Hardness of materials depends significantly on the indentation size and grain/sub-grain size via microindentation and nanoindentation tests of high-purity tungsten with different structures.The grain boundary effect a...Hardness of materials depends significantly on the indentation size and grain/sub-grain size via microindentation and nanoindentation tests of high-purity tungsten with different structures.The grain boundary effect and indentation size effect were explored.The indentation hardness was fitted using the Nix-Gao model by considering the scaling factor.The results show that the scaling factor is barely correlated with the grain/sub-grain size.The interaction between the plastically deformed zone(PDZ) boundary and the grain/sub-grain boundary is believed to be the reason that leads to an increase of the measured hardness at the specific depths.Results also indicate that the area of the PDZ is barely correlated with the grain/sub-grain size,and the indentation hardness starts to stabilize once the PDZ expands to the dimension of an individual grain/sub-grain.展开更多
To characterize the elastic-plastic properties of thin film materials on elastic-plastic substrates,a simple theory model was proposed,which included three steps:dimensionless analysis,finite element modeling and data...To characterize the elastic-plastic properties of thin film materials on elastic-plastic substrates,a simple theory model was proposed,which included three steps:dimensionless analysis,finite element modeling and data fitting.The dimensionless analysis was applied to deriving two preliminary nondimensional relationships of the material properties,and finite element modeling and data fitting were carried out to establish their explicit forms.Numerical indentation tests were carried out to examine the effectiveness of the proposed model and the good agreement shows that the proposed theory model can be applied in practice.展开更多
Mechanical properties of galvannealed (GA) steel sheet used for automotive exposed panel and predicted failure phenomenon of its coating layer were evaluated using finite element method. V-bending test was performed t...Mechanical properties of galvannealed (GA) steel sheet used for automotive exposed panel and predicted failure phenomenon of its coating layer were evaluated using finite element method. V-bending test was performed to understand better the fracture of coating layer of GA steel sheet during plastic deformation. Yield strength of the coating layer was calculated by using a relative difference between hardness of coating layer measured from the nano-indentation test and that of substrate. To measure shearing strength at the interface between substrate and coating layer, shearing test with two specimens attached by an adhesive was carried out. Using the mechanical properties measured, a series of finite element analyses coupled with a failure model was performed. Results reveal that the fracture of coating layer occurs in an irregular manner at the region where compressive deformation is dominant. Meanwhile, a series of vertical cracks perpendicular to material surface are observed at the tensile stressed-region. It is found that 0.26-0.28 of local equivalent plastic strain exists at the coating and substrate at the beginning of failure. The fracture of coating layer depends on ductility of the coating layer considerably as well.展开更多
The indentation test is a localized testing technique;therefore,the role of the material size-effect and local non-uniformity is of much importance.The influence of the heterogeneity in size-independent materials has ...The indentation test is a localized testing technique;therefore,the role of the material size-effect and local non-uniformity is of much importance.The influence of the heterogeneity in size-independent materials has been studied previously.The present work detailedly investigated the influence of the material size-effect and heterogeneity(inclusions near the indenter tip)on the indentation hardness using a size-dependent strain gradient plastic theory.And it was found that when considering the material size-ffect,shallow hard inclusions in the heterogeneous materials more significantly enhance the material indentation hardness compared with the size-independent materials which are based on the conventional plastic theory.This hardening effect is be-lieved to be related to the elevation of the load and local constraints of large deformation.The effect of material inhomogeneity mainly comes from the non-uniformity of the structure rather than the inclusion modulus itself especially when the size-effect is involved,and the transition range of the inclusion modulus'influence is pretty narrow.The effect of non-uniformity becomes negligible after the initial inclusion depth is larger than its diameter.The horizontal offset of the indenter from the inclusion is also of much sensitivity to the influence of the heterogeneous indentation.This paper focuses on the scaling relationships in micro-and nanoindentation,the influence of non-uniformity in microscopic materials is studied and supplemented as well.展开更多
