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离子色谱法同时测定奶粉中硝酸盐和多种磷酸盐 被引量:3
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作者 梁钰莹 江琦 +3 位作者 李锦清 张施敬 伍志航 綦艳 《食品工业》 CAS 北大核心 2018年第7期327-330,共4页
为了对硝酸盐和多种磷酸盐的稳定性进行研究,建立了离子色谱同时测定奶粉中硝酸盐和多种磷酸盐的分析方法。以水为提取液,超声辅助提取目标成分,沉淀蛋白,过柱净化,调节样液p H后,用AS11-HC阴离子交换柱进行分离,Na OH溶液梯度淋洗,电... 为了对硝酸盐和多种磷酸盐的稳定性进行研究,建立了离子色谱同时测定奶粉中硝酸盐和多种磷酸盐的分析方法。以水为提取液,超声辅助提取目标成分,沉淀蛋白,过柱净化,调节样液p H后,用AS11-HC阴离子交换柱进行分离,Na OH溶液梯度淋洗,电导检测器检测。试验结果表明,5种阴离子NO_3^-,P_2O_7^(4-),P_3O_(10)^(5-),P_3O_9^(3-),P_6O_(18)^(6-)分离效果满意,线性关系良好,相关系数为0.999 5~1.000 0,方法检出限为0.04~0.5 mg/kg,平均加标回收率为85.1%~100.5%,相对标准偏差为0.7%~7.6%。该方法灵敏度高,线性良好,精密度高,操作简便,检测时间短。 展开更多
关键词 离子色谱 硝酸盐 多种磷酸盐 奶粉
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Hydrographical parameters and phytoplankton assemblages along the Pondicherry—Nagapattinam coastal waters,southeast coast of India
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作者 Pitchai SAMPATHKUMAR Srinivasan BALAKRISHNAN +11 位作者 Krishnamoorthy KAMALAKANNAN Rethinavelu SANKAR Lakshmanan RAMKUMAR Subramani RAMESH Neelamegam KABILAN Thambusamy SURESHKUMAR Chellam THENMOZHI Mookapillai GOPINATH Sekar JAYASUDHA Amalanathan AROKIYASUNDRAM Thiruvarasan LENIN Thangavelu BALASUBRAMANIAN 《Advances in Climate Change Research》 SCIE CSCD 2015年第1期36-45,共10页
Hydrographical parameters and phytoplankton assemblages were determined along the Pondicherry, Parangipettai and Nagapattinam coastal waters, southeast coast of India. All the hydrographical parameters such as sea sur... Hydrographical parameters and phytoplankton assemblages were determined along the Pondicherry, Parangipettai and Nagapattinam coastal waters, southeast coast of India. All the hydrographical parameters such as sea surface temperature, salinity, p H, total alkalinity, dissolved oxygen and nutrients like nitrate, nitrite, inorganic phosphate and reactive silicate, chlorophyll a and phytoplankton assemblages were studied for a period of five months(May, August, September 2010, March and November 2011). Over 121 species of phytoplankton represented by 93 species of diatoms, 16 species of dinoflagellates, 9 species of blue-green algae, 2 species of greens and 1 species of silicoflagellate were recorded. High phytoplankton species diversity was found in March 2011 when salinity and nitrate concentrations were low and reactive silicate and inorganic phosphates were moderate. Species diversity was low during May 2010 when increased sea surface temperature, salinity and low nutrients availability were observed. Coscinodiscus centralis, Diatoma vulgaris and Proboscia alata were dominant, especially Coscinodiscus sp. distributed in all stations whereas Skeletonema costatum, Odontella sinensis and Ditylum brightwellii were abundant in August and September 2010. From principal component analysis and multiple regression analysis, it is evident that variables like sea surface temperature and dissolved oxygen are the most important factors influencing the seasonal pattern of phytoplankton population. 展开更多
关键词 Hydrographical parameters PHYTOPLANKTON Southeast coast Bay of Bengal Seasonal variations
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