Ti_(2)AlC/TiAl composites with different volume fractions were prepared by hot pressing technology,and their reinforced structural characteristics and mechanical properties were evaluated.The results showed that when ...Ti_(2)AlC/TiAl composites with different volume fractions were prepared by hot pressing technology,and their reinforced structural characteristics and mechanical properties were evaluated.The results showed that when the reinforced phase volume fraction of Ti_(2)AlC was 20%,three-dimensional interpenetrating network structures were formed in the composites.Above 20%,Ti_(2)AlC phase in the composites accumulated and grew to form thick skeletal networks.The microplastic deformation behavior of Ti_(2)AlC phase,such as kink band and delamination,improved the fracture toughness of the composites.Comparative analysis indicated that the uniform and small interconnecting network structures could further reinforce the composites.The bending strengths of composites prepared with 20 vol.%Ti_(2)AlC reached(900.9±45.0)MPa,which was 25.5% higher than that of TiAl matrix.In general,the co-continuous Ti_(2)AlC/TiAl composite with excellent mechanical properties can be prepared by powder metallurgy method.展开更多
Microstructural characteristics and mechanical behavior of hot extruded Al5083/B4C nanocomposites were studied.Al5083and Al5083/B4C powders were milled for50h under argon atmosphere in attrition mill with rotational s...Microstructural characteristics and mechanical behavior of hot extruded Al5083/B4C nanocomposites were studied.Al5083and Al5083/B4C powders were milled for50h under argon atmosphere in attrition mill with rotational speed of400r/min.For increasing the elongation,milled powders were mixed with30%and50%unmilled aluminum powder(mass fraction)with meanparticle size of>100μm and<100μm and then consolidated by hot pressing and hot extrusion with9:1extrusion ratio.Hot extrudedsamples were studied by optical microscopy,scanning electron microscopy(SEM),energy dispersive spectroscopy(EDS),transmission electron microscopy(TEM),tensile and hardness tests.The results showed that mechanical milling process andpresence of B4C particles increase the yield strength of Al5083alloy from130to566MPa but strongly decrease elongation(from11.3%to0.49%).Adding<100μm unmilled particles enhanced the ductility and reduced tensile strength and hardness,but usingthe>100μm unmilled particles reduced the tensile strength and ductility at the same time.By increasing the content of unmilledparticles failure mechanism changed from brittle to ductile.展开更多
The fabrication of high strength Al 7068?5%TiC (mass fraction) nanocomposite was studied by mechanical alloying and hot pressing routes. Considering densification importance and grain growth effects, hot pressing p...The fabrication of high strength Al 7068?5%TiC (mass fraction) nanocomposite was studied by mechanical alloying and hot pressing routes. Considering densification importance and grain growth effects, hot pressing process conditions for producing bulk nanocomposite were optimized using statistical Taguchi method based on compressive strength achievement. The Taguchi results indicate that 30 min hot pressing under pressure of 500 MPa at 385 °C provides high compressive strength and hardness of 938 MPa and HV 265, respectively. More interestingly, analysis of variance proves that the applied pressure is the most influential factor for hot pressing of the nanocomposite. The contribution percentages of factors in hot pressing terms are as follows: applied pressure (61.3%), exposed temperature (29.53%) and dwelling hot pressing time (4.49%).展开更多
Nanoindentation tests were conducted to investigate the near-surface mechanical properties of the individual components(fiber and matrix) for three-dimensional reinforced carbon/carbon composites(3D C/C).Optical micro...Nanoindentation tests were conducted to investigate the near-surface mechanical properties of the individual components(fiber and matrix) for three-dimensional reinforced carbon/carbon composites(3D C/C).Optical microscope and polarizing light microscope were used to characterize the microstructure of 3D C/C.The microscopy results show that large number of pores and cracks exist at both bundle/matrix interface and pitch carbon matrix.These defects have important effect on the mechanical behavior of 3D C/C.The in situ properties for components of 3D C/C were acquired by nanoindentation technique.Relative to the matrix sample,the fiber samples have more larger values for modulus,stiffness and hardness.However,there is no significant difference of modulus and stiffness among fiber samples with different directions.展开更多
