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地安磷的气相色谱分析
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作者 叶文炳 陈忠敏 《农药科学与管理》 CAS 1993年第3期17-18,共2页
本文以邻苯二甲酸二(2-乙基)已酯为内标,使用3%XE60/上试102AW-DMCS-键合处理(80~100目)白色担体,玻璃柱,氢火焰离子化检测器,对地安磷进行分离和测定,能准确、快速、简便地测得地安磷含量.
关键词 地安磷 气相色谱 分析方法
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地安磷的气相色谱分析
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作者 张勤 《农药》 CAS 北大核心 1993年第5期26-26,45,共2页
地安磷系有机磷杀虫剂,其定量分析方法国内未见报道。国外文献用高压液相色谱法。本文报道了以DC-550为固定液,邻苯二甲酸二正己酯为内标物的气相色谱法,快速、准确,取得满意结果。 实验部分 一、仪器与试剂 1.仪器:SP-501 型气相色谱仪... 地安磷系有机磷杀虫剂,其定量分析方法国内未见报道。国外文献用高压液相色谱法。本文报道了以DC-550为固定液,邻苯二甲酸二正己酯为内标物的气相色谱法,快速、准确,取得满意结果。 实验部分 一、仪器与试剂 1.仪器:SP-501 型气相色谱仪,带氢火焰离子化检测器(山东省鲁南化工仪器厂);通用汉化色谱工作站(大连化学物理研究所)。 展开更多
关键词 地安磷 有机磷杀虫剂 气相色谱
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Investigation and characterization of mining subsidence in Kaiyang Phosphorus Mine 被引量:8
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作者 邓建 边利 《Journal of Central South University of Technology》 EI 2007年第3期413-417,共5页
In Kaiyang Phosphorus Mine, serious environmental and safety problems are caused by large scale mining activities in the past 40 years. These problems include mining subsidence, low recovery ratio, too much dead ore i... In Kaiyang Phosphorus Mine, serious environmental and safety problems are caused by large scale mining activities in the past 40 years. These problems include mining subsidence, low recovery ratio, too much dead ore in pillars, and pollution of phosphorus gypsum. Mining subsidence falls into four categories: curved ground and mesa, ground cracks and collapse hole, spalling and eboulement, slope slide and creeping. Measures to treat the mining subsidence were put forward: finding out and managing abandoned stopes, optimizing mining method (cut and fill mining method), selecting proper backfilling materials (phosphogypsum mixtures), avoiding disorder mining operation, and treating highway slopes. These investigations and engineering treatment methods are believed to be able to contribute to the safety extraction of ore and sustainable development in Kaiyang Phosphorus Mine. 展开更多
关键词 mining subsidence ground cracking safety Kaiyang Phosphorus Mine cut and fill mining method
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