element in the traditional methods for synthesizing Mg2Si compounds,Mg2Si thermoelectric materials were prepared by solid state reaction and microwave radiation techniques.Structure and phase composition of the materials were investigated by X-ray diffraction.The electrical conductivity,Seebeck coefficient and thermal conductivity were measured as a function of temperature from 300 to 700 K.It is found that high purity Mg2Si powders can be obtained with excessive content of 8% Mg from the stoichiometric Mg2Si at 853 K and 2.5 kW for 30 min.A maximum dimensionless figure of merit,ZT,of about 0.13 was obtained for Mg2Si at 600 K.
文摘Aim To investigate the effects of the incident orientation on the microwave attenuation. Methods Attenuation allowing microwave signal transmitting in an oblique or vertical direction through the solid propellant exhaust plume was computed, and the experiments were performed utilizing a lab scale solid rocket motor with a fully expanded nozzle. Results The predicted results accord well with the experimental results. Conclusion The microwave attenuation in the oblique path is greater than that in the vertical path.
基金supported by National Natural Science Foundation of China(Grant No.40874059)the National Key Science Engineering Projects of the Ninth Five Year Plan([1999]1423)
文摘Array acoustic logging plays an important role in formation evaluation. Its data is a non-linear and non-stationary signal and array acoustic logging signals have time-varying spectrum characteristics. Traditional filtering methods are inadequate. We introduce a Hilbert- Huang transform (HHT) which makes full preservation of the non-linear and non-stationary characteristics and has great advantages in the acoustic signal filtering. Using the empirical mode decomposition (EMD) method, the acoustic log waveforms can be decomposed into a finite and often small number of intrinsic mode functions (IMF). The results of applying HHT to real array acoustic logging signal filtering and de-noising are presented to illustrate the efficiency and power of this new method.
基金Project(50827102)supported by the National Natural Science Foundation of ChinaProject(2010CB631202)supported by the National Basic Research Program of ChinaProject(28-TP-2009)supported by Research Fund of State Key Laboratory of Solidification Processing(NWPU),China
文摘The influence of melt convection on dendrite growth during the upward-directional solidification of Pb-33%Sn binary alloys was investigated.The melt convection was modulated by traveling magnetic field.When the direction of traveling magnetic field was changed from upward to downward,the primary dendrite spacing gradually increased,and the distribution peak of the primary dendrite spacing shifted to the field of narrower spacing.These result from the different intensities of melt convection,which are controlled by the traveling magnetic field.The effects of the traveling magnetic field on melt convection are similar to those of adjustment in the gravity level,thus,the primary dendrite spacing varies.When the intensity of the traveling magnetic field was 1 mT,and the drawing speed was 50 μm/s,the gravity acceleration reached 0.22g for the downward-traveling magnetic field and 3.07g for the upward-traveling magnetic field.
文摘Aim To prepare triamcinolone-acetonide-acetate (TAA)-loaded solid lipidnanoparticles (SLN) carbomer gel with tripalmitin glyceride (TPG), and investigate theircharacteristics and transdermal drug delivery. Methods SLN suspension was prepared by high-pressurehomogenization technique, and then mixed with carbomer gel matrix to get SLN gel. The morphology,particle size with polydispersi-ty index (PI) and zeta potential were examined by atomic forcemicroscopy (AFM) and photon correlation spectroscopy (PCS). The entrapment efficiency, stability andin vitro drug release were also studied. The transdermal drug delivery through porcine ear skin wasevaluated using modified Franz diffusion cells. Results The SLN had a spherical shape with theaverage size of (95.5 - 186.2) nm, the zeta potential of (-26.3- -15.7) mV and the entrapmentefficiency of 67.4%-90.3% for different TAA encapsulated compounds. TAA-SLN carbomer gel had goodstability, the release profile in vitro fitted Higuchi equation. In comparison with conventionalhydrogels, TAA-SLN carbomer gel resulted in higher drug permeation amount and drug deposition withinporcine ear skin after 24 h penetration experiment. Conclusion TAA-SLN carbomer gel is preparedwith stable physicochemical properties. The release profile and improved drug permeation into skinmake it be a promising vehicle for transdermal drug delivery.
基金Project(2018YFA0702800)supported by the National Key R&D Program of China。
文摘Carbon fiber reinforced plastics provide many excellent properties and are widely used in the aerospace industry.However,the existing composites autoclave process still faces difficulties such as high-energy consumption,uneven distribution of temperature field,complications of pressure transmission,and high cost,which limit their application in manufacturing of large complex composites components.In this study,the vibration treatment was introduced into the composites microwave curing process innovatively.On the basis of giving full play to the uniform heating characteristics of the microwave,the problems of a large number of internal defects and poor molding quality caused by the insufficient curing pressure have been solved.The results showed that the samples cured by the improved microwave process without external pressure had a few internal voids,excellent interface bonding conditions,and lower residual stress.Their properties were almost consistent with the samples prepared by the standard autoclave process,which provided a new method for the high-performance,efficient,safe,and low-cost manufacturing of large complex composites components.
文摘Through the simulation of explicit dynamic analysis software LS-DYNA,made an analysis to the particle velocity and the stress distribution of surrounding rock when the explosives blasting.Explicated the mechanical character of surrounding rock in the foun- dation pit blasting,provided a basis to set of blasting parameters and optimized the blast- ing construction.
基金Supported by the National Natural Science Foundation of China under Grant Nos 10474071, 60637010, 60671036 and 60278001, and the Tianjin Applied Fundamental Research Project under Grant No 07JCZDJC05900.
文摘A high power dual-wavelength Ti:sapphire laser system with wide turning range and high efficiency is described, which consists of two prism-dispersed resonators pumped by an a11-solid-state frequency-doubled Nd:YAG laser. Tunable dual-wavelength outputs, with one wavelength range from 750nm to 795nm and the other from 80Ohm to 850nm, have been demonstrated. With a pump power of 23 W at 532nm, a repetition rate of 6.5kHz and a pulse width of 67.6ns, the maximum dual-wavelength output power of 5.6 W at 785.3nm and 812.1 run, with a pulse width of 17.2ns and a line width of 2nm, has been achieved, leading to an optical-to-optical conversion efficiency of 24.4%.
文摘It has been shown that much dynamic information is hidden in the pressure fluctuation signals of a gas-solid fluidized bed. Unfortunately, due to the random and capricious nature of this signal, it is hard to realize reliable analysis using traditional signal processing methods such as statistical analysis or spectral analysis, which is done in Fourier domain. Information in different frequency band can be extracted by using wavelet analysis. On the evidence of the composition of the pressure fluctuation signals, energy of low frequency (ELF) is proposed to show the transition of fluidized regimes from bubbling fluidization to turbulent fluidization. Plots are presented to describe the fluidized bed's evolution to help identify the state of different flow regimes and provide a characteristic curve to identify the fluidized status effectively and reliably.