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顶空固相微萃取-气质联用法分析衡水老白干酒风味物质 被引量:9
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作者 王敏 张煜行 +6 位作者 李泽霞 姜东明 杜惠丽 程宗志 佟兰欣 张志民 肖冬光 《酿酒科技》 2015年第9期111-114,共4页
采用顶空-固相微萃取(HS-SPME)与气质联用(GC-MS)相结合对衡水老白干酒中的风味物质进行了初步分析,比较了4种不同涂层纤维的萃取头对衡水老白干酒风味成分的萃取效果和特点。结果表明,共定性衡水老白干酒风味物质101种,50/30μm DVB/CA... 采用顶空-固相微萃取(HS-SPME)与气质联用(GC-MS)相结合对衡水老白干酒中的风味物质进行了初步分析,比较了4种不同涂层纤维的萃取头对衡水老白干酒风味成分的萃取效果和特点。结果表明,共定性衡水老白干酒风味物质101种,50/30μm DVB/CAR/PDMS萃取头适用于老白干酒风味物质的分析,共定性91种主要风味物质,其中酯类47种,醇类15种,醛类8种,酮类7种,酸类4种,呋喃类3种,吡嗪类2种,萜烯类2种,其中大马士酮、里那醇是首次报道。 展开更多
关键词 顶空固相微萃取 气质联用 衡水老白干酒 风味成分 大马士 里那醇 白酒 Baijiu(liquor)
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制丝关键工艺参数对羟基化合物的影响研究 被引量:3
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作者 武凯 岳衡 +9 位作者 郑红艳 廖晓祥 杨光涛 熊开胜 魏宏 李雯琦 谭国治 易斌 段黎跃 聂蓉 《云南化工》 CAS 2018年第8期4-8,共5页
不饱和羟基化合物有增加烟草本香,改善香气质提高烟气浓度和丰富性等作用,大部分产生于制丝加工过程中的降解。通过均匀化试验设计,在一定范围内改变关键制丝工艺参数,研究了制丝加工过程中关键工艺参数对巨豆三烯酮和大马士酮相对含量... 不饱和羟基化合物有增加烟草本香,改善香气质提高烟气浓度和丰富性等作用,大部分产生于制丝加工过程中的降解。通过均匀化试验设计,在一定范围内改变关键制丝工艺参数,研究了制丝加工过程中关键工艺参数对巨豆三烯酮和大马士酮相对含量的影响。结果表明,超回蒸汽喷射比例、真空蒸湿温度、一周期抽空温度是影响纯丝中巨豆三烯酮含量的关键工艺参数,在试验范围内,随着超回蒸汽喷射比例的增加,制叶丝纯丝中巨豆三烯酮的相对含量呈上升趋势;随着真空蒸湿温度的增加,制叶丝纯丝中巨豆三烯酮质量分数先升高后降低;随真空回潮抽空温度的增加,制叶丝纯丝中巨豆三烯酮质量分数呈上升趋势。一周期抽空温度、真空蒸湿温度、超回蒸汽喷射比例、超回热风风量是影响纯丝中大马士酮含量的关键工艺参数,在试验范围内,随着一周期抽空温度的增加,制叶丝纯丝中大马士酮的含量呈上升趋势;随真空回潮蒸湿温度的增加,制叶丝纯丝中大马士酮质量分数呈抛物线趋势;随着超回蒸汽喷射比例的增加,制叶丝纯丝中大马士酮质量分数先减少后增加;随着超回热风风量的增加,制叶丝纯丝中大马士酮质量分数先增加后减少。 展开更多
关键词 均匀化设计 中式卷烟风格感官质量 品牌特征香 致香成分 羟基化合物 巨豆三烯酮 大马士
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萨达特的耶路撒冷之行
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作者 李伟 《国际展望》 1986年第15期30-32,共3页
六、法赫米背后桶刀“法赫米宣布辞职了.”这条消息几乎象萨达特总统宣布访以一样使外界震惊。人们万万没有想到萨达特倚为心腹的埃及副总理兼外长法赫米会在这种时候引退。对萨达特来说,这简直无异于背后被捅上一刀。萨达特知道法赫米... 六、法赫米背后桶刀“法赫米宣布辞职了.”这条消息几乎象萨达特总统宣布访以一样使外界震惊。人们万万没有想到萨达特倚为心腹的埃及副总理兼外长法赫米会在这种时候引退。对萨达特来说,这简直无异于背后被捅上一刀。萨达特知道法赫米反对他的耶路撒冷之行,但绝没有想到他会亮出辞职一招。 展开更多
关键词 萨达特 埃及人 大马士 穆巴拉克 以色列议会 阿萨德 以色列人 阿克萨清真寺 大卫王 实况转播
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航运业2017年有望迎来弱复苏
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《天津航海》 2017年第1期50-50,共1页
回望2016年,亏损、破产、重组成了航运市场的主题词,而与惨淡行情同步的是,航运供给侧增速大幅放缓,2017年航运主要细分市场有望迎来弱复苏。
关键词 破产保护 大马士 韩进 财报 集装箱运输 运力过剩 重组成 海运业 金融危机 名第
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交叉持股构筑产业命运共同体
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作者 杨培举 《中国船检》 2016年第4期8-12,112-113,共7页
中国远洋控股、武汉钢铁、中国船舶三家央企经过股权转换,形成了新的内部市场,一条崭新的全产业链重组路径渐渐浮现。进入2016年,航运企业和造船企业经营状况持续恶化的态势仍在蔓延,连世界航运老大马士基都要裁员了,足见航运冬天有多... 中国远洋控股、武汉钢铁、中国船舶三家央企经过股权转换,形成了新的内部市场,一条崭新的全产业链重组路径渐渐浮现。进入2016年,航运企业和造船企业经营状况持续恶化的态势仍在蔓延,连世界航运老大马士基都要裁员了,足见航运冬天有多"冷"。在这种背景下,中国航运业和造船业也在苦苦寻觅破解之道。 展开更多
关键词 交叉持股 命运共同体 武汉钢铁 大马士 全产业链 央企 破解之道 国资国企改革 武钢股份 中国船舶工业
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Ecological Suitability Assessment and Introduction Experiment on Rosa damascena trigintipetala in Sichuan Province, China 被引量:6
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作者 WANG Xiao-lan SU Chun-jiang +5 位作者 PENG Li WANG Hai-e WANG Hai-ming LIU Wei LI Ping FANG Yan 《Journal of Mountain Science》 SCIE CSCD 2014年第3期805-815,共11页
