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土壤有机质测定的计算公式说明 被引量:1
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作者 马爱生 张英利 《高校实验室工作研究》 2003年第1期17-17,共1页
土壤有机质测定是土壤分析中最基本的项目之一。其原理是用一定浓度的重铬酸钾一硫酸溶液在加热恒温的条件下(170℃—180℃加热沸腾5分钟)氧化土壤有机质中的碳,剩余的重铬酸钾用硫酸严铁滴定,根据所消耗的硫酸亚铁量。
关键词 土壤有机质测定 计算公式 硫酸亚铁 高校 土壤农化分析 重铬酸钾 实验条件
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全自动土壤有机质测定仪的校准
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作者 何云馨 许爱华 +5 位作者 邱黛君 杨超妹 李锋丽 苗春园 郭波 隋峰 《分析仪器》 CAS 2023年第3期91-93,共3页
设计了一种全自动土壤有机质测定仪的计量溯源方法,主要包括温度控制部分的示值误差、温度场的均匀性、消解模块的计时误差、仪器示值误差和重复性5个项目。通过试验分析,当全自动土壤有机质测定仪的温度示值误差以及温场均匀性不大于&#... 设计了一种全自动土壤有机质测定仪的计量溯源方法,主要包括温度控制部分的示值误差、温度场的均匀性、消解模块的计时误差、仪器示值误差和重复性5个项目。通过试验分析,当全自动土壤有机质测定仪的温度示值误差以及温场均匀性不大于±2.0℃,消解计时误差不大于±2.0%,土壤有机质成分含量范围在小于10g/kg时,示值误差计算结果不大于0.5g/k;有机质含量在10g/kg与50g/kg之间时,示值误差不大于1.0g/kg;仪器的重复性不大于3%。通过对各个参数的评价,此校准方法可行有效。 展开更多
关键词 全自动土壤有机质测定 校准方法 计量
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基于有机分析仪器的土壤有机质快速测定方法研究
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作者 俞新培 《中文科技期刊数据库(全文版)自然科学》 2024年第2期0062-0065,共4页
土壤有机质的准确测定对于农业、环境和土壤科学等领域至关重要,随着科学技术的不断发展,传统有机质测定方法在速度、精确度、效率方面均有所不足。为满足现代农业和环境监测需求,需加强对土壤有机质快速测定方法的研究,基于此,本文将... 土壤有机质的准确测定对于农业、环境和土壤科学等领域至关重要,随着科学技术的不断发展,传统有机质测定方法在速度、精确度、效率方面均有所不足。为满足现代农业和环境监测需求,需加强对土壤有机质快速测定方法的研究,基于此,本文将简要介绍土壤有机质的作用、适用于土壤有机质快速测定的有机分析仪器,并从重铬酸钾容量法、红外光谱法、碱传导测定法、生物传感器法等几方面入手,探讨基于有机分析仪器的土壤有机质快速测定方法,旨在为相关从业人员提供参考。 展开更多
关键词 有机分析仪器 土壤有机质测定 检测方法
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Determination and Analysis of Soil Organic Matter Content in Greenhouses around Lhasa City
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作者 师亚飞 李晓颖 边吉 《Agricultural Science & Technology》 CAS 2017年第5期830-833,共4页
The soil organic matter content in the greenhouses around Lhasa City was determined by potassium dichromate-sulfuric acid digestion method. The results showed that the soil organic matter content differed among differ... The soil organic matter content in the greenhouses around Lhasa City was determined by potassium dichromate-sulfuric acid digestion method. The results showed that the soil organic matter content differed among different soil layers of the greenhouses around Lhasa City, and it was relatively low in the deep soil. The soil organic matter content also differed among greenhouses with different cultivation modes. In the same soil layer, the organic matter content in arched greenhouse was lower than that in semi-arched greenhouse. Among all the soil samples, the samples with organic matter content below the critical value (20 g/kg) accounted for 61.33%, and the samples with higher organic matter content (≥30 g/kg) accounted for 10.64%. The soil organic matter content in the greenhouses of different counties of Lhasa City ranked as Dazi County's〉Duilongdeqing County's〉Qushui County's. In overall, the organic matter content in the soil of greenhouses around Lhasa City was medium-low, and the fertility of the greenhouse soil was at the middle level. 展开更多
关键词 GREENHOUSE Lhasa City Soil organic matter DETERMINATION
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Refining Soil Organic Matter Determination by Loss-on-Ignition 被引量:15
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作者 M.H.SALEHI O.HASHEMI BENI +2 位作者 H.BEIGI HARCHEGANI I.ESFANDIARPOUR BORUJENI H.R.MOTAGHIAN 《Pedosphere》 SCIE CAS CSCD 2011年第4期473-482,共10页
Wet oxidation procedure,i.e.,Walkley-Black (WB) method,is a routine,relatively accurate,and popular method for the determination of soil organic matter (SOM) but it is time-consuming,costly and also has a high potenti... Wet oxidation procedure,i.e.,Walkley-Black (WB) method,is a routine,relatively accurate,and popular method for the determination of soil organic matter (SOM) but it is time-consuming,costly and also has a high potential to cause environmental pollution because of disposal of chromium and strong acids used in this analysis.Therefore,loss-on-ignition (LOI) procedure,a simple and cheap method for SOM estimation,which also avoids chromic acid wastes,deserves more attention.The aims of this research were to study the statistical relationships between SOM determined with the LOI (SOMLOI) and WB (SOMWB) methods to compare the spatial variability of SOM in two major plains,Shahrekord and Koohrang plains,of Chaharmahal-va-Bakhtiari Province,Iran.Fifty surface soil samples (0-25 cm) were randomly collected in each plain to determine SOM using the WB method and the LOI procedure at 300,360,400,500 and 550 ℃ for 2 h.The samples covered wide ranges of soil texture and calcium carbonate equivalent (CCE).The general linear form of the regression equation was calculated to estimate SOM LOI from SOM obtained by the WB method for both overall samples and individual plains.Forty soil samples were also randomly selected to compare the SOM and CCE before and after ignition at each temperature.Overall accuracy of the continuous maps generated for the LOI and WB methods was considered to determine the accordance of two procedures.Results showed a significant positive linear relationship between SOM LOI and SOM WB.Coefficients of determination (R2) of the equations for individual plains were higher than that of the overall equation.Coefficients of determination and line slopes decreased and root mean square error (RMSE) increased with increasing ignition temperature,which may be due to the mineral structural water loss and destruction of carbonates at higher temperatures.A temperature around 360 ℃ was identified as optimum as it burnt most organic carbon,destroyed less inorganic carbon,caused less clay structural water loss,and used less electrical energy.Although the trends of SOM in the kriged maps by the two procedures accorded well,low overall accuracy was observed for the maps obtained by the two methods.While not suitable for determination where high accuracy is required,determination of organic carbon through LOI is likely suitable for exploratory soil surveys where rough estimation of organic matter is required. 展开更多
关键词 calcium carbonate equivalent ignition temperature kriged maps spatial variability wet oxidation
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