A new style Ni-containing alumina ceramic foam based continuous three-dimensional interconnected skeleton was prepared by impregnating a polymeric sponge with aqueous ceramic slurry.Subsequently,alumina ceramic foam/s...A new style Ni-containing alumina ceramic foam based continuous three-dimensional interconnected skeleton was prepared by impregnating a polymeric sponge with aqueous ceramic slurry.Subsequently,alumina ceramic foam/steel metal matrix composites(MMCs) were prepared successfully by sand mold casting technique.The microstructure and mechanical properties of MMCs were investigated by SEM,EDS and compressive test.The results show that the depth of infiltration is about 40 μm to the bonding interface of ceramic/steel and the fracture strength σmax and plastic strain limit εp of composite are 520 MPa and 11.2%,respectively.The fretting wear mechanism of MMCs is mainly performed at the oxidative wear mode with lower load/friction frequency and the predominant oxidation wear together with slight adhesive wear and abrasive wear multiple mode with higher load/ friction frequency.Moreover,the infiltration bonding and continuous three-dimensional interconnected ceramic skeleton play a vital role in the stability of the bonding interface and excellent mechanical properties.展开更多
According to a mathematical model which describes the curing process of composites constructed from continuous fiber-reinforced, thermosetting resin matrix prepreg materials, and the consolidation of the composites, t...According to a mathematical model which describes the curing process of composites constructed from continuous fiber-reinforced, thermosetting resin matrix prepreg materials, and the consolidation of the composites, the solution method to the model is made and a computer code is developed, which for flat-plate composites cured by a specified cure cycle, provides the variation of temperature distribution, the cure reaction process in the resin, the resin flow and fibers stress inside the composite, the void variation and the residual stress distribution.展开更多
To consider the internal pressure loaded by both the cylindrical Ti-Al alloy liner and the carbon fiber resin composite (CFRC) wound layers, two models are built. The first one is a cylinder loaded with the internal p...To consider the internal pressure loaded by both the cylindrical Ti-Al alloy liner and the carbon fiber resin composite (CFRC) wound layers, two models are built. The first one is a cylinder loaded with the internal pressure in the hoop direction only. In this model, the total hoop direction load is distributed over all layers under the internal pressure. The second one is a cylinder loaded with the internal pressure in the axial direction only. In this model, the total axial load is distributed over all cylinders under the internal pressure. Taking the boundary conditions of the continuous displacement between layers into account, a group of equations are built. From these equations, we get the solutions of stresses in both hoop direction and axial direction loaded by every layer under internal pressures. After the stresses are obtained, a reasonable design can be done. An example is given in the final section of this study.展开更多
基金the financial supports from the National Natural Science Foundation of China(No.52065009)the Joint Funds of the Science and Technology Foundation of Guizhou Province,China(No.20157219)the Science and Technology Planning Project of Guizhou Province,China(No.20191069).
文摘Ti_(2)AlC/TiAl composites with different volume fractions were prepared by hot pressing technology,and their reinforced structural characteristics and mechanical properties were evaluated.The results showed that when the reinforced phase volume fraction of Ti_(2)AlC was 20%,three-dimensional interpenetrating network structures were formed in the composites.Above 20%,Ti_(2)AlC phase in the composites accumulated and grew to form thick skeletal networks.The microplastic deformation behavior of Ti_(2)AlC phase,such as kink band and delamination,improved the fracture toughness of the composites.Comparative analysis indicated that the uniform and small interconnecting network structures could further reinforce the composites.The bending strengths of composites prepared with 20 vol.%Ti_(2)AlC reached(900.9±45.0)MPa,which was 25.5% higher than that of TiAl matrix.In general,the co-continuous Ti_(2)AlC/TiAl composite with excellent mechanical properties can be prepared by powder metallurgy method.
文摘Microstructural characteristics and mechanical behavior of hot extruded Al5083/B4C nanocomposites were studied.Al5083and Al5083/B4C powders were milled for50h under argon atmosphere in attrition mill with rotational speed of400r/min.For increasing the elongation,milled powders were mixed with30%and50%unmilled aluminum powder(mass fraction)with meanparticle size of>100μm and<100μm and then consolidated by hot pressing and hot extrusion with9:1extrusion ratio.Hot extrudedsamples were studied by optical microscopy,scanning electron microscopy(SEM),energy dispersive spectroscopy(EDS),transmission electron microscopy(TEM),tensile and hardness tests.The results showed that mechanical milling process andpresence of B4C particles increase the yield strength of Al5083alloy from130to566MPa but strongly decrease elongation(from11.3%to0.49%).Adding<100μm unmilled particles enhanced the ductility and reduced tensile strength and hardness,but usingthe>100μm unmilled particles reduced the tensile strength and ductility at the same time.By increasing the content of unmilledparticles failure mechanism changed from brittle to ductile.