This study comprehensively considered the climate, soil, terrain, and land-use type conditions suitable for Rosa damascena trigintipetala and further established an ecological suitability evaluation model of R. damasc... This study comprehensively considered the climate, soil, terrain, and land-use type conditions suitable for Rosa damascena trigintipetala and further established an ecological suitability evaluation model of R. damascena triginffpetala in Sichuan Province, China, based on geographic information systems (GIS) and Agro-Ecological Zone (AEZ) models; then we assessed the different ecological suitability grades for this species in Sichuan Province of China and summarized the suitable land areas and spatial distribution pattern for R. damascena trigintipetala. The results show that the suitable areas (which contain highly suitable, generally suitable, and critically suitable areas) for R. damascena trigintipetala are 307.268×lO4 hm^2, which accounts for 6.34% of the total provincial area. Results also indicate that shrub land and open forest land are the major land-use types suitable for R. damascena trigintipetala, with the suitable areas of 303.162×lO4 hm2 (6.25% of the total provincial area). An introduction test was conducted in one of the suitable areas, Xichang City, which demonstrated that R. damascena trigintipetala grows well at theexperimental sites. The quality of rose oil extracted from R. damascena trigintipetala planted in Xichang meets the Bulgaria Rose Oil Standard, thus verifying the accuracy and reliability of the ecological suitability assessment results. 展开更多
关键词 Rosa damascena trigintipetala Ecological suitability INTRODUCTION Agro-ecologicalzone Sichuan Province
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Preliminary Experiences in Pheromone Trap Monitoring of Zeuzera pyrina (L.) in Syrian Apple Orchards
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作者 Adel Almanoufi Kamil Chanan +3 位作者 Majd Jamal Enrico De Lillo Eustachio Tarasco Anna Maria D'Onghia 《Journal of Agricultural Science and Technology(A)》 2012年第5期610-618,共9页
The leopard moth (Zeuzera pyrina L), is a cossid whose larvae bore into twigs, branches and trunks of various woody species, weakening and killing trees or shrubs. Recently it caused serious losses of apple trees in... The leopard moth (Zeuzera pyrina L), is a cossid whose larvae bore into twigs, branches and trunks of various woody species, weakening and killing trees or shrubs. Recently it caused serious losses of apple trees in Syria. The flight dynamics of Z. pyrina was monitored by pheromone traps (first time in Syria) compared to light trap device. This study was carried out in Damascus countryside, Qunaytirah and Sweida provinces during 2007-2008. Results indicated that the flight of moths during 2007 started in early June in Damascus countryside and Sweida provinces. The highest number of caught adults (the highest peak) was concentrated in mid July in Sweida province, whereas in Damascus countryside province there were a high peak in mid June and a small peak in early July. On the other hand, flight of moths during 2008 started in mid-May in Damascus countryside province while in Qunaytirah province started in early June. The highest number of caught adults (the highest peak) was concentrated in late July in Damascus countryside, whereas in Qunaytirah province there were small peaks in mid June and mid July. Experiments conducted to evaluate capturing efficiency of different types of traps (pheromone traps and light trap) demonstrated that there was significantly high difference within the trap devices, wherein Capta trap got the best results and caught more males than the others. 展开更多
关键词 SYRIA apple orchard leopard moth borer Zeuzera pyrina L. flight dynamics pheromone traps.
