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大相比鼓泡油膜萃取氰化废水中的低浓度金 被引量:3
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作者 刘杰 黄焜 +1 位作者 吴怀之 刘会洲 《中国有色金属学报》 EI CAS CSCD 北大核心 2018年第1期199-204,共6页
提出一种大相比鼓泡油膜萃取新方法,从氰化提金废水中萃取回收极低浓度金。考察季铵盐N263萃取体系大相比鼓泡油膜萃取过程的水相流量、油相流量、有机相负载量、有机相再生等因素对极低浓度金萃取回收的影响。结果表明:大相比鼓泡油膜... 提出一种大相比鼓泡油膜萃取新方法,从氰化提金废水中萃取回收极低浓度金。考察季铵盐N263萃取体系大相比鼓泡油膜萃取过程的水相流量、油相流量、有机相负载量、有机相再生等因素对极低浓度金萃取回收的影响。结果表明:大相比鼓泡油膜萃取可高效、经济地回收氰化提金废水中的极低浓度金。萃余液中金浓度可降至0.01 mg/L以下,金萃取回收率达99%以上。低浓度金的萃取速率取决于水相流量、气泡表面包覆的有机萃取剂油膜层厚度、以及有机油膜层中的金属离子负载量等。 展开更多
关键词 萃取 大相比 油膜 氰化 低浓度
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离心萃取-紫外光谱法测定可乐饮料中咖啡因的含量 被引量:28
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作者 丁明珍 邹建凯 《分析化学》 SCIE EI CAS CSCD 北大核心 2008年第3期381-384,共4页
建立了一种快速、准确,溶剂消耗少的测定可乐饮料中咖啡因含量的紫外光谱分析方法,并将大相比离心萃取应用于仪器分析样品微制备过程。该方法将2mL三氯甲烷直接加入装有100μL可乐饮料的离心试管中,离心萃取3min后取清液在278nm处进行... 建立了一种快速、准确,溶剂消耗少的测定可乐饮料中咖啡因含量的紫外光谱分析方法,并将大相比离心萃取应用于仪器分析样品微制备过程。该方法将2mL三氯甲烷直接加入装有100μL可乐饮料的离心试管中,离心萃取3min后取清液在278nm处进行紫外光谱测定,操作简单、快速,重现性好,相对标准偏差小于3%;在3种可乐饮料中加入不同浓度的咖啡因标准溶液,回收率在96.6%~106.1%之间。线性范围为0.5~30mg/L,相关系数为0.9999;检出限为0.001mg/L。将本方法应用于市售可乐饮料中咖啡因含量分析,取得了满意的结果。 展开更多
关键词 离心萃取 大相比 紫外光谱 微制备 咖啡因 可乐饮料
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Spatial channel pairing-based maximum ratio combining algorithm for cooperative relay networks
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作者 胡锦松 束锋 +4 位作者 许正文 阙非 黄晓晖 刘婷婷 陆锦辉 《Journal of Southeast University(English Edition)》 EI CAS 2016年第2期146-150,共5页
To improve the reliable performance of information transmission in cooperative relay networks, the scheme of the max-rate spatial channel pairing (SCP) based on maximum ratio combining (MRC) is proposed. The schem... To improve the reliable performance of information transmission in cooperative relay networks, the scheme of the max-rate spatial channel pairing (SCP) based on maximum ratio combining (MRC) is proposed. The scheme includes three steps: channel phase cancellation, MRC, and SCP. Eventually, the solution of the scheme is modeled as convex optimization. The objective function of the optimization problem is to maximize the transmission rate and the optimization variable is the strategy of pairing between the uplink spatial sub-channels of each user and the corresponding downlink spatial ones. The theorem of the arrangement inequalities is adopted to obtain the approximate closed-form solution of the optimal pairing for this convex optimization. Simulation results demonstrate that compared to the existing distributed space-time block coding and coherent combined schemes without SCP, the proposed max-rate SCP plus MRC algorithm achieves appreciable improvements in symbol error rate in medium and high signal-to-noise ratio regimes. The achievable performance gain is due to the use of maxrate SCP. 展开更多
关键词 RELAY maximum ratio combining coherentcombining spatial channel pairing distributed space-timeblock coding
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Microstructure and mechanical properties of TC4 titanium alloy K-TIG welded joints 被引量:12
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作者 Shu-wan CUI Yong-hua SHI Cheng-shi ZHANG 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2021年第2期416-425,共10页
The 12 mm-thick Ti−6Al−4V(TC4)titanium alloy plates were welded using keyhole tungsten inert gas(K-TIG)welding at various heat inputs.The microstructure,grain boundary(GB)characteristics and mechanical properties of t... The 12 mm-thick Ti−6Al−4V(TC4)titanium alloy plates were welded using keyhole tungsten inert gas(K-TIG)welding at various heat inputs.The microstructure,grain boundary(GB)characteristics and mechanical properties of the weld metal zone(WMZ)were analyzed.The test results show that the K-TIG welds are well formed,and no obvious defects are observed when the heat input is 2.30−2.62 kJ/mm.When the heat input gradually increases,αlaths increase in length,andα′phase and residualβphase are reduced.The electron backscatter diffraction(EBSD)test results indicate that the high-angle GB proportion in the WMZ increases with the increase of heat input.The tensile strength of the WMZ gradually decreases and the elongation of the WMZ increases when the heat input increases from 2.30 to 2.62 kJ/mm.The impact toughness of the WMZ increases as the heat input increases. 展开更多