文摘The fabrication of high strength Al 7068?5%TiC (mass fraction) nanocomposite was studied by mechanical alloying and hot pressing routes. Considering densification importance and grain growth effects, hot pressing process conditions for producing bulk nanocomposite were optimized using statistical Taguchi method based on compressive strength achievement. The Taguchi results indicate that 30 min hot pressing under pressure of 500 MPa at 385 °C provides high compressive strength and hardness of 938 MPa and HV 265, respectively. More interestingly, analysis of variance proves that the applied pressure is the most influential factor for hot pressing of the nanocomposite. The contribution percentages of factors in hot pressing terms are as follows: applied pressure (61.3%), exposed temperature (29.53%) and dwelling hot pressing time (4.49%).
基金Project(61391) supported by the National Security Basic Research Program of ChinaProject (91016029) supported by the National Natural Science Foundation of China
文摘Nanoindentation tests were conducted to investigate the near-surface mechanical properties of the individual components(fiber and matrix) for three-dimensional reinforced carbon/carbon composites(3D C/C).Optical microscope and polarizing light microscope were used to characterize the microstructure of 3D C/C.The microscopy results show that large number of pores and cracks exist at both bundle/matrix interface and pitch carbon matrix.These defects have important effect on the mechanical behavior of 3D C/C.The in situ properties for components of 3D C/C were acquired by nanoindentation technique.Relative to the matrix sample,the fiber samples have more larger values for modulus,stiffness and hardness.However,there is no significant difference of modulus and stiffness among fiber samples with different directions.
基金Project(51271080) supported by the National Natural Science Foundation of ChinaProject(2012JSSPITP1968) supported by the Innovative Foundation for Students of Jiangsu Province,ChinaProject(CKJB201204) supported by the Innovation Fund of Nanjing Institute of Technology,China
文摘A new style Ni-containing alumina ceramic foam based continuous three-dimensional interconnected skeleton was prepared by impregnating a polymeric sponge with aqueous ceramic slurry.Subsequently,alumina ceramic foam/steel metal matrix composites(MMCs) were prepared successfully by sand mold casting technique.The microstructure and mechanical properties of MMCs were investigated by SEM,EDS and compressive test.The results show that the depth of infiltration is about 40 μm to the bonding interface of ceramic/steel and the fracture strength σmax and plastic strain limit εp of composite are 520 MPa and 11.2%,respectively.The fretting wear mechanism of MMCs is mainly performed at the oxidative wear mode with lower load/friction frequency and the predominant oxidation wear together with slight adhesive wear and abrasive wear multiple mode with higher load/ friction frequency.Moreover,the infiltration bonding and continuous three-dimensional interconnected ceramic skeleton play a vital role in the stability of the bonding interface and excellent mechanical properties.
文摘According to a mathematical model which describes the curing process of composites constructed from continuous fiber-reinforced, thermosetting resin matrix prepreg materials, and the consolidation of the composites, the solution method to the model is made and a computer code is developed, which for flat-plate composites cured by a specified cure cycle, provides the variation of temperature distribution, the cure reaction process in the resin, the resin flow and fibers stress inside the composite, the void variation and the residual stress distribution.
文摘To consider the internal pressure loaded by both the cylindrical Ti-Al alloy liner and the carbon fiber resin composite (CFRC) wound layers, two models are built. The first one is a cylinder loaded with the internal pressure in the hoop direction only. In this model, the total hoop direction load is distributed over all layers under the internal pressure. The second one is a cylinder loaded with the internal pressure in the axial direction only. In this model, the total axial load is distributed over all cylinders under the internal pressure. Taking the boundary conditions of the continuous displacement between layers into account, a group of equations are built. From these equations, we get the solutions of stresses in both hoop direction and axial direction loaded by every layer under internal pressures. After the stresses are obtained, a reasonable design can be done. An example is given in the final section of this study.