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Microclimate in Hot Dry Damascus: The Influence of the Urban Environment on Human Perception
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作者 Moohammed Wasim Yahia Erik Johansson 《Journal of Earth Science and Engineering》 2013年第8期554-561,共8页
There is a broad recognition that microclimatic conditions contribute to the quality of life in cities. A favorable microclimate has a positive influence on both commercial and social activities. The aim of this study... There is a broad recognition that microclimatic conditions contribute to the quality of life in cities. A favorable microclimate has a positive influence on both commercial and social activities. The aim of this study is to investigate the relationship between the human being and the surrounding thermal environment in terms of thermal acceptability, physical quality of the place, emotional state and the usage of the urban space in hot dry Damascus, Syria. The study is based on questionnaire surveys during the summer and winter in six locations with different microclimates. It is shown that the urban design plays a significant role in improving the microclimate, especially during the summer. The study also illustrates that when people's thermal perception is within the thermally acceptable range (i.e., slightly cool, comfortable and slightly warm) they experience the urban design as significantly more beautiful and more pleasant than during thermally unacceptable conditions. The results indicate that there is an interactive relationship between the urban design and humans' emotional state. Our findings suggest that a new perspective is needed for determining urban microclimate requirements and incorporating them into the urban design process to enhance the thermal environment in outdoor urban spaces in Damascus. 展开更多
关键词 Damascus hot dry climate outdoor urban spaces thermal perception urban design.
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Proteome Analysis in the Discovery of Serological Pregnancy Biomarkers in Damascus Goats
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作者 Ibrahim Noor Syaheera Taib Mohamad Aziz Shuib Adawiyah Suriza 《Journal of Agricultural Science and Technology(A)》 2013年第6期465-474,共10页
Early detection of pregnancy is advantageous to breeders. However, tools that were used in the early pregnancy detection are expensive, laboratory-based and not efficient and applicable enough in the field to farmers.... Early detection of pregnancy is advantageous to breeders. However, tools that were used in the early pregnancy detection are expensive, laboratory-based and not efficient and applicable enough in the field to farmers. Thus, there is a need to find a biomarker which not only can detect pregnancy but also could be applied to the livestock on the field. Proteomic approach was used in this study as to search for early pregnancy biomarker. When goat sera at day 14 of gestation were resolved by using two dimensional gel electrophoresis, five differentially expressed proteins were detected. Four of the proteins were identified as albumin precursors, immunoglobulin lambda light chain and zinc-alpha-2-glycoprotein. Pregnancy associated glycoprotein-1 was detected by using liquid chromatography mass spectrometry and the protein was validated by immunoblotting. These proteins have potential to be used as a biomarker for early pregnancy detection, however, more extensive analysis are needed to validate its possibility. 展开更多
关键词 Damascus serum PAG pregnancy biomarker PROTEOMIC Maldi-Tof/Tof LC-MS/MS.
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Japanese Cooperation for Urban Planning in the Old Capital of Damascus
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作者 Kosuke Matsubara 《Journal of Civil Engineering and Architecture》 2013年第4期487-505,共19页
Historic cities are cultural achievements that are gradually created by inhabitants over the centuries. In developed countries, the conservation of historic cities seems to be generally acknowledged as a method of com... Historic cities are cultural achievements that are gradually created by inhabitants over the centuries. In developed countries, the conservation of historic cities seems to be generally acknowledged as a method of community development that does not depend on huge exploitation. On the other hand, no sufficient countermeasures have been taken in developing countries because most native stakeholders are still interested in development. Here the author could focus on so-called "international cooperation", but urban conservation for historic cities where inhabitants actually live is still a minor consideration except for some government-based conservation projects for monuments and isolated examples of cultural heritage. In this paper, the example was taken of a conservation project which has been carried out by JICA (Japanese International Cooperation Agency) in Damascus, the old capital of Syria. The target area for the project is "Qanawat South". Although the origin of"Qanawat South" dates back to the Roman age, efforts for urban conservation have not been well organized, partly because the area is located outside of the so-called old city registered as a world heritage site. For example, the master plan of 1968 indicated the redistribution of the traditional quarters, while some conservation laws have been restricting the regeneration of the area. Moreover, there is not yet any consensus among the stakeholders concerning the historical value of the quarter, they are still questioning why the area should be conserved rather than being freely sold or developed and what and how they should contribute to conservation. Based on analysis of the actual situation of Qasr al-Hajjaj Street, this paper examines a method called "restoration-type" facade improvement adopted by JICA, for which the final goal is not only to maintain the appearance of the street but also to activate the life of the habitants of the street. 展开更多
关键词 JICA Gyoji Banshoya Damascus facade improvement architectural vocabulary.