关键词 K-TIG welding heat input α′phase high-angle grain boundary Charpy impact fracture surface
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Multi-user quantum private comparison with scattered preparation and one-way convergent transmission of quantum states 被引量:2
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作者 TianYu Ye ZhaoXu Ji 《Science China(Physics,Mechanics & Astronomy)》 SCIE EI CAS CSCD 2017年第9期7-16,共10页
Quantum private comparison(QPC) aims to accomplish the equality comparison of the secrets from different users without disclosing their genuine contents by using the principles of quantum mechanics. In this paper, we ... Quantum private comparison(QPC) aims to accomplish the equality comparison of the secrets from different users without disclosing their genuine contents by using the principles of quantum mechanics. In this paper, we summarize eight modes of quantum state preparation and transmission existing in current QPC protocols first. Then, by using the mode of scattered preparation and one-way convergent transmission, we construct a new multi-user quantum private comparison(MQPC) protocol with two-particle maximally entangled states, which can accomplish arbitrary pair's comparison of equality amongK users within one execution. Analysis turns out that its output correctness and its security against both the outside attack and the participant attack are guaranteed. The proposed MQPC protocol can be implemented with current technologies. It can be concluded that the mode of scattered preparation and one-way convergent transmission of quantum states is beneficial to designing the MQPC protocol which can accomplish arbitrary pair's comparison of equality among K users within one execution. 展开更多
关键词 multi-user quantum private comparison (MQPC) scattered preparation one-way convergent transmission
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Phase group synchronization between any signals and its physical characteristics 被引量:2
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作者 DU BaoQiang SHI LinLin +4 位作者 CHEN YaoMing DONG ShaoFeng YANG ZhiGang CAO LingZhi GUO ShuTing 《Science China(Physics,Mechanics & Astronomy)》 SCIE EI CAS 2014年第4期674-679,共6页
The phase group synchronization between any signals is further revealed,which is based on proposing the new concepts of the greatest common factor frequency,the least common multiple period,quantized phase shift resol... The phase group synchronization between any signals is further revealed,which is based on proposing the new concepts of the greatest common factor frequency,the least common multiple period,quantized phase shift resolution,equivalent phase comparison frequency and so on.Then the problem of phase comparison and processing between different frequency signals is solved and shown in detail.Using the basic principle and the variation law of group phase difference,the frequency stability better than 10-14/s can be easily obtained in the time&frequency measurement and control domain,and experimental results also show the phase relations between atomic energy level transition signal and the locked crystal oscillator signal in an active hydrogen atomic clock are strict phase group synchronization,and locked precision with 10-13/s can be reached based on phase group synchronization.The phase group synchronization can provide technical support to frequency linking among radio frequency,microwave and light frequency. 展开更多
关键词 equivalent phase comparison frequency least common multiple period group phase difference group period phase processing phase group synchronization
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