Based on load-displacement curves,indentation is widely used to extract the elastoplastic properties of materials.It is generally believed that such a measure is non-unique and a full stress-strain curve cannot be obt...Based on load-displacement curves,indentation is widely used to extract the elastoplastic properties of materials.It is generally believed that such a measure is non-unique and a full stress-strain curve cannot be obtained using plural sharp and deep spherical indenters.In this paper we show that by introducing an additional dimensionless function of A/A (the ratio of residual area to the area of an indenter profile) in the reverse analysis,the elastoplastic properties of several unknown materials that exhibit visually indistinguishable load-displacement curves can be uniquely determined with a sharp indentation.展开更多
Ultrasonic vibration can be used for the micro-molding of metallic glasses(MGs)due to stress-softening and fast surface-diffusion effects.However,the structural rearrangement under ultrasonic vibration and its impact ...Ultrasonic vibration can be used for the micro-molding of metallic glasses(MGs)due to stress-softening and fast surface-diffusion effects.However,the structural rearrangement under ultrasonic vibration and its impact on the mechanical response of metallic glasses remain a puzzle.In this work,the plastic flow of the Zr35Ti30Cu8.25Be26.75 metallic glass with the applied ultrasonic-vibration energy of 140 J was investigated by nanoindentation.Both Kelvin and Maxwell-Voigt models have been adopted to analyze the structural evolution during the creep deformation.The increase of the characteristic relaxation time and the peak intensity of relaxation spectra can be found in the sample after ultrasonic vibration.It effectively improves the activation energy of atomic diffusion during the glass transition(Eg)and the growth of the crystal nucleus(Ep).A more homogenous plastic deformation with a weak loading-rate sensitivity of stress exponent is observed in the ultrasonic-vibrated sample,which coincides with the low pile-up and penetration depth as shown in the cross profile of indents.The structural rearrangement under resonance actuation demonstrated in this work might help us better understand the defect-activation mechanism for the plastic flow of amorphous systems.展开更多
基金Project(51174235)supported by the National Natural Science Foundation of China
文摘Hardness of materials depends significantly on the indentation size and grain/sub-grain size via microindentation and nanoindentation tests of high-purity tungsten with different structures.The grain boundary effect and indentation size effect were explored.The indentation hardness was fitted using the Nix-Gao model by considering the scaling factor.The results show that the scaling factor is barely correlated with the grain/sub-grain size.The interaction between the plastically deformed zone(PDZ) boundary and the grain/sub-grain boundary is believed to be the reason that leads to an increase of the measured hardness at the specific depths.Results also indicate that the area of the PDZ is barely correlated with the grain/sub-grain size,and the indentation hardness starts to stabilize once the PDZ expands to the dimension of an individual grain/sub-grain.
基金Projects(50531060,10525211,10828205)supported by the National Natural Science Foundation of ChinaProject(10525211)supported by National Science Found for Distinguished Young Scholars of ChinaProject(076044)supported by the Cultivation Fund of the Key Scientific and Technical Innovation Project,Ministry of Education of China
文摘To characterize the elastic-plastic properties of thin film materials on elastic-plastic substrates,a simple theory model was proposed,which included three steps:dimensionless analysis,finite element modeling and data fitting.The dimensionless analysis was applied to deriving two preliminary nondimensional relationships of the material properties,and finite element modeling and data fitting were carried out to establish their explicit forms.Numerical indentation tests were carried out to examine the effectiveness of the proposed model and the good agreement shows that the proposed theory model can be applied in practice.
基金supported by Basic Science Research Program through the National Research Foundation of Korea (NRF) funded by the Ministry of Education, Science and Technology (2009-0074936)
文摘Mechanical properties of galvannealed (GA) steel sheet used for automotive exposed panel and predicted failure phenomenon of its coating layer were evaluated using finite element method. V-bending test was performed to understand better the fracture of coating layer of GA steel sheet during plastic deformation. Yield strength of the coating layer was calculated by using a relative difference between hardness of coating layer measured from the nano-indentation test and that of substrate. To measure shearing strength at the interface between substrate and coating layer, shearing test with two specimens attached by an adhesive was carried out. Using the mechanical properties measured, a series of finite element analyses coupled with a failure model was performed. Results reveal that the fracture of coating layer occurs in an irregular manner at the region where compressive deformation is dominant. Meanwhile, a series of vertical cracks perpendicular to material surface are observed at the tensile stressed-region. It is found that 0.26-0.28 of local equivalent plastic strain exists at the coating and substrate at the beginning of failure. The fracture of coating layer depends on ductility of the coating layer considerably as well.