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The Study of Effervescent Tablet Processing Using Red Roses (Rosa damascena Mill) Pigments Extract
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作者 Elfi Anis Saati Siti Zaenab +1 位作者 Simon Bambang Widjanarko Yunianta 《Journal of Food Science and Engineering》 2012年第2期88-94,共7页
Rose is one of the farming products that used as an accessory plantation, which is also known to contain vitamin C and anthocyanins which can be used as an antioxidant. The purpose of this study is to identify the col... Rose is one of the farming products that used as an accessory plantation, which is also known to contain vitamin C and anthocyanins which can be used as an antioxidant. The purpose of this study is to identify the colour effect of flower through the quality effervescent tablet, to know the interaction between the flower colour and the sugar type through the quality effervescent rose tablet. This study was done with two steps. Step I was divided into 2 levels of examinations using simple random: Rose colouring, M1 (dark red) and M2 (pink), while step II consisted of three levels of examinations, those were G 1 (sucrose), G2 (dextrose), and G3 (sorbitol). The result showed that the dark red colour has a better extract pigment quality, the level of the light color (L) was 77.3 and the redness level (b+) was 25.033. The best rose effervescent tablet was produced by the combination of M 1 G3 (dark red: corn sugar/sorbitol), that has 8.179% of water content; the solute velocity was 0.029 g/sec; the lightness level (L) was 84.133, the redness level (a+) was 18.3. The product of the rose effervescent drinks has a value of 6.46 pH; viscosities 342.867 cps and total of sugar 52.150%. 展开更多
关键词 Red rose ANTHOCYANIN PIGMENT effervescent.
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波斯湾还会有一场风波?——关于阿布穆萨岛的争端
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作者 张良福 《世界知识》 北大核心 1992年第20期14-15,共2页
行动和指责海湾合作委员会(沙特、科威特、阿联酋、巴林、卡塔尔和阿曼)外长会议于9月9日发表公报,对阿联酋与伊朗之间的阿布穆萨岛领土争端表示极大关注,要求公正合理地解决这一争端。
关键词 穆萨 阿布 外长会议 领土争端 海湾合作委员会 大马士 公正合理 伊朗人 穆巴拉克 外交部发言人
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蟒蛇巴布 三 首次猎杀
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作者 雨街 吉春鸣(图) 《金色少年(读写小达人)》 2019年第9期2-15,共14页
目睹了獴蛇激战,巴布对天敌有了更深刻的认识。这时,一场新的战争又出现在它眼前,这次的主角是猎豹鲍威尔和角马耳它。在角马耳它落地的同时,猎豹鲍威尔也重重地砸在耳它的肚子上。肚子柔软得就像一个保护气垫,鲍威尔的身体只是颠簸了一... 目睹了獴蛇激战,巴布对天敌有了更深刻的认识。这时,一场新的战争又出现在它眼前,这次的主角是猎豹鲍威尔和角马耳它。在角马耳它落地的同时,猎豹鲍威尔也重重地砸在耳它的肚子上。肚子柔软得就像一个保护气垫,鲍威尔的身体只是颠簸了一下,然后借势向下一压,张嘴就咬着了耳它的喉头,这也是猎豹的惯用伎俩,猎物很难再逃脱,很快就会因窒息死亡。 展开更多
关键词 胡兀鹫 大马士 鲍威尔
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Discussion of Random and Informal Settlements in Damascus
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作者 KHADOUR Yassar KAFA Main 《Geo-Spatial Information Science》 2009年第4期289-295,共7页
Toadies cities are accumulating the global population in their territories, occurring formally and informally. The increase of urban informality is the most significant trend shaping the 21st century world. Furthermor... Toadies cities are accumulating the global population in their territories, occurring formally and informally. The increase of urban informality is the most significant trend shaping the 21st century world. Furthermore, the urban informality "theory" should be considered in urbanization courses and development studies. With the rapid economic market development, changes mapped the major Syrian cities. Damascus is in the midst of a profound transformation of architectural and planning changes. Damascus urbanization is crowded simultaneously with informal settlements. In consequence, a detonation of urban sprawl placing random districts and informal settlements around the city (elmokhalafat & elmanatiq elashwaiya) Damascus urban informality is a way of supplying shelters and houses as a fundamental human need. The study hereby high-lights the informal phenomenon and its effects on the city at present through analytical study showing solutions and asking questions, and, finally, deals with informality in an urbanized way with self-help constructs and upgrades to aid the low income and urban poor. 展开更多
关键词 Damascus city random districts informal settlements urban informality
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