基金the National Natural Science Foundation of China(Grant Nos.11890681,12032001,and 11521202).
文摘The indentation test is a localized testing technique;therefore,the role of the material size-effect and local non-uniformity is of much importance.The influence of the heterogeneity in size-independent materials has been studied previously.The present work detailedly investigated the influence of the material size-effect and heterogeneity(inclusions near the indenter tip)on the indentation hardness using a size-dependent strain gradient plastic theory.And it was found that when considering the material size-ffect,shallow hard inclusions in the heterogeneous materials more significantly enhance the material indentation hardness compared with the size-independent materials which are based on the conventional plastic theory.This hardening effect is be-lieved to be related to the elevation of the load and local constraints of large deformation.The effect of material inhomogeneity mainly comes from the non-uniformity of the structure rather than the inclusion modulus itself especially when the size-effect is involved,and the transition range of the inclusion modulus'influence is pretty narrow.The effect of non-uniformity becomes negligible after the initial inclusion depth is larger than its diameter.The horizontal offset of the indenter from the inclusion is also of much sensitivity to the influence of the heterogeneous indentation.This paper focuses on the scaling relationships in micro-and nanoindentation,the influence of non-uniformity in microscopic materials is studied and supplemented as well.
基金supported by the National Natural Science Foundation of China (Grant Nos.11102176,11002122,51172192,and 11172258)the Natural Science Foundation of Hunan Province for Innovation Group(Grant No.09JJ7004)the Key Special Program for Science and Technology of Hunan Province (Grant No.2009FJ1002)
文摘Based on load-displacement curves,indentation is widely used to extract the elastoplastic properties of materials.It is generally believed that such a measure is non-unique and a full stress-strain curve cannot be obtained using plural sharp and deep spherical indenters.In this paper we show that by introducing an additional dimensionless function of A/A (the ratio of residual area to the area of an indenter profile) in the reverse analysis,the elastoplastic properties of several unknown materials that exhibit visually indistinguishable load-displacement curves can be uniquely determined with a sharp indentation.
基金the National Natural Science Foundation of China(51631003,51871157 and 51601038)the Key Basic and Applied Research Program of Guangdong Province,China(2019B030302010)+3 种基金the Natural Science Foundation of Jiangsu Province,China(BK20171354)the Fundamental Research Funds for the Central Universities(2242020K40002)the Research and Practice Innovation Program for Postgraduates in Jiangsu Province(SJCX20_0038)Jiangsu Key Laboratory for Advanced Metallic Materials(BM2007204)。
文摘Ultrasonic vibration can be used for the micro-molding of metallic glasses(MGs)due to stress-softening and fast surface-diffusion effects.However,the structural rearrangement under ultrasonic vibration and its impact on the mechanical response of metallic glasses remain a puzzle.In this work,the plastic flow of the Zr35Ti30Cu8.25Be26.75 metallic glass with the applied ultrasonic-vibration energy of 140 J was investigated by nanoindentation.Both Kelvin and Maxwell-Voigt models have been adopted to analyze the structural evolution during the creep deformation.The increase of the characteristic relaxation time and the peak intensity of relaxation spectra can be found in the sample after ultrasonic vibration.It effectively improves the activation energy of atomic diffusion during the glass transition(Eg)and the growth of the crystal nucleus(Ep).A more homogenous plastic deformation with a weak loading-rate sensitivity of stress exponent is observed in the ultrasonic-vibrated sample,which coincides with the low pile-up and penetration depth as shown in the cross profile of indents.The structural rearrangement under resonance actuation demonstrated in this work might help us better understand the defect-activation mechanism for the plastic flow of amorphous systems.